scholarly journals Fatty Acids Composition of Lard by Gas-Chromatography

1964 ◽  
Vol 11 (12) ◽  
pp. 530-533
Author(s):  
TOSHIMI AKIYA ◽  
MEGUMI YAMAZAKI
1998 ◽  
Vol 358 (2) ◽  
pp. 163-175 ◽  
Author(s):  
Dong-Sun Lee ◽  
Bong-Soo Noh ◽  
Sun-Young Bae ◽  
Kun Kim

2012 ◽  
Vol 18 (4-1) ◽  
pp. 555-561 ◽  
Author(s):  
Djura Vujic ◽  
Marijana Acanski ◽  
Marija Bodroza-Solarov ◽  
Nikola Hristov ◽  
Milica Krunic

Gas chromatography with mass spectrometry was used for performing a qualitative analysis of liposoluble flour extract made of different types of small grains (bread wheat, barley and triticale). The results show that the dominant methyl-esters of fatty acids composition is same for all samples, but the percentage of their representation in various types of small grains is different. Transesterification reagent was TMSH (Trimethylsulfonium hydroxide, 0.2M in methanol). With transesterification reaction fatty acids from acilglycerol esterifyed to methyl-esters. In all extract analyzed methyl linoleate predominated, followed by methyl palmitate, methyl oleate and methyl stearate in decreasing order. The following tests cluster analysis was used for the comparison of the liposoluble flour extract different types of small grains.


Author(s):  
Jansen Silalahi ◽  
Lida Karo Karo ◽  
Siti Morin Sinaga ◽  
Yosy Cinthya Eriwaty Silalahi

The nutritional value and biochemical properties of oil are measured by the fatty acids composition  in oil and the position of fatty acids (sn-1,2,3) in the triacylglycerol (TAG) molecule. The purpose of this study was to measure the nutritional value based on the fatty acids composition of  virgin coconut oil (VCO) and palm kernel oil (PKO), and the position of lauric acid in sn-2. The VCO used was VCO obtained from one of the Pharmacies store in Medan, and PKO from the Oil Processing Plant. The total fatty acid composition was measured by Gas Chromatography. The nutritional value of fat was evaluated by the percentage deviation from 33.33% (ratio: 1: 1: 1) of each group of fatty acid (saturated fatty acids; SFA: monounsaturated fatty acids; MUFA:polyunsaturated fatty acid (PUFA). The distribution of lauric acid in TAG was conducted through hydrolysis by using specific lipase enzymes active at sn-1,3 positions, so that free fatty acids and 2-monoacylglycerol were produced from one TAG molecule. Then free fatty acids were determined by Gas Chromatography. The distribution of lauric acid at sn-2 position was the difference between total lauric acid on TAG before hydrolysis and free lauric acid from sn-1.3 position after hydrolysis. The results showed that PKO nutritional value was better because of the smaller deviation (95.29%) compared with nutritional value of VCO with a greater deviation (118.55%). Lauric acid in sn-2 from VCO and PKO showed that the distribution of lauric acid in sn-2 position was not different,48.33and 48.59%. Keywords: virgin coconut oil, palm kernel oil, composition of fatty acids, sn-2 position, lauric acids


2021 ◽  
Author(s):  
Asmaa H. M. Moneeb ◽  
Ahmed R. A. Hammam ◽  
Abdelfatah K. A. Ahmed ◽  
Mahmoud E. Ahmed ◽  
Khalid A. Alsaleem

Author(s):  
Cristian Tudor MATEA ◽  
Adrian MAZAREL ◽  
Maria MORAR ◽  
Constantin BELE ◽  
Andreea BUNEA

Intake of dietary lipid is relevant to human health and should be subject of an extended research regarding quantitative and qualitative aspects. Catering food products investigated in the current study have been chosen from two food groups: fish based food products and meat based food products. Fatty acids were analyzed by gas chromatography (GC) with flame ionization detection (FID), a Shimadzu GC-17A series gas-chromatograph, equipped with a 30m polyethylene glycol coated column (Alltech AT-WAX, 0.25mm I.D., 0.25µm film thickness). Helium was used as the carrier gas at a pressure of 147 kPa. The injector and detector temperatures were set at 260ºC. For the oven temperature the following programe was used: 70ºC for 2 min. then raised to 150ºC at 10ºC/ min. rate and held at 150ºC for 3min., then further raised up to 235ºC at a 4ºC/min. A number of ten food samples were investigated. It was found that in the case of products from both food groups analyzed the predominant fatty acid is the oleic acid (18:1) and significant values for palmitic (16:0), linoleic (18:2) and stearic acid (18:0). The ratio between PUFA/SFA is 0.4 for the fish based products and 0.6 for the meat based products, lower than the threshold of 1.5 which is considered not to raise negative health effects.


LWT ◽  
2019 ◽  
Vol 108 ◽  
pp. 437-445 ◽  
Author(s):  
Changrui Xing ◽  
Xiangyu Yuan ◽  
Xueyou Wu ◽  
Xiaolong Shao ◽  
Jian Yuan ◽  
...  

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