Flow Effects on the Transient Behavior of Vapor Film and Bubbles During Forced-Convective Quenching Experiments

Author(s):  
R. Cruces-Reséndez ◽  
B. Hernández-Morales ◽  
J.E.V. Guzmán

Abstract The transient behavior of boiling phenomena during quenching of an AISI 304 stainless steel, conical-end, cylindrical probe in flowing water at 60 °C was studied. Two free-stream velocities (0.2 and 0.6 m/s) and two initial probe temperatures (850 and 950 °C) were investigated. From high-speed video recordings, undulations of the liquid vapor interface that appear periodically and propagate in the direction of the flow stream were observed during the vapor film stage. After the collapse of the vapor film, a wetting front is formed which consists of many small bubbles that coalesce rapidly in a small area while fewer and larger bubbles nucleate and grow below it. The initial temperature has a marginal effect on the size and half-life of the large bubbles. However, the water flow rate produces larger values of maximum diameter and half-life time for water flowing at 0.2 m/s than their equivalents for 0.6 m/s.

1983 ◽  
Vol 49 (02) ◽  
pp. 109-115 ◽  
Author(s):  
M Hoylaerts ◽  
E Holmer ◽  
M de Mol ◽  
D Collen

SummaryTwo high affinity heparin fragments (A/r 4,300 and M, 3,200) were covalently coupled to antithrombin III (J. Biol. Chem. 1982; 257: 3401-3408) with an apparent 1:1 stoichiometry and a 30-35% yield.The purified covalent complexes inhibited factor Xa with second order rate constants very similar to those obtained for antithrombin III saturated with these heparin fragments and to that obtained for the covalent complex between antithrombin III and native high affinity heparin.The disappearance rates from plasma in rabbits of both low molecular weight heparin fragments and their complexes could adequately be represented by two-compartment mammillary models. The plasma half-life (t'/j) of both low Afr-heparin fragments was approximately 2.4 hr. Covalent coupling of the fragments to antithrombin III increased this half-life about 3.5 fold (t1/2 ≃ 7.7 hr), approaching that of free antithrombin III (t1/2 ≃ 11 ± 0.4 hr) and resulting in a 30fold longer life time of factor Xa inhibitory activity in plasma as compared to that of free intact heparin (t1/2 ≃ 0.25 ± 0.04 hr).


2020 ◽  
Vol 27 ◽  
Author(s):  
Shwethashree Malla ◽  
Sathyanarayana N. Gummadi

Background: Physical parameters like pH and temperature play a major role in the design of an industrial enzymatic process. Enzyme stability and activity are greatly influenced by these parameters; hence optimization and control of these parameters becomes a key point in determining the economic feasibility of the process. Objective: This study was taken up with the objective to optimize physical parameters for maximum stability and activity of xylose reductase from D. nepalensis NCYC 3413 through separate and simultaneous optimization studies and comparison thereof. Method: Effects of pH and temperature on the activity and stability of xylose reductase from Debaryomyces nepalensis NCYC 3413 were investigated by enzyme assays and independent variables were optimised using surface response methodology. Enzyme activity and stability were optimised separately and concurrently to decipher the appropriate conditions. Results: Optimized conditions of pH and temperature for xylose reductase activity were determined to be 7.1 and 27 ℃ respectively, with predicted responses of specific activity (72.3 U/mg) and half-life time (566 min). The experimental values (specific activity 50.2 U/mg, half-life time 818 min) were on par with predicted values indicating the significance of the model. Conclusion: Simultaneous optimization of xylose reductase activity and stability using statistical methods is effective as compared to optimisation of the parameters separately.


1997 ◽  
Vol 62 (6) ◽  
pp. 855-865 ◽  
Author(s):  
Katarína Erentová ◽  
Vladimír Adamčík ◽  
Andrej Staško ◽  
Oskar Nuyken ◽  
Arming Lang ◽  
...  

The cathodically and photochemically induced decomposition of thioazo compounds XC6H4-N2-S-C6H4CH3 and their polymers with X = NO2, COOH, and SO3H were investigated. The formation of carbon-centered XC6H4. and sulfur-centered .S-C6H4Y radicals was confirmed using spin-trap technique. These reactive radicals either abstract hydrogen from CH3CN solvent molecule forming .CH2CN radical or they recombine to cage products XC6H4-S-C6H4CH3 eliminating N2. The decomposition rate of the investigated thioazo compounds is characterized by a formal half-life time of 5 to 10 s.


2021 ◽  
Vol 13 (5) ◽  
pp. 168781402110208
Author(s):  
Yuan Zhang ◽  
Lifeng Wang ◽  
Yaodong Zhang ◽  
Yongde Zhang

The thermal deformation of high-speed motorized spindle will affect its reliability, so fully considering its thermal characteristics is the premise of optimal design. In order to study the thermal characteristics of high-speed motorized spindles, a coupled model of thermal-flow-structure was established. Through experiment and simulation, the thermal characteristics of spiral cooling motorized spindle are studied, and the U-shaped cooled motorized spindle is designed and optimized. The simulation results show that when the diameter of the cooling channel is 7 mm, the temperature of the spiral cooling system is lower than that of the U-shaped cooling system, but the radial thermal deformation is greater than that of the U-shaped cooling system. As the increase of the channel diameter of U-shaped cooling system, the temperature and radial thermal deformation decrease. When the diameter is 10 mm, the temperature and radial thermal deformation are lower than the spiral cooling system. And as the flow rate increases, the temperature and radial thermal deformation gradually decrease, which provides a basis for a reasonable choice of water flow rate. The maximum error between experiment and simulation is 2°C, and the error is small, which verifies the accuracy and lays the foundation for future research.


1997 ◽  
Vol 119 (2) ◽  
pp. 161-170 ◽  
Author(s):  
Yanyao Jiang ◽  
Peter Kurath

Current research focuses on proportional cyclic hardening and non-Massing behaviors. The interaction of these two hardenings can result in the traditionally observed overall softening, hardening or mixed behavior exhibited for fully reversed strain controlled fatigue tests. Proportional experiments were conducted with five materials, 304 stainless steel, normalized 1070 and 1045 steels, and 7075-T6 and 6061-T6 aluminum alloys. All the materials display similar trends, but the 304 stainless steel shows the most pronounced transient behavior and will be discussed in detail. Existing algorithms for this behavior are evaluated in light of the recent experiments, and refinements to the Armstrong-Frederick class of incremental plasticity models are proposed. Modifications implemented are more extensive than the traditional variation of yield stress, and a traditional strain based memory surface is utilized to track deformation history. Implications of the deformation characteristics with regard to fatigue life estimation, especially variable amplitude loading, will be examined. The high-low step loading is utilized to illustrate the effect of transient deformation on fatigue life estimation procedures, and their relationship to the observed and modeled deformation.


Author(s):  
Afshin Goharzadeh ◽  
Keegan Fernandes

This paper presents an experimental investigation on a modified airlift pump. Experiments were undertaken as a function of air-water flow rate for two submergence ratios (ε=0.58 and 0.74), and two different riser geometries (i) straight pipe with a constant inner diameter of 19 mm and (ii) enlarged pipe with a sudden expanded diameter of 19 to 32 mm. These transparent vertical pipes, of 1 m length, were submerged in a transparent rectangular tank (0.45×0.45×1.1 m3). The compressed air was injected into the vertical pipe to lift the water from the reservoir. The flow map regime is established for both configurations and compared with previous studies. The two phase air-water flow structure at the expansion region is experimentally characterized. Pipeline geometry is found to have a significant influence on the output water flow rate. Using high speed photography and electrical conductivity probes, new flow regimes, such as “slug to churn” and “annular to churn” flow, are observed and their influence on the output water flow rate and efficiency are discussed. These experimental results provide fundamental insights into the physics of modified airlift pump.


2010 ◽  
Vol 638-642 ◽  
pp. 1035-1040 ◽  
Author(s):  
Tetsuyuki Hiroe ◽  
Kazuhito Fujiwara ◽  
Hidehiro Hata ◽  
Mitsuru Yamauchi ◽  
Kiyotaka Tsutsumi ◽  
...  

Explosive loading techniques are applied to expand tubular cylinders, spherical shells and rings of 304 stainless steel to fragmentation, and the effects of wall thicknesses, explosive driver diameters and the constant proportionality of the in-plane biaxial stretching rates are investigated on the deformation and fracture behavior of three basic structures experimentally and numerically. In the cylinder tests, the driver is a column of high explosive PETN, inserted coaxially into the bore of a cylinder and initiated by exploding a fine wire bundle at the column axis using a discharge current from a high-voltage capacitor bank. In case of the ring tests, ring specimens are placed onto a single cylinder filled with the PETN as a expansion driver, and for sphere tests, specimens filled with the PETN are also initiated by exploding a fine copper wire line with small length located at the central point. Two types of experiments are conducted for every specimen and test condition. The first type uses high speed cameras to observe the deformation and crack generation of expanding specimens showing the final maximum in-plane stretching rate of above , and the second uses soft capturing system recovering typically most fragments successfully. The fragments are measured and investigated using a fragmentation model. The effects of test parameters on the deformation and fracture behavior for three types of structures are discussed in need of modified fragmentation model for shell structural elements.


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