scholarly journals Effect of a Combination of Moderate-Temperature Heat Treatment and Subsequent Wax Impregnation on Wood Hygroscopicity, Dimensional Stability, and Mechanical Properties

Forests ◽  
2020 ◽  
Vol 11 (9) ◽  
pp. 920 ◽  
Author(s):  
Lin Yang ◽  
Hong-Hai Liu

Wood is an environmentally friendly material, but some natural properties limit its wide application. To study the effect of a combination of heat treatment (HT) and wax impregnation (WI) on wood hygroscopicity, dimensional stability, and mechanical properties, samples of Pterocarpus macrocarpus Kurz wood were subjected to HT at a moderate temperature of 120 °C and a high temperature of 180 °C, for a 4 h duration. Subsequently, half of the 120 °C HT samples were treated with WI at 90 °C. The results showed that 180 °C HT and WI decreased the capacity of adsorption and liquid water uptake and swelled the wood significantly, while WI had the biggest reduction. The effect of 120 °C HT was significant only on decreasing the capacity of adsorption and the swelling of liquid water uptake. The bending strength (MOR) of wood decreased only after 180 °C HT, and 120 °C/4h HT and WI had no significant influence on MOR. The bending stiffness (MOE) increased significantly after 180 °C HT and WI, while 120 °C/4h HT had no significant influence on MOE. Therefore, the combination of moderate-temperature HT can act synergistically in the improvement of certain aspects of wood properties such as capacity of water adsorption and liquid water uptake. WI effectively improved wood hygroscopicity, dimensional stability, and mechanical properties.

Holzforschung ◽  
2003 ◽  
Vol 57 (5) ◽  
pp. 539-546 ◽  
Author(s):  
P. Bekhta ◽  
P. Niemz

Summary In this study the effect of high temperature on mechanical properties, dimensional stability and color of spruce was investigated. Wood specimens conditioned at different relative humidities (50, 65, 80 and 95%) were subjected to heat treatment at 200°C for 2, 4, 8, 10 and 24 h and at 100, 150 and 200°C for 24 h. Color changes were measured in the Minolta Croma-Meter CR-300 color system. Bending strength and modulus of elasticity were determined according to DIN 52186. The results show that heat treatment mainly resulted in a darkening of wood tissues, improvement of the dimensional stability of wood and reduction of its mechanical properties. The darkening accelerated generally when treatment temperature exceeded approximately 200°C. Most of the darkening occurred within the first 4 h of exposure. For the specimens heated to high temperatures, the average decrease in bending strength was about 44–50%, while modulus of elasticity was reduced by only 4–9%. We found that treatment time and temperature were more important than relative humidity regarding the color responses. Strong correlations between total color difference and both modulus of elasticity and bending strength were found. Thus, the color parameters can be estimated quantitatively and used as a prediction of wood strength.


BioResources ◽  
2008 ◽  
Vol 4 (1) ◽  
pp. 370-404
Author(s):  
Bruno M. Esteves ◽  
Helena M. Pereira

Wood heat treatment has increased significantly in the last few years and is still growing as an industrial process to improve some wood properties. The first studies on heat treatment investigated mainly equilibrium moisture, dimensional stability, durability and mechanical properties. Mass loss, wettability, wood color, and chemical transformations have been subsequently extensively studied, while recent works focus on quality control, modeling, and study the reasons for the improvements. This review explains the recent interest on the heat treatment of wood and synthesizes the major publications on this subject on wood properties, chemical changes, wood uses, and quality control.


BioResources ◽  
2008 ◽  
Vol 4 (1) ◽  
pp. 370-404 ◽  
Author(s):  
Bruno M. Esteves ◽  
Helena M. Pereira

Wood heat treatment has increased significantly in the last few years and is still growing as an industrial process to improve some wood properties. The first studies on heat treatment investigated mainly equilibrium moisture, dimensional stability, durability and mechanical properties. Mass loss, wettability, wood color, and chemical transformations have been subsequently extensively studied, while recent works focus on quality control, modeling, and study the reasons for the improvements. This review explains the recent interest on the heat treatment of wood and synthesizes the major publications on this subject on wood properties, chemical changes, wood uses, and quality control.


Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1261
Author(s):  
Catarina S. P. Borges ◽  
Alireza Akhavan-Safar ◽  
Eduardo A. S. Marques ◽  
Ricardo J. C. Carbas ◽  
Christoph Ueffing ◽  
...  

Short fiber reinforced polymers are widely used in the construction of electronic housings, where they are often exposed to harsh environmental conditions. The main purpose of this work is the in-depth study and characterization of the water uptake behavior of PBT-GF30 (polybutylene terephthalate with 30% of short glass fiber)as well as its consequent effect on the mechanical properties of the material. Further analysis was conducted to determine at which temperature range PBT-GF30 starts experiencing chemical changes. The influence of testing procedures and conditions on the evaluation of these effects was analyzed, also drawing comparisons with previous studies. The water absorption behavior was studied through gravimetric tests at 35, 70, and 130 °C. Fiber-free PBT was also studied at 35 °C for comparison purposes. The effect of water and temperature on the mechanical properties was analyzed through bulk tensile tests. The material was tested for the three temperatures in the as-supplied state (without drying or aging). Afterwards, PBT-GF30 was tested at room temperature following water immersion at the three temperatures. Chemical changes in the material were also analyzed through Fourier-transform infrared spectroscopy (FTIR). It was concluded that the water diffusion behavior is Fickian and that PBT absorbs more water than PBT-GF30 but at a slightly higher rate. However, temperature was found to have a more significant influence on the rate of water diffusion of PBT-GF30 than fiber content did. Temperature has a significant influence on the mechanical properties of the material. Humidity contributes to a slight drop in stiffness and strength, not showing a clear dependence on water uptake. This decrease in mechanical properties occurs due to the relaxation of the polymeric chain promoted by water ingress. Between 80 and 85 °C, after water immersion, the FTIR profile of the material changes, which suggests chemical changes in the PBT. The water absorption was simulated through heat transfer analogy with good results. From the developed numerical simulation, the minimum plate size to maintain the water ingress unidirectional was 30 mm, which was validated experimentally.


Author(s):  
Wellington da Silva Mattos ◽  
George Edward Totten ◽  
Lauralice de Campos Franceschini Canale

This article describes the concept of uphill quenching process applied in the heat treatment of aluminum alloys. Uphill quenching is interesting since residual stress reductions of up to 80% has been reported. In addition, substantial improvements in dimensional stability have been achieved for several types of aluminum parts. Often, uphill quenching is applied after quenching and before aging during the heat treatment of aluminum alloys. The uphill quenching process consists of the immersion of the part in a cryogenic environment, and after homogenization of the temperature, the part is transferred to the hot steam chamber to obtain a temperature gradient that will maintain the mechanical properties gained with this process. The results obtained are lower residual stress and better dimensional stability. The aim of this article is to provide a review of this process and to compare it with conventional heat treatment.


2020 ◽  
Vol 10 (22) ◽  
pp. 8231
Author(s):  
Jing-Wen Zhang ◽  
Hong-Hai Liu ◽  
Lin Yang ◽  
Tian-Qi Han ◽  
Qin Yin

Thermal modification (TM) improves the hydrophobicity, dimensional stability, and durability of wood, but TM commonly results in severe color change and mechanical strength loss as wood is treated at higher temperature. In this study, Pterocarpus macrocarpus Kurz wood was thermally modified at moderate temperature (150 °C) and higher temperature (200 °C), and subsequently TM wood at 150 °C was subjected to wax impregnation (WI), the effect of a combination of TM and WI on the hygroscopicity, dimensional stability, and mechanical properties, as well as the micro-structure of wood, were investigated and compared. The results showed that the mass loss of wood was slight at 150 °C TM, while it became severe at 200 °C TM conditions. TM conditions affected the amount of the subsequent wax impregnation; the equilibrium moisture content (EMC), water absorption ratio, and adsorption and absorption swelling of the 150 °C TM + WI group were lower than that of 200 °C TM, and presented the lowest value. Moderate temperature TM could improve the hydrophobicity and dimensional stability of wood, but WI played a key role in the improvement. TM decreased the modulus of rupture (MOR) of wood, while WI improved the MOR. TM increased the modulus of elasticity (MOE) of wood, but WI had little effect on MOE; Scanning electron microscope (SEM) observation showed that the wax was successfully impregnated into the wood interior, and presented an even distribution on the internal surfaces of wood cells; Fourier-transform infrared spectroscopy (FTIR) spectra verified the changes of –OH and C=O after TM and TM + WI, which contributed to decreasing hygroscopicity and improving the dimensional stability of the wood. Impregnated wax improved wood mechanical strength, but decreased the lightness, and deepened the color of wood. The combination of thermal modification at moderate temperature with subsequent wax impregnation is a practical approach for improving wood properties.


Forests ◽  
2019 ◽  
Vol 10 (2) ◽  
pp. 189 ◽  
Author(s):  
Vlastimil Borůvka ◽  
Roman Dudík ◽  
Aleš Zeidler ◽  
Tomáš Holeček

This work deals with the quality of birch (Betula pendula) wood from different sites and the impact of heat treatment on it. Two degrees of heat treatment were used, 170 °C and 190 °C. The resulting property values were compared with reference to untreated wood samples. These values were wood density, compressive strength, modulus of elasticity (MOE), bending strength (MOR), impact bending strength (toughness), hardness, swelling, limit of hygroscopicity, moisture content and color change. It was supposed that an increase in heat-treatment temperature could reduce strength properties and, adversely, lead to better shape and dimensional stability, which was confirmed by experiments. It was also shown that the properties of the wood before treatment affected their condition after heat treatment, and that the characteristic values and variability of birch properties from 4 sites, 8 stems totally, were reflected in the properties of the heat-treated wood. Values of static MOR were the exception, where the quality of the input wood was less significant at a higher temperature, and this was even more significant in impact bending strength, where it manifested at a lower temperature degree. Impact bending strength also proved to be significantly negatively affected by heat treatment, about 48% at 170 °C, and up to 67% at 190 °C. On the contrary, the most positive results were the MOE and hardness increases at 170 °C by about 30% and about 21%, respectively, with a decrease in swelling at 190 °C by about 31%. On the basis of color change and other ascertained properties, there is a possibility that, after suitable heat treatment, birch could replace other woods (e.g., beech) for certain specific purposes, particularly in the furniture industry.


2011 ◽  
Vol 306-307 ◽  
pp. 823-826
Author(s):  
Ming Wen ◽  
Yun Long Yue ◽  
Hai Tao Zhang ◽  
Yang Li

Parameters of processing (heat treatment temperature, holding time) and properties (Bending strength and Microhardness) of Ti2AlC/TiAl compound materials were obtained through mechanical properties examination, the network model was built by BP artificial neural network. The results show that the built model can reflect the relationships between processing and properties very well and has certain accuracy. It can be used for the prediction of the properties of Ti2AlC/TiAl compound materials after heating processing under different experiment conditions. Meanwhile, the model can also serve as a guide for the preparation technology of Ti2AlC/TiAl compound materials.


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