scholarly journals Multiscale Characterization of E-Glass/Epoxy Composite Exposed to Extreme Environmental Conditions

2021 ◽  
Vol 5 (3) ◽  
pp. 80
Author(s):  
George Youssef ◽  
Scott Newacheck ◽  
Nha Uyen Huynh ◽  
Carlos Gamez

Fiber-reinforced polymer matrix composites continue to attract scientific and industrial interest since they offer superior strength-, stiffness-, and toughness-to-weight ratios. The research herein characterizes two sets of E-Glass/Epoxy composite skins: stressed and unstressed. The stressed samples were previously installed in an underground power distribution vault and were exposed to fire while the unstressed composite skins were newly fabricated and never-deployed samples. The mechanical, morphological, and elemental composition of the samples were methodically studied using a dynamic mechanical analyzer, a scanning electron microscope (SEM), and an x-ray diffractometer, respectively. Sandwich composite panels consisting of E-glass/Epoxy skin and balsa wood core were originally received, and the balsa wood was removed before any further investigations. Skin-only specimens with dimensions of ~12.5 mm wide, ~70 mm long, and ~6 mm thick were tested in a Dynamic Mechanical Analyzer in a dual-cantilever beam configuration at 5 Hz and 10 Hz from room temperature to 210 °C. Micrographic analysis using the SEM indicated a slight change in morphology due to the fire event but confirmed the effectiveness of the fire-retardant agents in quickly suppressing the fire. Accompanying Fourier transform infrared and energy dispersive X-ray spectroscopy studies corroborated the mechanical and morphological results. Finally, X-ray diffraction showed that the fire event consumed the surface level fire-retardant and the structural attributes of the E-Glass/Epoxy remained mainly intact. The results suggest the panels can continue field deployment, even after short fire incident.

Processes ◽  
2020 ◽  
Vol 8 (1) ◽  
pp. 103 ◽  
Author(s):  
Luan TranVan ◽  
Vincent Legrand ◽  
Pascal Casari ◽  
Revathy Sankaran ◽  
Pau Loke Show ◽  
...  

In this study, the hygro–thermo–mechanical responses of balsa core sandwich structured composite was investigated by using experimental, analytical and numerical results. These investigations were performed on two types of specimen conditions: dry and moisture saturation sandwich composite specimens that are composed of E-glass/polyester skins bonded to a balsa core. The wet specimens were immersed in distilled water at 40 °C until saturated with water. The both dry and wet sandwich composite specimens were heated by fire. The mass loss kinetic and the mechanical properties were investigated by using a cone calorimeter following the ISO 5660 standard and three-point bending mechanical test device. Experimental data show that the permeability and fire resistance of the sandwich structure are controlled by two composite skins. Obtained results allow us to understand the Hygro–Thermo–Mechanical Responses of the sandwich structured composite under application conditions.


Materials ◽  
2020 ◽  
Vol 13 (15) ◽  
pp. 3345
Author(s):  
Janusz Zmywaczyk ◽  
Judyta Sienkiewicz ◽  
Piotr Koniorczyk ◽  
Jan Godzimirski ◽  
Mateusz Zieliński

In this paper, thermophysical and viscoelastic dynamic mechanical measurements (DMA) were performed for bare and clad aluminum AW-2024-T3 alloys. Specific heat, thermal diffusivity, and dynamic module (storage and loss) tests were performed in the range of 50 to 500 °C, except for DMA ones (RT–400 °C). All tests were carried out using the following specialized measuring stands: a light flash apparatus (LFA), differential scanning calorimeter (DSC), and a dynamic mechanical analyzer (DMA). The microstructures and compositions of alloys were investigated by light microscope (LM), scanning electron microscope (SEM), and energy-dispersive X-ray spectroscopy (EDS). Furthermore, Vickers micro-hardness measurements were conducted prior to and after DSC studies. Different precipitation kinetics of the θ′ and S′ metastable phases in the bare 2024-T3 compared to the clad alloy were observed by DSC. Additionally, the DSC results for a few selected scan rates were analyzed by the Kissinger method to give activation energies for the precipitation of θ′ and S′ metastable phases in the alloys. The apparent activation energy of the θ′ and S′ phases corresponds to 137.1 ± 4.4 kJ· mol−1 for the bare alloy and 131.0 ± 6.0 (exo) and 104.1 ± 2.1 (exo) (two peaks) for the clad alloy.


2018 ◽  
Vol 5 (11) ◽  
pp. 25486-25493 ◽  
Author(s):  
Anant Joshi ◽  
Santosh Savnur ◽  
Vinayak S Uppin ◽  
P.S. Shivakumar Gouda ◽  
I. Sridhar ◽  
...  

2003 ◽  
Vol 11 (2) ◽  
pp. 115-122
Author(s):  
Kálmán Marossy ◽  
Pál Bárczy

Blends of high density polyethylene (HDPE) and chlorinated polyethylene (CPE) have been tested across the whole concentration range. Polyethylene is used to modify the properties of CPE in the elastomer industry, but modification of the properties of polyethylene with CPE is still not usual. Conventional mechanical tests and dynamic mechanical tests were carried out. The blends were found to be multiphase systems of excellent technological compatibility. Between 10 and 15% by weight CPE increased the modulus of polyethylene. X-ray scattering studies showed that the blends contained structural units not present either in the polyethylene or in the CPE. The blends were melt processable and may have industrial applications, too.


1975 ◽  
Vol 15 (10) ◽  
pp. 697-702 ◽  
Author(s):  
Eng Pi Chang ◽  
Rudy Kirsten ◽  
Ronald Salovey

2006 ◽  
Vol 20 (25n27) ◽  
pp. 4577-4582
Author(s):  
SUNG SOO HAN ◽  
YANG-WHAN CHO ◽  
SOO-YOUNG PARK

The structural development of nylon6/layered silicate nanocomposite during zone-drawing was studied using X-ray scattering and dynamic mechanical thermal analysis. The γ form, which was favored in the pressed film, was converted into the α form during zone-drawing. The newly developed α form, during zone-drawing, has a better orientation than the existing γ form, thus supporting the claim that the α form crystallizes away from the polymer-silicate inter-phase region during drawing. The degree of orientation of the layered silicate, projected along the TD direction, increases with the increase of the draw ratio, suggesting that the layered silicate has become straighter during zone-drawing, although the layered silicate within the zone-drawn film buckled perpendicular to the draw direction. The β transition of the dynamic mechanical thermal analysis is independent of the crystalline phase, although the α transition is strongly dependent upon the crystalline phase. This can be explained by the free volume that exists in the inter-phase between the γ lamellar and the layered silicate.


2018 ◽  
Vol 25 (5) ◽  
pp. 2020-2028 ◽  
Author(s):  
Subhash Nimanpure ◽  
S. A. R. Hashmi ◽  
Rajnish Kumar ◽  
Archana Nigrawal ◽  
Ajay Naik

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