scholarly journals Bioactive Tetracalcium Phosphate Scaffolds Fabricated by Selective Laser Sintering for Bone Regeneration Applications

Materials ◽  
2020 ◽  
Vol 13 (10) ◽  
pp. 2268 ◽  
Author(s):  
Tian Qin ◽  
Xiaoqian Li ◽  
Hui Long ◽  
Shizhen Bin ◽  
Yong Xu
Keyword(s):  
Mechanical Properties ◽  
Bone Regeneration ◽  
Laser Power ◽  
Selective Laser Sintering ◽  
Three Dimensional ◽  
Laser Sintering ◽  
Scaffold Material ◽  
Promising Candidate ◽  
Tetracalcium Phosphate ◽  
Good Biocompatibility

Tetracalcium phosphate (TTCP), a potential biological scaffold material, has attracted increasing interest for bone regeneration applications due to its good biodegradability and biocompatibility. In this research, three-dimensional porous TTCP scaffolds were manufactured via selective laser sintering (SLS), and an in-depth and meticulous study on the influence of laser power on the microstructure and mechanical properties of TTCP scaffolds was performed. The results showed that the TTCP particles fused together and formed a solid object due to the decrease in the number of micro-pores in the scaffold as the laser power increased from 6 W to 9 W. The maximum compressive strength that the scaffold could withstand and the strength of the fracture toughness were 11.87 ± 0.64 MPa and 1.12 ± 0.1 MPa·m1/2, respectively. When the laser power increased from 9 W to 10 W, the TTCP grains grew abnormally, resulting in diminished mechanical properties. The bioactivity tests showed that the surfaces of the scaffolds were entirely covered by bone-like apatite layers after soaking in simulated body fluid (SBF) for three days, indicating that the scaffolds exhibit excellent bioactivity. Moreover, cell experiments showed that the TTCP scaffolds had good biocompatibility. This study indicated that SLS-fabricated TTCP scaffolds may be a promising candidate for bone regeneration applications.

scholarly journals Selective Laser Sintering of PA6: Effect of Powder Recoating on Fibre Orientation

2020 ◽  
Vol 4 (3) ◽  
pp. 108
Author(s):  
Tobias Heckner ◽  
Michael Seitz ◽  
Sven Robert Raisch ◽  
Gerrit Huelder ◽  
Peter Middendorf
Keyword(s):  
Computed Tomography ◽  
Mechanical Properties ◽  
Layer Thickness ◽  
Laser Power ◽  
Laser Energy ◽  
Fibre Orientation ◽  
Selective Laser Sintering ◽  
Laser Sintering ◽  
Shear Stresses ◽  
Imaging Results

In Selective Laser Sintering, fibres are strongly orientated during the powder recoating process. This effect leads to an additional increase of anisotropy in the final printed parts. This study investigates the influence of process parameter variation on the mechanical properties and the fibre orientation. A full factorial design of experiment was created to evaluate the processing parameters of recoating speed, layer thickness and laser power on the part’s modulus of elasticity. Based on the mechanical testing, computed tomography was applied to selected samples to investigate the process-induced fibre microstructure, and calculate the fibre orientation tensors. The results show increasing part stiffness in the deposition direction, with decreasing layer thickness and increasing laser power, while the recoating speed only shows little effect on the mechanical performance. This complies with computed tomography imaging results, which show an increase in fibre orientation with smaller layer thickness. With thinner layers, and hence smaller shear gaps, shear stresses induced by the roller during recoating increase significantly, leading to excessive fibre reorientation and alignment. The high level of fibre alignment implies an increase of strength and stiffness in the recoating direction. In addition, thinner layer thickness under constant laser energy density results in improved melting behaviour, and thus improved fibre consolidation, consequently further increasing the mechanical properties. Meanwhile, the parameters of recoating speed and laser power do not have a significant impact on fibre orientation within their applicable process windows.

Effects of the Processing Parameters on Porosity of Selective Laser Sintered Aliphatic Polycarbonate

2014 ◽  
Vol 915-916 ◽  
pp. 1000-1004 ◽  
Author(s):  
Xiao Hui Song ◽  
Yu Sheng Shi ◽  
Ping Hui Song ◽  
Qing Song Wei ◽  
Wei Li
Keyword(s):  
Mechanical Properties ◽  
Biomedical Engineering ◽  
Laser Power ◽  
Orthogonal Experiment ◽  
Selective Laser Sintering ◽  
Processing Parameters ◽  
Laser Sintering ◽  
Optimal Parameters ◽  
Micro Structure ◽  
Aliphatic Polycarbonate

Selective Laser Sintering (SLS) has been successfully and broadly applied in biomedical engineering to fabricated biomedical part. And the porosity and microstructure of part can be controlled by main sintered parameters. This research focused aliphatic Polycarbonate (PC) sintered with SLS. According to the orthogonal experiment, the effect of laser power energy and interaction between main sintered parameters on porosity has been studied. Then the micro structure and mechanical properties of specimens sintered with the best optimal parameters have been analyzed.

scholarly journals Emerging trend in manufacturing of 3D biomedical components using selective laser sintering: A review

2020 ◽  
Vol 184 ◽  
pp. 01047 ◽  
Author(s):  
Pankaj Kumar ◽  
Gazanfar Mustafa Ali syed
Keyword(s):  
Mechanical Properties ◽  
Laser Processing ◽  
Laser Power ◽  
Review Paper ◽  
Selective Laser Sintering ◽  
Scanning Speed ◽  
Laser Sintering ◽  
Sintering Process ◽  
Research Papers ◽  
Published Research

Additive manufacturing (also known as 3D printing) process is an emerging technique for the fabrication of biomedical components. Selective laser sintering or melting is one of the widely used additive printing technology for manufacturing of metallic and non-metallic components used in the industry. This review paper presents, a summary of the published research papers on the fabrication of biomedical components using selective laser sintering technique. Therefore, author meticulously attempted to investigate individual biocompatible material-wise review which includes Ti6Al4V, Ti-7.5 Mo alloy, β-Ti35Zr28Nb, PEEK, PA2200, and Polyamide/Hydroxyapatite. In addition, this article also explores the effects of the various laser sintering process parameters such as laser power, scanning speed, density of the material on the mechanical properties, tribological properties, porosity and surface roughness of the fabricated alloy. Moreover, the author also investigated challenges and future prospective of the laser processing of biomedical implants.

Sintering quality and parameters optimization of sisal fiber/PES composite fabricated by selective laser sintering (SLS)

2020 ◽  
pp. 089270572093917
Author(s):  
Aboubaker IB Idriss ◽  
Jian Li ◽  
Yanling Guo ◽  
Yangwei Wang ◽  
Xingdong Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Process Parameters ◽  
Laser Power ◽  
Selective Laser Sintering ◽  
Scanning Speed ◽  
Laser Sintering ◽  
Sisal Fiber ◽  
Optimum Parameters ◽  
Preheating Temperature

This article aims to improve the sintering quality of the sisal fiber/poly-(ether sulfone) (PES) composite (SFPC) part fabricated via selective laser sintering (SLS). The sisal fiber and PES powders were proposed as the feedstock of the SFPC powder bed for SLS. An orthogonal experimental methodology with four levels and five factors was applied to optimize the process parameters for the single-layer sintering experiment. The mechanical properties and accurate dimensions of the sintered part were tested using a universal testing machine and Vernier caliper. The preheating temperature, scanning speed, and laser power were selected as influencing factors on the mechanical properties and accuracy dimensions of the SFPC part. Furthermore, the influence factors on the quality of the sintered part were studied and analyzed. Additionally, the synthesis weighted scoring method was used to determine the optimum parameters of the SLS part. The results showed that the optimal parameters (factors) were preheating temperature of 82°C, scanning speed of 2 m s−1, laser power of 14 W, and laser wavelength of 10.6 μm. Thus, the quality of SFPC part was significantly enhanced when the optimum parameters were applied in SLS process. This article provided the main reference value for the choice of the process parameters of the biomass composite.

scholarly journals Optimal design of three-dimensional non-uniform nylon lattice structures for selective laser sintering manufacturing

2018 ◽  
Vol 10 (7) ◽  
pp. 168781401879083 ◽  
Author(s):  
Xin Jin ◽  
Guo Xi Li ◽  
Meng Zhang
Keyword(s):  
Mechanical Properties ◽  
Topology Optimization ◽  
Optimal Design ◽  
Cell Size ◽  
Selective Laser Sintering ◽  
Three Dimensional ◽  
Laser Sintering ◽  
Manufacturing Constraints ◽  
Lattice Structures ◽  
Cell Type

As a kind of novel multifunctional structure with three-dimensional pores characterized by low relative density, lattice structures can attain a lightweight design while maintaining high specific mechanical properties in three-dimensional solid structures. Focusing on the challenge of finding the optimal design of lattice structures in the design object, a design and modeling method of non-uniform three-dimensional lattice structures is proposed while ensuring the selective laser sintering manufacturability. Optimization for cell type, cell size, and strut size distribution of lattices is specified with the mechanical properties analyzed and the material model calculated beforehand. The manufacturing constraints are analyzed and expressed in topology optimization and the optimal distribution of topology optimization results is mapped to the strut size distribution of lattice cells. The rapid and automatic computer-aided design modeling of optimized structures is realized by the parametric definition and assembling of lattice components. Finally, the non-uniform structures are successfully manufactured by selective laser sintering and it is shown by means of finite element analysis and experiments that the proposed design approach can improve the mechanical performance compared to the uniform lattice structure under the same weight reduction. And for the design object in this study, body-centered structure with cell size [Formula: see text]mm is chosen as the optimal cell type and cell size under the given selective laser sintering manufacturing constraints.

On Mechanical Properties of Cellular Steel Solids With Shell-Like Periodic Architectures Fabricated by Selective Laser Sintering

2019 ◽  
Vol 141 (2) ◽  
Author(s):  
Oraib Al-Ketan ◽  
Reza Rowshan ◽  
Anthony N. Palazotto ◽  
Rashid K. Abu Al-Rub
Keyword(s):  
Mechanical Properties ◽  
Material Selection ◽  
Selective Laser Sintering ◽  
Three Dimensional ◽  
Laser Sintering ◽  
Cellular Materials ◽  
Structure Property ◽  
Printing Quality ◽  
High Control ◽  
Proper Material

Historically, the approach in material selection was to find the proper material that serves a specific application. Recently, a new approach is implemented such that materials are being architected and topologically tailored to deliver a specific functionality. Periodic cellular materials are increasingly gaining interest due to their tunable structure-related properties. However, the concept of structure–property relationship is not fully employed due to limitations in manufacturing capabilities. Nowadays, additive manufacturing (AM) techniques are facilitating the fabrication of complex structures with high control over the topology. In this work, the mechanical properties of additively manufactured periodic metallic cellular materials are investigated. The presented cellular materials comprise a shell-like topology based on the mathematically known triply periodic minimal surfaces (TPMS). Maraging steel samples with different topologies and relative densities have been fabricated using the powder bed fusion selective laser sintering (SLS) technique, and three-dimensional printing quality was assessed by means of electron microscopy. Samples were tested in compression and the compressive mechanical properties have been deduced. Effects of changing layer thickness and postprocessing such as heat treatment are discussed. Results showed that the diamond TPMS lattice has shown superior mechanical properties among the examined topologies.

scholarly journals Production and Processing of a Spherical Polybutylene Terephthalate Powder for Laser Sintering

2019 ◽  
Vol 9 (7) ◽  
pp. 1308 ◽  
Author(s):  
Rob Kleijnen ◽  
Manfred Schmid ◽  
Konrad Wegener
Keyword(s):  
Mechanical Properties ◽  
Thermal Processing ◽  
Selective Laser Sintering ◽  
Spherical Shape ◽  
Laser Sintering ◽  
Polybutylene Terephthalate ◽  
Powder Production ◽  
Injection Molded ◽  
Continuous Extrusion ◽  
Matrix Powder

This work describes the production of a spherical polybutylene terephthalate (PBT) powder and its processing with selective laser sintering (SLS). The powder was produced via melt emulsification, a continuous extrusion-based process. PBT was melt blended with polyethylene glycol (PEG), creating an emulsion of spherical PBT droplets in a PEG matrix. Powder could be extracted after dissolving the PEG matrix phase in water. The extrusion settings were adjusted to optimize the size and yield of PBT particles. After classification, 79 vol. % of particles fell within a range of 10–100 µm. Owing to its spherical shape, the powder exhibited excellent flowability and packing properties. After powder production, the width of the thermal processing (sintering) window was reduced by 7.6 °C. Processing of the powder on a laser sintering machine was only possible with difficulties. The parts exhibited mechanical properties inferior to injection-molded specimens. The main reason lied in the PBT being prone to thermal degradation and hydrolysis during the powder production process. Melt emulsification in general is a process well suited to produce a large variety of SLS powders with exceptional flowability.

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