scholarly journals Effects of Fatigue Damage on the Microscopic Modulus of Cortical Bone Using Nanoindentation

Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3252
Author(s):  
Xianjia Meng ◽  
Chuanyong Qu ◽  
Donghui Fu ◽  
Chuan Qu

Alterations to the bone structure from cycle loadings can undermine its damage resistance at multiple scales. The accumulation of fatigue damage in a bone is commonly characterized by the reduction in the elastic modulus. In this study, nano-indentation was used for investigating microscopic damage evolution of bovine tibia samples subjected to fatigue loading. Indentation tests were conducted in the same 60 μm × 120 μm area with different degrees of damage, including fracture, and the evolution of reduced modulus was observed. The results showed that bone’s reduced modulus decreased significantly during the initial 40% of the life fraction, whereas it proceeded slowly during the remaining period. As the size of the residual indentations was about 4 μm in length, the degradation of bone’s reduced modulus reflected the accumulation of fatigue damage at smaller scales.

2021 ◽  
Author(s):  
Xianjia Meng ◽  
Qinghua Qin ◽  
Chuanyong Qu

Abstract Background The role of bone fatigue damage at the nanostructural level, and its effect on fatigue properties is an understudied and important subject. An understanding of the subtler aspects of bone’s properties is crucial to understanding bone fragility caused by aging, disease, and fatigue damage. The primary strength of this study was the demonstration of the degradation of bone’s microscopic mechanical properties by nanoindentation following fatigue loading. Methods Nanoindentation was used to probe the micro-mechanical properties of bovine tibiae subjected to fatigue loading in four-point bending. Indentation tests were conducted in the same 30×120 µm region before fatigue loading and after loading to fracture. We analysed the effects of residual indentations on bone’s fatigue resistance using an optical microscope and scanning electron microscope. The mechanical properties calculated using nanoindentation were reduced modulus and hardness, the time constant based on creep, long-term creep viscosity and the dissipated work. Differences of each parameter before loading and post fracture were examined using paired t-tests. Results The morphology of the initial residual indentation before fatigue loading appeared the same as that after loading to fracture. The results show that the reduced modulus decreased significantly (p = 9.47×10− 3) by 7.62%~15.16% after fracture whereas the time constant of creep increased slightly (p = 0.049) by 2.81%~5.41%. The p-value was significantly lower (p < 0.001) for reduced modulus compared to all other mechanical properties. Conclusion Residual indents different from fatigue damage created no crack initiators that would weaken bone’s resistance to fatigue loading. Fatigue loading has the most heavy effect on bone’s reduced modulus compared to all other microscopic mechanical properties.


2006 ◽  
Vol 514-516 ◽  
pp. 804-809
Author(s):  
S. Gao ◽  
Ewald Werner

The forging die material, a high strength steel designated W513 is considered in this paper. A fatigue damage model, based on thermodynamics and continuum damage mechanics, is constructed in which both the previous damage and the loading sequence are considered. The unknown material parameters in the model are identified from low cycle fatigue tests. Damage evolution under multi-level fatigue loading is investigated. The results show that the fatigue life is closely related to the loading sequence. The fatigue life of the materials with low fatigue loading first followed by high fatigue loading is longer than that for the reversed loading sequence.


Author(s):  
Fei Qin ◽  
Shuai Zhao ◽  
Yanwei Dai ◽  
Lingyun Liu ◽  
Tong An ◽  
...  

Abstract Thermo-mechanical reliability assessment for sintered silver is a crucial issue as sintered silver is a promising candidate of die-attachment materials for power devices. In this paper, the nano-indentation tests are performed for sintered silver in typical die-attach interconnection under different thermal cycles. Based on thermal cycling test, the Young's modulus and hardness of sintered silver layer have been presented. It is found that the Young's modulus and hardness of sintered silver layer changes slightly although the microstructure of sintered silver also presents some variations. The stress and strain curves for different thermal cycling tests for sintered silver based on reverse analysis of nano-indentation are also given. The results show that the elastoplastic constitutive equations change significantly after thermal cycling tests, and the yielding stress decreases remarkably after 70 thermal cycles. The experimental investigation also show that the cracking behaviors of sintered silver depends on its geometry characteristics, which implies that the possible optimization of sintered silver layer could enhance its thermo-mechanical performance.


Author(s):  
Rohit Shankaran ◽  
Alexander Rimmer ◽  
Alan Haig

In recent years due to use of drilling risers with larger and heavier BOP/LMRP stacks, fatigue loading on subsea wellheads has increased, which poses potential restrictions on the duration of drilling operations. In order to track wellhead and conductor fatigue capacity consumption to support safe drilling operations a range of methods have been applied: • Analytical riser model and measured environmental data; • BOP motion measurement and transfer functions; • Strain gauge data. Strain gauge monitoring is considered the most accurate method for measuring fatigue capacity consumption. To compare the three approaches and establish recommendations for an optimal approach and method to establish fatigue accumulation of the wellhead, a monitoring data set is obtained on a well offshore West of Shetland. This paper presents an analysis of measured strain, motions and analytical predictions with the objective of better understanding the accuracy, limitations, or conservatism in each of the three methods defined above. Of the various parameters that affect the accuracy of the fatigue damage estimates, the paper identifies that the selection of analytical conductor-soil model is critical to narrowing the gap between fatigue life predictions from the different approaches. The work presented here presents the influence of alternative approaches to model conductor-soil interaction than the traditionally used API soil model. Overall, the paper presents the monitoring equipment and analytical methodology to advance the accuracy of wellhead fatigue damage measurements.


Author(s):  
J. Kusumoto ◽  
H. Watanabe ◽  
A. Kanaya ◽  
K. Ichikawa ◽  
S. Sakurai

In order to develop the life prediction method under creep-fatigue loading for gas turbine combustion transition piece, creep-fatigue tests were carried out on both as-received and aged Ni-based superalloy Nimonic 263. Crack initiation and propagation behaviors for the smooth specimen were observed. An unique relationship was obtained between life fraction and the maximum surface crack length under triangular wave shape loading tests, except the results for the trapezoidal wave loading tests. The latter results were due to the over estimation of the surface crack length at the crack initiation. These were caused from an oxide film break during straining. In the case of removing the oxide film before the measurement of surface crack, the relationship between life fraction and the maximum surface crack length obtained as unique relationship regardless of triangular and trapezoidal strain wave shapes. Using the life prediction method proposed, which is based on maximum surface crack length, the damage of combustion transition piece materials in service was evaluated.


Author(s):  
Geovana Drumond ◽  
Bianca Pinheiro ◽  
Ilson Pasqualino ◽  
Francine Roudet ◽  
Didier Chicot

The hardness of a material shows its ability to resist to microplastic deformation caused by indentation or penetration and is closely related to the plastic slip capacity of the material. Therefore, it could be significant to study the resistance to microplastic deformations based on microhardness changes on the surface, and the associated accumulation of fatigue damage. The present work is part of a research study being carried out with the aim of proposing a new method based on microstructural changes, represented by a fatigue damage indicator, to predict fatigue life of steel structures submitted to cyclic loads, before macroscopic cracking. Here, Berkovich indentation tests were carried out in the samples previously submitted to high cycle fatigue (HCF) tests. It was observed that the major changes in the microhardness values occurred at the surface of the material below 3 μm of indentation depth, and around 20% of the fatigue life of the material, proving that microcracking is a surface phenomenon. So, the results obtained for the surface of the specimen and at the beginning of the fatigue life of the material will be considered in the proposal of a new method to estimate the fatigue life of metal structures.


2019 ◽  
Author(s):  
Elaine C. Schmidt ◽  
Todd J. Hullfish ◽  
Kathryn M. O’Connor ◽  
Michael W. Hast ◽  
Josh R. Baxter

ABSTRACTAchilles tendon disorders are among the most difficult sports-related injuries to predict with current diagnostic tools. The purpose of this study was to identify a clinically useful marker for early tendon damage. We hypothesized that alterations in mean echogenicity are linked with changes in vitro tendon mechanics. To test our hypothesis, we harvested Achilles tendons from 10 fresh-frozen cadaveric feet and cyclically fatigued them using a universal test frame while we continuously acquired ultrasound images. Throughout this fatigue protocol, we applied 2 stress tests every 500 loading cycles to quantify changes in ultrasound imaging echogenicity. We continued this fatigue protocol until each tendon either failed completely or survived 150,000 cycles. Tendons that failed during the fatigue loading (6/10) underwent greater changes in mean echogenicity compared to tendons that did not fail (P = 0.031). These tendons that failed during fatigue loading demonstrated greater changes in mean echogenicity that surpassed 1.0%; whereas survivor tendons exhibited less than 0.5% changes in mean echogenicity. We found that changes in mean echogenicity measured with ultrasound increased proportionally with increased tendon damage. The magnitude of these changes was relatively small (<1.5% change in mean echogenicity) but may be an effective predictor of tendon failure. Mean echogenicity is a promising marker for quantifying fatigue damage in cadaveric Achilles tendons during a stress test. Although these changes cannot be detected with the naked eye, computer-based predictive models may effectively assess risk of tendon damage in physically active adults.Level of evidenceControlled laboratory experiment


Materials ◽  
2022 ◽  
Vol 15 (1) ◽  
pp. 341
Author(s):  
Marc Thiele ◽  
Stephan Pirskawetz

The fatigue process of concrete under compressive cyclic loading is still not completely explored. The corresponding damage processes within the material structure are especially not entirely investigated. The application of acoustic measurement methods enables a better insight into the processes of the fatigue in concrete. Normal strength concrete was investigated under compressive cyclic loading with regard to the fatigue process by using acoustic methods in combination with other nondestructive measurement methods. Acoustic emission and ultrasonic signal measurements were applied together with measurements of strains, elastic modulus, and static strength. It was possible to determine the anisotropic character of the fatigue damage caused by uniaxial loading based on the ultrasonic measurements. Furthermore, it was observed that the fatigue damage seems to consist not exclusively of load parallel oriented crack structures. Rather, crack structures perpendicular to the load as well as local compacting are likely components of the fatigue damage. Additionally, the ultrasonic velocity appears to be a good indicator for fatigue damage beside the elastic modulus. It can be concluded that acoustic methods allow an observation of the fatigue process in concrete and a better understanding, especially in combination with further measurement methods.


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