scholarly journals Electrophoretically Deposited Chitosan/Eudragit E 100/AgNPs Composite Coatings on Titanium Substrate as a Silver Release System

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4533
Author(s):  
Łukasz Pawłowski ◽  
Michał Bartmański ◽  
Aleksandra Mielewczyk-Gryń ◽  
Bartłomiej Michał Cieślik ◽  
Grzegorz Gajowiec ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Bacterial Infections ◽  
Composite Coatings ◽  
Titanium Substrate ◽  
Deposition Parameters ◽  
Eudragit E ◽  
Scientific Goal ◽  
Titanium Grade ◽  
Silver Release ◽  
Implant Coatings

Due to the possibility of bacterial infections occurring around peri-implant tissues, it is necessary to provide implant coatings that release antibacterial substances. The scientific goal of this paper was to produce by electrophoretic deposition (EPD) a smart, chitosan/Eudragit E 100/silver nanoparticles (chit/EE100/AgNPs) composite coating on the surface of titanium grade 2 using different deposition parameters, such as the content of AgNPs, applied voltage, and time of deposition. The morphology, surface roughness, thickness, chemical and phase composition, wettability, mechanical properties, electrochemical properties, and silver release rate at different pH were investigated. Using lower values of deposition parameters, coatings with more homogeneous morphology were obtained. The prepared coatings were sensitive to the reduced pH environment.

scholarly journals Electrophoretic Deposition and Characterization of Chitosan/Eudragit E 100 Coatings on Titanium Substrate

Coatings ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 607 ◽  
Author(s):  
Łukasz Pawłowski ◽  
Michał Bartmański ◽  
Gabriel Strugała ◽  
Aleksandra Mielewczyk-Gryń ◽  
Magdalena Jażdżewska ◽  
...  
Keyword(s):  
Corrosion Resistance ◽  
Degradation Rate ◽  
Artificial Saliva ◽  
Titanium Substrate ◽  
High Sensitivity ◽  
Titanium Implants ◽  
The Body ◽  
Chitosan Coating ◽  
Eudragit E ◽  
Titanium Grade

Currently, a significant problem is the production of coatings for titanium implants, which will be characterized by mechanical properties comparable to those of a human bone, high corrosion resistance, and low degradation rate in the body fluids. This paper aims to describe the properties of novel chitosan/Eudragit E 100 (chit/EE100) coatings deposited on titanium grade 2 substrate by the electrophoretic technique (EPD). The deposition was carried out for different parameters like the content of EE100, time of deposition, and applied voltage. The microstructure, surface roughness, chemical and phase composition, wettability, mechanical and electrochemical properties, and degradation rate at different pH were examined in comparison to chitosan coating without the addition of Eudragit E 100. The applied deposition parameters significantly influenced the morphology of the coatings. The chit/EE100 coating with the highest homogeneity was obtained for Eudragit content of 0.25 g, at 10 V, and for 1 min. Young’s modulus of this sample (24.77 ± 5.50 GPa) was most comparable to that of human cortical bone. The introduction of Eudragit E 100 into chitosan coatings significantly reduced their degradation rate in artificial saliva at neutral pH while maintaining high sensitivity to pH changes. The chit/EE100 coatings showed a slightly lower corrosion resistance compared to the chitosan coating, however, significantly exceeding the substrate corrosion resistance. All prepared coatings were characterized by hydrophilicity.

scholarly journals Deposition of titanium based coatings by reactive detonation spraying

2018 ◽  
Vol 62 (1) ◽  
pp. 6-13 ◽  
Author(s):  
S. Panin ◽  
I. Vlasov ◽  
D. Dudina ◽  
V. Ulyanitsky ◽  
R. Stankevich ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Composite Coatings ◽  
Detonation Spraying ◽  
Gas Detonation ◽  
Carrier Gas ◽  
Deposition Parameters ◽  
Spraying Parameters ◽  
Wide Range ◽  
The Individual ◽  
Gas Detonation Spraying

Abstract The structure and mechanical properties of the coatings formed by reactive detonation spraying of titanium in a wide range of spraying conditions were studied. The variable deposition parameters were the nature of the carrier gas, the spraying distance, the O2/C2H2 ratio, and the volume of the explosive mixture. The phase composition of the coatings and the influence of the spraying parameters on the mechanical properties of the coatings were investigated. In addition, nanohardness of the individual phases contained the coatings was evaluated. It was found that the composition of the strengthening phases in the coatings depends on the O2/C2H2 ratio and the nature of the carrier gas. Detonation spraying conditions ensuring the formation of composite coatings with a set of improved mechanical properties are discussed.

scholarly journals Improving the microstructure and mechanical properties of laser cladded Ni-based alloy coatings by changing their composition: A review

2020 ◽  
Vol 59 (1) ◽  
pp. 340-351
Author(s):  
Lin Yinghua ◽  
Ping Xuelong ◽  
Kuang Jiacai ◽  
Deng Yingjun
Keyword(s):  
Mechanical Properties ◽  
Wear Resistance ◽  
Corrosion Resistance ◽  
Rare Earth ◽  
Composite Coatings ◽  
Single Element ◽  
Properties Of Coatings ◽  
Hard Particles ◽  
Microstructure And Mechanical Properties ◽  
Nickel Based Alloy

AbstractNi-based alloy coatings prepared by laser cladding has high bonding strength, excellent wear resistance and corrosion resistance. The mechanical properties of coatings can be further improved by changing the composition of alloy powders. This paper reviewed the improved microstructure and mechanical properties of Ni-based composite coatings by hard particles, single element and rare earth elements. The problems that need to be solved for the particle-reinforced nickel-based alloy coatings are pointed out. The prospects of the research are also discussed.

scholarly journals Few-layer graphene aqueous suspensions for polyurethane composite coatings

MRS Advances ◽  
2016 ◽  
Vol 2 (1) ◽  
pp. 57-62 ◽  
Author(s):  
Eunice Cunha ◽  
Fernando Duarte ◽  
M. Fernanda Proença ◽  
M. Conceição Paiva
Keyword(s):  
Mechanical Properties ◽  
Tensile Testing ◽  
Composite Coatings ◽  
Composite Films ◽  
Water Vapor Permeability ◽  
Waterborne Polyurethane ◽  
Vapor Permeability ◽  
Layer Graphene ◽  
Polyurethane Composite ◽  
Few Layer Graphene

ABSTRACTGraphite nanoplates (GnP) have recently attracted attention as an economically viable alternative for the development of functional and structural nanocomposites. The incorporation of GnP into waterborne polyurethane (WPU) with loadings from 0.1 to 10 wt.% was studied. The mechanical properties of the composite films were assessed by tensile testing showing an increase of the Young’s modulus up to 48%. The electrical conductivity increased by 9 orders of magnitude and the water vapor permeability of the composite films decreased 57% for composites containing 5.0 wt.% of GnP.

About Determing the Microhardness of Composite Coatings

2021 ◽  
Vol 1037 ◽  
pp. 486-493
Author(s):  
Sergey Y. Zhachkin ◽  
Anatoly I. Zavrazhnov ◽  
Nikita A. Penkov ◽  
George V. Kudryavtsev ◽  
Paul V. Tsisarenko
Keyword(s):  
Composite Coating ◽  
Mechanical Treatment ◽  
Composite Coatings ◽  
Operational Parameters ◽  
Deposition Parameters ◽  
Cylinder Liners ◽  
High Degree ◽  
Applied Coating ◽  
Positive Effect ◽  
Selection Of

One of the fundamental tasks in restoring the operability of cylinder liners is the application of a composite coating with a predetermined microhardness value. The authors have developed a technology for applying composite coatings based on iron on cylindrical surfaces, which makes it possible to vary the physical, mechanical and operational parameters of the formed iron-containing coating due to the planned selection of the deposition parameters. This eliminates the need for mechanical treatment of the applied coating, which is the reason for the high degree of rejection parts that undergo the iron-on operation. Contact interaction of the working tool with the formed layer of the composite coating has a positive effect on the value of its roughness.

scholarly journals Influence of Polyurea Composite Coating on Selected Mechanical Properties of AISI 304 Steel

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3137 ◽  
Author(s):  
Monika Duda ◽  
Joanna Pach ◽  
Grzegorz Lesiuk
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resin ◽  
Composite Coating ◽  
Composite Coatings ◽  
Glass Fabric ◽  
Coated Sample ◽  
Hemp Fiber ◽  
Aisi 304 ◽  
Aisi 304 Steel ◽  
The Impact

This paper contains experimental results of mechanical testing of the AISI 304 steel with composite coatings. The main goal was to investigate the impact of the applied polyurea composite coating on selected mechanical properties: Adhesion, impact resistance, static behavior, and, finally, fatigue lifetime of notched specimens. In the paper the following configurations of coatings were tested: EP (epoxy resin), EP_GF (epoxy resin + glass fabric), EP_GF_HF (epoxy resin + glass fabric hemp fiber), EP_PUA (epoxy resin + polyurea) resin, EP_GF_PUA (epoxy resin + glass fabric + polyurea) resin, and EP_GF_HF_PUA (epoxy resin + glass fabric + hemp fiber + polyurea) resin. The highest value of force required to break adhesive bonds was observed for the EP_PUA coating, the smallest for the single EP coating. A tendency of polyurea to increase the adhesion of the coating to the base was noticed. The largest area of delamination during the impact test was observed for the EP_GF_HF coating and the smallest for the EP-coated sample. In all tested samples, observed delamination damage during the pull-off test was located between the coating and the metallic base of the sample.

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