scholarly journals Compressive Strength of Conventional Glass Ionomer Cement Modified with TiO2 Nano-Powder and Marine-Derived HAp Micro-Powder

Materials ◽  
2021 ◽  
Vol 14 (17) ◽  
pp. 4964
Author(s):  
Ana Ivanišević ◽  
Valentina Brzović Rajić ◽  
Ana Pilipović ◽  
Matej Par ◽  
Hrvoje Ivanković ◽  
...  

The aim of this research was to investigate the compressive strength (CS), breaking strength (BS), and compressive modulus (CM) of conventional glass ionomer cement (GIC) modified with TiO2 nano particles, marine-derived hydroxyapatite (md-HAp) microparticles (<45 µm), and a combination of TiO2 NP and md-HAp particles. The materials used in the study were conventional GIC Fuji IX GP Extra (GC Corporation, Tokyo, Japan), TiO2 powder P25 (Degussa, Essen, Germany), and HAp synthesized from cuttlefish bone and ground in a mortar to obtain md-HAp powder. md-HAp was characterized using FTIR and SEM analysis. There were four groups of GIC samples: (i) Fuji IX control group, (ii) powder modified with 3 wt% TiO2, (iii) powder modified with 3 wt% HAp, and (iv) powder modified with 1.5 wt% TiO2 + 1.5 wt% HAp. Measurements were performed in a universal testing machine, and CS, BS, and CM were calculated. Statistical analysis was performed using ANOVA and Tukey’s tests. CS, BS, and CM differed significantly between the Fuji IX control group and all experimental groups while differences between the experimental groups were not statistically significant. The addition of TiO2 NP, md-HAp micro-sized particles, and a combination of TiO2 and md-HAp reduced the CS, BS, and CM of conventional GICs when mixed at the powder/liquid (p/l) ratio recommended by the manufacturer.

2016 ◽  
Vol 40 (5) ◽  
pp. 400-403 ◽  
Author(s):  
P Subramaniam ◽  
KL Girish Babu ◽  
G Neeraja ◽  
S Pillai

Propolis is a natural resinous substance produced by honey bees. The antimicrobial effects of glass ionomer cement have been shown to improve with the addition of propolis; however its effect on the physicomechanical properties of the cement is not known. Aim: The purpose of this study was to evaluate the compressive strength and solubility of conventional restorative glass ionomer cement following the addition of propolis. Study design: Twenty half cylindrical samples were prepared with conventional restorative glass ionomer cement formed the control group. Another twenty samples were prepared with propolis added to conventional restorative glass ionomer cement formed the experimental group. The compressive strength was assessed using universal testing machine. To assess solubility, the samples were immersed in deionised water at room temperature, for 7 days. The solubility was measured as a difference in the weight of the sample; prior to immersion and following immersion at the end of each day. Results: The control group had a significantly higher mean compressive strength of 146.26 Mpa as compared to the experimental group (135.06 Mpa). The solubility between the groups was significant. Conclusion: In comparison to the control group, incorporation of propolis to conventional restorative glass ionomer cement decreased the compressive strength significantly. The solubility of the cement in the experimental group increased significantly over 7day period as compared to the control group.


2017 ◽  
Vol 41 (1) ◽  
pp. 62-65 ◽  
Author(s):  
P Subramaniam ◽  
KL Girish Babu ◽  
G Neeraja ◽  
S Pillai

Propolis is a natural resinous substance produced by honey bees. The antimicrobial effects of glass ionomer cement have been shown to improve with the addition of propolis; however its effect on the physicomechanical properties of the cement is not known. Aim: The purpose of this study was to evaluate the compressive strength and solubility of conventional restorative glass ionomer cement following the addition of propolis. Study design: Twenty half cylindrical samples were prepared with conventional restorative glass ionomer cement formed the control group. Another twenty samples were prepared with propolis added to conventional restorative glass ionomer cement formed the experimental group. The compressive strength was assessed using universal testing machine. To assess solubility, the samples were immersed in deionised water at room temperature, for 7 days. The solubility was measured as a difference in the weight of the sample; prior to immersion and following immersion at the end of each day. Results: The control group had a significantly higher mean compressive strength of 146.26 Mpa as compared to the experimental group (135.06 Mpa). The solubility between the groups was significant. Conclusion: In comparison to the control group, incorporation of propolis to conventional restorative glass ionomer cement decreased the compressive strength significantly. The solubility of the cement in the experimental group increased significantly over 7day period as compared to the control group.


2007 ◽  
Vol 21 (3) ◽  
pp. 204-208 ◽  
Author(s):  
André Mallmann ◽  
Jane Clei Oliveira Ataíde ◽  
Rosa Amoedo ◽  
Paulo Vicente Rocha ◽  
Letícia Borges Jacques

The purpose of this study was to evaluate the compressive strength of two glass ionomer cements, a conventional one (Vitro Fil® - DFL) and a resin-modified material (Vitro Fil LC® - DFL), using two test specimen dimensions: One with 6 mm in height and 4 mm in diameter and the other with 12 mm in height and 6 mm in diameter, according to the ISO 7489:1986 specification and the ANSI/ADA Specification No. 66 for Dental Glass Ionomer Cement, respectively. Ten specimens were fabricated with each material and for each size, in a total of 40 specimens. They were stored in distilled water for 24 hours and then subjected to a compressive strength test in a universal testing machine (EMIC), at a crosshead speed of 0.5 mm/min. The data were statistically analyzed using the Kruskal-Wallis test (5%). Mean compressive strength values (MPa) were: 54.00 ± 6.6 and 105.10 ± 17.3 for the 12 mm x 6 mm sample using Vitro Fil and Vitro Fil LC, respectively, and 46.00 ± 3.8 and 91.10 ± 8.2 for the 6 mm x 4 mm sample using Vitro Fil and Vitro Fil LC, respectively. The resin-modified glass ionomer cement obtained the best results, irrespective of specimen dimensions. For both glass ionomer materials, the 12 mm x 6 mm matrix led to higher compressive strength results than the 6 mm x 4 mm matrix. A higher variability in results was observed when the glass ionomer cements were used in the larger matrices.


e-GIGI ◽  
2015 ◽  
Vol 3 (1) ◽  
Author(s):  
Vanessa M. Roeroe ◽  
Dinar A. Wicaksono ◽  
Juliatri .

Abstract: Glass ionomer cement is restorative materials that attached on the enamel and dentin through chemical combination, that consists of powder and liquid. GIC powder and liquid are alumino silikat glass and from poliakrilik acid. Characters of GIC are biocompatible, removing fluoride, prevent developing cariest, esthetic, translucent, low solubility, anti bacterial. Nowadays, aperitif that consumed by people has sour nature and solvent. The purpose of this research is to know description compressive strength transformation of type II GIC that soaked in variant percentage of aperitif. This was an experimental research used post test only control group design. Each samples were 5 for every treat. Sample consisted of Type II SIK materials which soaked during 24 hours in 5%, 10%, 40% aperitif, and aquades as control. Endurance and Strength of Type II GIC measured by compression test device. From research result available that mean of strength GIC measurement which soaked in aperitif 5%, 10%, 40%, aquades such as 2,84 MPa, 3,36 MPa, 4,5 MPa, and 2,58 MPa as control variable. Description of this research is transformation of compressive strength GIC increasing if soaked in higher percentage aperitif because sample appication was not yet perfect.Keywords: compressive strength, glass ionomer cement, aperitifAbstrak: Semen ionomer kaca adalah bahan restorasi yang melekat pada enamel dan dentin melalui ikatan kimia, terdiri dari campuran powder dan liquid. PowderSIK adalah kaca aluminosilikat dan liquid larutan asam poliakrilik. Beberapa sifat yang dimiliki semen ionomer kaca yaitu biokompatibilitas melepas fluor sehingga dapat mencegah karies lebih lanjut, estetis, daya larut rendah, translusen, dan bersifat anti bakteri. Minuman beralkohol yang banyak dikonsumsi masyarakat saat ini mempunyai sifat asam dan sebagai pelarut. Tujuan penelitian ini untuk mengetahui gambaran perubahan kekuatan tekan bahan tumpatan SIK tipe II yang direndam dalam minuman beralkohol dengan berbagai presentase. Penelitian ini merupakan penelitian eksperimental menggunakan post test only control group design. Masing-masing sampel dibuat 5 buah untuk setiap perlakuan. Sampel terdiri atas bahan SIK tipe II yang direndam dengan variasi presentase 5%, 10%, 40% alkohol dan aquades sebagai kontrol selama 24 jam. Kekuatan tekan SIK diukur menggunakan alat tes kompresi. Berdasarkan hasil penelitian didapatkan rata-rata pengukuran kekuatan SIK yang direndam dalam alkohol 5%, 10%, 40%, dan kontrol aquades masing-masing 2,84 MPa, 3,36 MPa, 4,5 MPa, 2,58 MPa. Gambaran dari hasil penelitian ini bahwa perubahan kekuatan tekan SIK semakin meningkat apabila direndam dalam kadar minuman beralkohol lebih tinggi karena proses pembuatan sampel SIK belum sempurna.Kata kunci: kekuatan tekan, semen ionomer kaca, minuman beralkohol


2018 ◽  
Vol 14 (1) ◽  
pp. 24
Author(s):  
Dr. Sazan Sherdil Saleem

The present study was aimed to evaluate and compare the compressive strength ofconventional glass ionomer cement with resin modified glass ionomer, compomer andmicrohybrid composite. A total of 40 specimens of esthetic restorative materials werefabricated using customized cylindrical teflon mould measuring 6mm height and 4mmdiameter and were grouped with ten specimens in each group, Group I: Conventionalglass ionomer cement (Fuji II). Group II: Resin modified glass ionomer (Fuji II LC).Group III: Compomer (Dyract AP) and Group IV: Microhybrid composite resin(Tetric Ceram).They were covered with Mylar strip and were cured using LED lightcuring unit. Compressive strength was evaluated using Universal testing machine. Theresult showed that there were a significant difference among the groups in whichTetric Ceram showed highest compressive strength and Fuji II showed the leastcompressive strength


2020 ◽  
Vol 10 (11) ◽  
pp. 1960-1964
Author(s):  
Mansour K. A. Assery ◽  
Abdulrahman Alshubat ◽  
AlWaleed Abushanan ◽  
Nawaf Labban ◽  
Mohamed Hashem

The study evaluated the addition of silver (Ag) and titanium dioxide (TiO2) nanoparticles to conventional glass ionomer cement (GIC), considering compressive strength (CS), diametral tensile strength (DTS), flexural strength (FS), and hardness. Ag and TiO2 nanoparticles were blended into the powder of a commercially available GIC restorative material at 5% (w/w). Unblended powder was used as a control. One hundred twenty samples were prepared from two study groups and one control group (n = 10). CS, DTS, and FS were evaluated using a universal testing machine, while hardness was measured by Vickers microhardness testing. The data obtained were analyzed using One-way analysis of variance and the Tukey?s test (p < 0.05). GIC containing Ag and TiO2 nanoparticles significantly improved the CS, DTS, and hardness compared to the control group (p < 0.05). However, the FS was not much affected by the addition of either of the nanoparticles (p >0.05). TiO2 blended GIC demonstrated significantly higher CS (154.20+2.38) and DTS (13.2±0.5 MPa) compared to control 117.2±1.2 MPa and 7.2 ±0.8 MPa, respectively. While Blend of GIC+Ag nanoparticles showed the highest FS (29.0±0.7 MPa). Additionally, the blend of GIC+TiO2 exhibited the highest hardness (90.4±1.1 VHN). Ag and TiO2 blended GICs might guarantee their use in occlusal or higher stress-bearing areas.


2020 ◽  
Vol 47 (3) ◽  
pp. 320-326
Author(s):  
Kunho Lee ◽  
Jongsoo Kim ◽  
Jisun Shin ◽  
Miran Han

The aim of this study was to compare compressive strength and microhardness of recently introduced alkasite restorative materials with glass ionomer cement and flowable composite resin.For each material, 20 samples were prepared respectively for compressive strength and Vickers microhardness test. The compressive strength was measured with universal testing machine at crosshead speed of 1 mm/min. And microhardness was measured using Vickers Micro hardness testing machine under 500 g load and 10 seconds dwelling time at 1 hour, 1 day, 7 days, 14 days, 21 days and 35 days.The compressive strength was highest in composite resin, followed by alkasite, and glass ionomer cement. In microhardness test, composite resin, which had no change throughout experimental periods, showed highest microhardness in 1 hour, 1 day, and 7 days measurement. The glass ionomer cement showed increase in microhardness for 7 days and no difference was found with composite resin after 14 days measurement. For alkasite, maximum microhardness was measured on 14 days, but showed gradual decrease.


2014 ◽  
Vol 43 (4) ◽  
pp. 236-240 ◽  
Author(s):  
Luana Mafra MARTI ◽  
Elcilaine Rizzato AZEVEDO ◽  
Margareth da MATA ◽  
Elisa Maria Aparecida GIRO ◽  
Angela Cristina Cilense ZUANON

INTRODUCTION:For presenting wide antibacterial activity, chlorhexidine (CHX) has been extensively used in dentistry and can be easily incorporated into the glass ionomer cement (GIC) and consequently released into the oral cavity.AIM: The aim of this study was porosity and compression strength of a GIC, that was added to different concentrations of CHX.MATERIAL AND METHOD: Specimens were prepared with GIC (Ketac Molar Esaymix) and divided into 4 groups according to the concentration of CHX: control, 0.5% and 1% and 2% (n = 10). For analysis of pores specimens were fractured with the aid of hammer and chisel surgical, so that the fracture was performed in the center of the specimens, dividing it in half and images were obtained from a scanning electron microscope (SEM) analyzed in Image J software. The compressive strength test was conducted in a mechanical testing machine (EMIC - Equipment and Testing Systems Ltd., Joseph of the Pines, PR, Brazil). Statistical analysis was performed by ANOVA, Tukey test. Significance level of 5%.RESULT: No statistically significant changes between the study groups was observed both for the number of pores as well as for the compressive strength.CONCLUSION: The use of GIC associated with CHX gluconate 1% and 2% is the best option to be used in dental practice.


2011 ◽  
Vol 264-265 ◽  
pp. 508-512
Author(s):  
Ammar A. Mustafa ◽  
Khalid A. S. Al-Khateeb ◽  
Ahmad Faris Ismail

Experimental glass ionomer cement was prepared for the purpose of this study. Twenty disk specimens (16mm diameter x 10mm height) of test-GIC were prepared for the diametral tensile strength (DTS) test and twenty cylindrical specimens (6 mm diameter x 16mm height) were prepared for the compressive strength (CS) test. Specimens were stored in an artificial saliva at 37º C and (50±10%) of relative humidity in an incubator until testing. Five specimens of each GIC were submitted to CS and DTS test in each period, namely 1 hour, 24 hours, 7 days and 28 days. The specimens were tested in a Universal Testing Machine (Instron 1122, Instron corp., High Wycombe, U.K.) at a crosshead speed of 1.0mm/min for CS and 0.5mm/min for the DTS test until failure occurred. The results have revealed that incorporation of lithium fluoride in the formula of the test GIC might impart an increase in the mechanical properties of the GICs


2021 ◽  
Vol 10 (7) ◽  
pp. e5110716150
Author(s):  
Walber Maeda ◽  
Wayne Martins Nascimento ◽  
Marcelo Santos Coelho ◽  
Danilo de Luca Campos ◽  
João Paulo Drumond ◽  
...  

Aim: In this study was evaluated the fracture resistance of endodontically treated maxillary premolars restored with      different restorative materials. Methods: Sixty maxillary premolars were submitted to the same mesio-occlusal-distal cavity preparation, endodontic treatment and divided into 5 groups (n = 10): Coltosol Group – GCO restored with calcium silicate material; Glass Ionomer Cement Group – GGIC, restored with Maxxion R; Modified Glass Ionomer Cement – GMGIC, restored with Gold Label 2; Composite Group - GC, restored with Z100, and the positive control group (GP) - left unrestored. One group remained intact (n=10) serving as negative control (GN). Samples were subjected to fracture resistance testing by the universal testing machine until fracture occurred and was registered in newtons (N). Fracture pattern was assessed and described as favorable or unfavorable. The results were statistically analyzed by 1-way analysis of variance and the post hoc Tukey test with significant statistical difference at P < 0.05.  Results: Higher fracture resistance results were found for GC (1,128.35 ± 249.17), GMGIC (1,250.77 ± 173.29), and GN (1,277.22 ± 433.44) (P < .05). More favorable fractures were observed in the GCO (6), GC (7), and GN (7) (P < .05). Conclusion: Teeth restored with composite and modified GIC presented the same resistance as intact teeth. Teeth restored with Coltosol and GGIC presented similar resistance to unrestored teeth.


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