scholarly journals Inverse Determination of Johnson–Cook Parameters of Additively Produced Anisotropic Maraging Steel

Materials ◽  
2021 ◽  
Vol 15 (1) ◽  
pp. 26
Author(s):  
Rocco Eisseler ◽  
Daniel Gutsche ◽  
Clemens Maucher ◽  
Hans-Christian Möhring
Keyword(s):  
Cutting Force ◽  
Orthogonal Cutting ◽  
Test Load ◽  
Powder Bed ◽  
Inverse Approach ◽  
Process Characteristics ◽  
Property Identification ◽  
Layer Orientation ◽  
Good Agreement

In powder bed-based additive manufacturing (AM), complex geometries can be produced in a layer-wise approach. Results of material science experiments regarding material property identification, e.g., tensile strength, show interdependencies between the test load direction and the layer orientation. This goes hand-in-hand with the measured cutting force, changing with the relative angle between cutting direction and layer orientation in orthogonal cutting tests. However, due to the specific process characteristics, the layer orientation results in anisotropic material properties. Therefore, during machining, the material behaves depending on the buildup direction, which influences the cutting process. To predict this behavior, a simplified inverse approach is developed to determine the buildup direction-dependent parameters of a modified Johnson–Cook model for cutting simulation. To qualify these cutting models, mainly the cutting force and additionally the chip formation examined during orthogonal cuts are used. In the present paper, the influence of the laser-powder-bed-fusion (LPBF) process parameters on subtractive post-processing are shown. A good agreement between verification experiments and simulations is achieved.

Study on Determination of Friction Model at the Tool-Chip Interface of Titanium Alloy Ti6Al4V Based on Orthogonal Cutting

2011 ◽  
Vol 117-119 ◽  
pp. 1788-1791
Author(s):  
Yue Feng Yuan ◽  
Wu Yi Chen
Keyword(s):  
Titanium Alloy ◽  
Cutting Force ◽  
Metal Cutting ◽  
Orthogonal Cutting ◽  
Cutting Speed ◽  
Friction Model ◽  
Carbide Tool ◽  
Orthogonal Turning ◽  
Titanium Alloy Ti6al4v

It is necessary for cutting simulation to determine the friction model at the tool-chip interface suitable for metal cutting process. Cutting force experiments in orthogonal turning titanium alloy TI6AL4V are carried out with cement carbide tool KW10. The Coulomb frictions at the tool-chip interface are calculated based on measured cutting force, and the friction model is regressed, where cutting speed and feed rate are presented.

COMPARATIVE ACTION OF VARIOUS OESTROGENIC COMPOUNDS ON MOUSE VAGINAL SIALIC ACIDS (II)

1969 ◽  
Vol 62 (4) ◽  
pp. 663-670 ◽  
Author(s):  
Lars Carlborg
Keyword(s):  
Sialic Acid ◽  
Response Curve ◽  
Sialic Acids ◽  
Clear Cut ◽  
Suitable Parameter ◽  
Sufficient Degree ◽  
Comparative Action ◽  
Relative Potencies ◽  
Good Agreement

ABSTRACT Oestrogens administered in lower doses than necessary to induce full cornification of the mouse vagina induce mucification. It was shown previously that the degree of mucification could be estimated by quantitative determination of sialic acids. A suitable parameter for oestrogen assay was the measurement of vaginal sialic acid concentration which exhibited a clear cut dose response curve. Eleven assays of various oestrogens were performed with this method. Their estimated relative potencies were in good agreement with other routine oestrogen assays. A statistically sufficient degree of precision was found. The sensitivity was of the same order, or slightly higher, than the Allen-Doisy test.

Determination of cutting force of roll-formed section in shaped dies-knife guillotine

2020 ◽  
pp. 373-376
Author(s):  
S.V. Povorov ◽  
D.V. Egorov ◽  
D.S. Volgin
Keyword(s):  
Cutting Force ◽  
Cutting Process ◽  
Sheet Blank

The change in cutting force in the cutting process of roll-formed section in shaped dies-knife guillotine is studied. It is established that to calculate the cutting force in shaped guillotine, one can use formulas to determine the cutting force of sheet blank on conventional straight knives guillotine.

scholarly journals Serrated Chips Formation in Micro Orthogonal Cutting of Ti6Al4V Alloys with Equiaxial and Martensitic Microstructures

Micromachines ◽  
2019 ◽  
Vol 10 (3) ◽  
pp. 197 ◽  
Author(s):  
ZeJia Zhao ◽  
Suet To ◽  
ZhuoXuan Zhuang
Keyword(s):  
Cutting Force ◽  
Unit Length ◽  
Orthogonal Cutting ◽  
Machining Process ◽  
Orthogonal Machining ◽  
Large Yield ◽  
Power Spectral ◽  
Straight Line ◽  
Serrated Chips ◽  
Electropulsing Treatment

The formation of serrated chips is an important feature during machining of difficult-to-cut materials, such as titanium alloy, nickel based alloy, and some steels. In this study, Ti6Al4V alloys with equiaxial and acicular martensitic microstructures were adopted to analyze the effects of material structures on the formation of serrated chips in straight line micro orthogonal machining. The martensitic alloy was obtained using highly efficient electropulsing treatment (EPT) followed by water quenching. The results showed that serrated chips could be formed on both Ti6Al4V alloys, however the chip features varied with material microstructures. The number of chip segments per unit length of the alloy with martensite was more than that of the equiaxial alloy due to poor ductility. Besides, the average cutting and thrust forces were about 8.41 and 4.53 N, respectively, for the equiaxed Ti6Al4V alloys, which were consistently lower than those with a martensitic structure. The high cutting force of martensitic alloy is because of the large yield stress required to overcome plastic deformation, and this force is also significantly affected by the orientations of the martensite. Power spectral density (PSD) analyses indicated that the characteristic frequency of cutting force variation of the equiaxed alloy ranged from 100 to 200 Hz, while it ranged from 200 to 400 Hz for workpieces with martensites, which was supposedly due to the formation of serrated chips during the machining process.

An Automated Method for the Determination of Serum Calcium with Glyoxal Bis (2-Hydroxyanil)

1967 ◽  
Vol 13 (6) ◽  
pp. 515-520 ◽  
Author(s):  
Genevieve Farese ◽  
Janice L Schmidt ◽  
Milton Mager
Keyword(s):  
Serum Calcium ◽  
Automated Analysis ◽  
Automated Method ◽  
Good Agreement

Abstract A completely automated analysis is described for the determination of serum calcium with glyoxal bis (2-hydroxyanil) solution (GBHA). The method is simple and precise, and the data obtained are in good agreement with results obtained by the manual GBHA procedure.

Numerical evaluation of hydrodynamic characteristics of planing hulls by using a hybrid method

2021 ◽  
pp. 147509022199024
Author(s):  
Emre Kahramanoglu ◽  
Silvia Pennino ◽  
Huseyin Yilmaz
Keyword(s):  
Experimental Data ◽  
Hybrid Method ◽  
Design Stage ◽  
Hydrodynamic Characteristics ◽  
Calm Water ◽  
Preliminary Design Stage ◽  
Reduction Function ◽  
Hull Forms ◽  
Good Agreement

The hydrodynamic characteristics of the planing hulls in particular at the planing regime are completely different from the conventional hull forms and the determination of these characteristics is more complicated. In the present study, calm water hydrodynamic characteristics of planing hulls are investigated using a hybrid method. The hybrid method combines the dynamic trim and sinkage from the Zarnick approach with the Savitsky method in order to calculate the total resistance of the planing hull. Since the obtained dynamic trim and sinkage values by using the original Zarnick approach are not in good agreement with experimental data, an improvement is applied to the hybrid method using a reduction function proposed by Garme. The numerical results obtained by the hybrid and improved hybrid method are compared with each other and available experimental data. The results indicate that the improved hybrid method gives better results compared to the hybrid method, especially for the dynamic trim and resistance. Although the results have some discrepancies with experimental data in terms of resistance, trim and sinkage, the improved hybrid method becomes appealing particularly for the preliminary design stage of the planing hulls.

scholarly journals An SPRi Biosensor for Determination of the Ovarian Cancer Marker HE4 in Human Plasma

Sensors ◽  
2021 ◽  
Vol 21 (10) ◽  
pp. 3567
Author(s):  
Beata Szymanska ◽  
Zenon Lukaszewski ◽  
Beata Zelazowska-Rutkowska ◽  
Kinga Hermanowicz-Szamatowicz ◽  
Ewa Gorodkiewicz
Keyword(s):  
Ovarian Cancer ◽  
Cancer Patients ◽  
Tumor Resection ◽  
Analytical Signal ◽  
Cancer Marker ◽  
Human Epididymis Protein 4 ◽  
Pearson Coefficient ◽  
Rabbit Polyclonal Antibody ◽  
Good Agreement

Human epididymis protein 4 (HE4) is an ovarian cancer marker. Various cut-off values of the marker in blood are recommended, depending on the method used for its determination. An alternative biosensor for HE4 determination in blood plasma has been developed. It consists of rabbit polyclonal antibody against HE4, covalently attached to a gold chip via cysteamine linker. The biosensor is used with the non-fluidic array SPRi technique. The linear range of the analytical signal response was found to be 2–120 pM, and the biosensor can be used for the determination of the HE4 marker in the plasma of both healthy subjects and ovarian cancer patients after suitable dilution with a PBS buffer. Precision (6–10%) and recovery (101.8–103.5%) were found to be acceptable, and the LOD was equal to 2 pM. The biosensor was validated by the parallel determination of a series of plasma samples from ovarian cancer patients using the Elecsys HE4 test and the developed biosensor, with a good agreement of the results (a Pearson coefficient of 0.989). An example of the diagnostic application of the developed biosensor is given—the influence of ovarian tumor resection on the level of HE4 in blood serum.

scholarly journals Influence of tool edge form factor and cutting parameters on milling performance

2021 ◽  
Vol 13 (4) ◽  
pp. 168781402110090
Author(s):  
Xuefeng Zhao ◽  
Hao Qin ◽  
Zhiguo Feng
Keyword(s):  
Form Factor ◽  
Simulation Model ◽  
Cutting Force ◽  
Surface Quality ◽  
High Speed ◽  
Orthogonal Cutting ◽  
Cutting Temperature ◽  
Tool Edge ◽  
Drag Finishing ◽  
Edge Preparation

Tool edge preparation can improve the tool life, as well as cutting performance and machined surface quality, meeting the requirements of high-speed and high-efficiency cutting. In general, prepared tool edges could be divided into symmetric or asymmetric edges. In the present study, the cemented carbide tools were initially edge prepared through drag finishing. The simulation model of the carbide cemented tool milling steel was established through Deform software. Effects of edge form factor, spindle speed, feed per tooth, axial, and radial cutting depth on the cutting force, the tool wear, the cutting temperature, and the surface quality were investigated through the orthogonal cutting simulation. The simulated cutting force results were compared to the results obtained from the orthogonal milling experiment through the dynamometer Kistler, which verified the simulation model correctness. The obtained results provided a basis for edge preparation effect along with high-speed and high effective cutting machining comprehension.

scholarly journals Potentiometric Surfactant Sensor Based on 1,3-Dihexadecyl-1H-benzo[d]imidazol-3-ium for Anionic Surfactants in Detergents and Household Care Products

Molecules ◽  
2021 ◽  
Vol 26 (12) ◽  
pp. 3627
Author(s):  
Nikola Sakač ◽  
Dubravka Madunić-Čačić ◽  
Dean Marković ◽  
Lucija Hok ◽  
Robert Vianello ◽  
...  
Keyword(s):  
Anionic Surfactants ◽  
Negative Impact ◽  
Ion Pair ◽  
Two Phase ◽  
Potentiometric Response ◽  
Titration Curves ◽  
Signal Change ◽  
Nernstian Slope ◽  
Good Agreement

A 1,3-dihexadecyl-1H-benzo[d]imidazol-3-ium-tetraphenylborate (DHBI-TPB) ion-pair implemented in DHBI-TPB surfactant sensor was used for the potentiometric quantification of anionic surfactants in detergents and commercial household care products. The DHBI-TPB ion-pair was characterized by FTIR spectroscopy and computational analysis which revealed a crucial contribution of the C–H∙∙∙π contacts for the optimal complex formation. The DHBI-TPB sensor potentiometric response showed excellent analytical properties and Nernstian slope for SDS (60.1 mV/decade) with LOD 3.2 × 10−7 M; and DBS (58.4 mV/decade) with LOD 6.1 × 10−7 M was obtained. The sensor possesses exceptional resistance to different organic and inorganic interferences in broad pH (2–10) range. DMIC used as a titrant demonstrated superior analytical performances for potentiometric titrations of SDS, compared to other tested cationic surfactants (DMIC > CTAB > CPC > Hyamine 1622). The combination of DHBI-TPB sensor and DMIC was successfully employed to perform titrations of the highly soluble alkane sulfonate homologues. Nonionic surfactants (increased concentration and number of EO groups) had a negative impact on anionic surfactant titration curves and a signal change. The DHBI-TPB sensor was effectively employed for the determination of technical grade anionic surfactants presenting the recoveries from 99.5 to 101.3%. The sensor was applied on twelve powered samples as well as liquid-gel and handwashing home care detergents containing anionic surfactants. The obtained results showed good agreement compared to the outcomes measured by ISE surfactant sensor and a two-phase titration method. The developed DHBI-TPB surfactant sensor could be used for quality control in industry and has great potential in environmental monitoring.

scholarly journals Bichromatic Photoassociation Spectroscopy for the Determination of Rotational Constants of Cs2 0 u + Long-Range State below the 6S1/2 + 6P1/2 Asymptote

Molecules ◽  
2020 ◽  
Vol 25 (17) ◽  
pp. 3963
Author(s):  
Jizhou Wu ◽  
Jie Ma ◽  
Yuqing Li ◽  
Wenliang Liu ◽  
Peng Li ◽  
...  
Keyword(s):  
Long Range ◽  
Spectroscopic Technique ◽  
Rigid Rotor ◽  
Simple Analysis ◽  
Rotational Constants ◽  
Vibrational Levels ◽  
Photoassociation Spectroscopy ◽  
Rotor Model ◽  
Good Agreement

This article demonstrates new observation of the high-resolution ro-vibrational bichromatic photoassociation spectra (BPAS) of Cs2 in the 0u+ long-range state below the asymptotes 6S1/2 + 6P1/2. By combining with a modulation spectroscopic technique, precise references of the frequency differences have been engineered through the BPAS, with which the rotational constants of low-lying vibrational levels of the Cs20u+ long-range state have been accurately determined by fitting the frequency differences to the non-rigid-rotor model. The rotational constants for the newly observed seven ro-vibrational levels are summarized and disagreement for the level ῦ = 498 is clarified. The rotational constants of different vibrational levels demonstrate strong perturbations of the related energy structures. A simple analysis is performed and shows good agreement with experimental results.

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