scholarly journals A Comprehensive Study of Dynamic Recrystallization Behavior of Mg Alloy with 3 wt.% Bi Addition

Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 838
Author(s):  
Hui Yu ◽  
Hao Liu ◽  
Binan Jiang ◽  
Wei Yu ◽  
Shaoming Kang ◽  
...  

The effect of the addition of bismuth on the dynamic recrystallization (DRX) behavior of the matrix has been investigated by comparing coarse grain pure Mg with the addition of 3 wt.% Bi, using a uniaxial compression test in the temperature range of 473–623 K and the strain rate of 0.01–10 s−1. The constitutive equation, processing map, microstructure, and texture evolution of the Mg-3Bi alloy were systematically investigated. The results showed that the Bi addition could refine the grain size and accelerate the DRX process. The DRX kinetics is discussed in detail, accompanied by extensive characterization employing EBSD analysis. The DRX of the Mg-3Bi alloy depended on the deformation temperature rather than the strain rate. The {10–12} tensile twin appeared at 573 K/0.01–0.1 s−1, and discontinuous DRX (DDRX), continuous DRX (CDRX) as the main mechanism in the case of 573 K/0.01 s−1, while the dominant mechanism was DDRX when deformation temperature and strain rate increased. Particle-stimulated nucleation (PSN) was also involved in the DRX of this new RE-free Mg alloy.

2018 ◽  
Vol 37 (7) ◽  
pp. 635-647 ◽  
Author(s):  
Le Li ◽  
Li-yong Wang

AbstractIn order to study dynamic recrystallization behavior of the as-extruded 3Cr20Ni10W2 under isothermal compression conditions, a cellular automaton (CA) model was applied to simulate hot compression. Analysis on the strain–stress curves indicates that dynamic recrystallization is the main softening mechanism for the 3Cr20Ni10W2 when the deformation occurred in the temperature range of 1203–1303 K with an interval of 50 K and strain rate range of 0.01–10 s−1. The deformation temperature and strain rate have a significant influence on the dynamically recrystallized grain size. Subsequently, a CA model is established to simulate the dynamic recrystallization behaviors of the studied alloy. The simulated results show that the mean grain size increases with the increased deformation temperature and decreases with the increased strain rate, which is consistent with the experimental result. In addition, the average absolute relative error, which is 13.14%, indicates that the process of the dynamic recrystallization and the dynamically recrystallized grain size can be well predicted by the present CA model.


2016 ◽  
Vol 693 ◽  
pp. 674-679
Author(s):  
Hai Peng Ji ◽  
Li Ge Zhang ◽  
Jing Liu ◽  
Tai Yong Wang

The established cellular automata model of dynamic recrystallization for 316LN simulated microstructure evolution of recrystallization nucleation and grain growth under different conditions. And on the basis of cellular automata model, the influence of strain, strain rate, deformation temperature on dynamic recrystallization behavior was analyzed. Though the hot compress experiment done on the Gleeble-3500 thermo mechanical simulator, combined with metallographic experiment, the microstructure at deformation temperature of 950 oC, 1050 oC and 1150 oC with strain rate of 0.001 s-1, 0.01 s-1, 0.1 s-1 and 1 s-1 was obtained. Simulation results are compared with metallographic microstructure, the error is small.


2013 ◽  
Vol 446-447 ◽  
pp. 117-121
Author(s):  
Hai Lin Xu ◽  
Hong Bo Dong ◽  
Yong Wang

The dynamic recrystallization behavior of TC21 alloy during hot compression deformation was investigated at 870~990 °C and strain rate of 0.001~10 s-1 on a Gleeble-3500 thermo-simulation machine. The results show that dynamic recovery and dynamic recrystallization occurs during hot deformation. As the deformation temperature increases and strain rate decreases, the softening caused by dynamic recrystallization is more obvious. According to the relevance of flow stress, strain rate and deformation temperature, the dynamic recrystallization activation energy is obtained. The constitutive equation and dynamic recrystallization kinetics motel are set up through analyzing and calculating the data of thermo-simulation.


Materials ◽  
2021 ◽  
Vol 14 (17) ◽  
pp. 5059
Author(s):  
Yuelin Song ◽  
Jiangkun Fan ◽  
Xudong Liu ◽  
Peizhe Zhang ◽  
Jinshan Li

Plane strain compression tests were used to study the deformation behavior of an Inconel 625 alloy sheet at various temperatures and strain rates. The peak stress was selected to establish the constitutive equation, and the processing maps under different strains were drawn. The results show that the effective stress–strain curve of Inconel 625 has typical dynamic recrystallization (DRX) characteristics. With the increasing deformation temperature and the decreasing strain rate, the softening effect is significantly enhanced. The parameters of the constitutive equation are calculated, and the average error of the constitutive equation is 5.68%. Through the analysis of the processing map, a deformation temperature of 950–960 °C with a strain rate of 0.007–0.05 s−1 were determined as the unstable region, and obvious local plastic-rheological zones were found in the unstable region. The optimum deformation condition was found to be 1020–1060 °C/0.005–0.03 s−1. Through electron backscattered diffraction (EBSD) characterization, it was found that both the increase of temperature and the decrease of strain rate significantly promote the recrystallization process. At a low strain rate, the main recrystallization mechanism is discontinuous dynamic recrystallization (DDRX). It is expected that the above results can provide references for the optimization of the rolling process and microstructure control of an Inconel 625 alloy sheet.


Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 605
Author(s):  
Franco Lizzi ◽  
Kashyap Pradeep ◽  
Aleksandar Stanojevic ◽  
Silvana Sommadossi ◽  
Maria Cecilia Poletti

Inconel®718 is a well-known nickel-based super-alloy used for high-temperature applications after thermomechanical processes followed by heat treatments. This work describes the evolution of the microstructure and the stresses during hot deformation of a prototype alloy named IN718WP produced by powder metallurgy with similar chemical composition to the matrix of Inconel®718. Compression tests were performed by the thermomechanical simulator Gleeble®3800 in a temperature range from 900 to 1025 °C, and strain rates scaled from 0.001 to 10 s−1. Flow curves of IN718WP showed similar features to those of Inconel®718. The relative stress softening of the IN718WP was comparable to standard alloy Inconel®718 for the highest strain rates. Large stress softening at low strain rates may be related to two phenomena: the fast recrystallization rate, and the coarsening of micropores driven by diffusion. Dynamic recrystallization grade and grain size were quantified using metallography. The recrystallization grade increased as the strain rate decreased, although showed less dependency on the temperature. Dynamic recrystallization occurred after the formation of deformation bands at strain rates above 0.1 s−1 and after the formation of subgrains when deforming at low strain rates. Recrystallized grains had a large number of sigma 3 boundaries, and their percentage increased with strain rate and temperature. The calculated apparent activation energy and strain rate exponent value were similar to those found for Inconel®718 when deforming above the solvus temperature.


Materials ◽  
2020 ◽  
Vol 13 (16) ◽  
pp. 3623 ◽  
Author(s):  
Danying Zhou ◽  
Hua Gao ◽  
Yanhua Guo ◽  
Ying Wang ◽  
Yuecheng Dong ◽  
...  

A self-designed Ti-35421 (Ti-3Al-5Mo-4Cr-2Zr-1Fe wt%) titanium alloy is a new type of low-cost high strength titanium alloy. In order to understand the hot deformation behavior of Ti-35421 alloy, isothermal compression tests were carried out under a deformation temperature range of 750–930 °C with a strain rate range of 0.01–10 s−1 in this study. Electron backscatter diffraction (EBSD) was used to characterize the microstructure prior to and post hot deformation. The results show that the stress–strain curves have obvious yielding behavior at a high strain rate (>0.1 s−1). As the deformation temperature increases and the strain rate decreases, the α phase content gradually decreases in the α + β phase region. Meanwhile, spheroidization and precipitation of α phase are prone to occur in the α + β phase region. From the EBSD analysis, the volume fraction of recrystallized grains was very low, so dynamic recovery (DRV) is the dominant deformation mechanism of Ti-35421 alloy. In addition to DRV, Ti-35421 alloy is more likely to occur in continuous dynamic recrystallization (CDRX) than discontinuous dynamic recrystallization (DDRX).


2020 ◽  
Vol 321 ◽  
pp. 12008
Author(s):  
Y.Y. Luo ◽  
X.N. Mao ◽  
H.Y. Yang ◽  
Y.F. Yin ◽  
Z.Z. Zhao ◽  
...  

The dynamic recrystallization behavior of as-cast Ti-46.5Al-3Ta-2Cr-0.2W alloy during isothermal compression process with nominal deformation of 50% and strain rates from 0.01s to 1s was investigated by electron microscopy. The results showed that the deformation mechanism of this alloy can be concluded as grain boundary sliding and mechanical twins, which induce the final dynamic recrystallization. The phase boundary bulging was found to be the major nucleation mechanism responsible for the lamellar globularization and the formation of recrystallized γ grains inside the lamellar colony under the high strain rate. The recrystallized γ grains induced by the twinning is the main mechanism for refining α2 lamellar microstructures under low strain rate.


Materials ◽  
2019 ◽  
Vol 12 (3) ◽  
pp. 510 ◽  
Author(s):  
Zhi Jia ◽  
Zexi Gao ◽  
Jinjin Ji ◽  
Dexue Liu ◽  
Tingbiao Guo ◽  
...  

High-temperature compression and electron backscatter diffraction (EBSD) techniques were used in a systematic investigation of the dynamic recrystallization (DRX) behavior and texture evolution of the Inconel625 alloy. The true stress–true strain curves and the constitutive equation of Inconel625 were obtained at temperatures ranging from 900 to 1200 °C and strain rates of 10, 1, 0.1, and 0.01 s−1. The adiabatic heating effect was observed during the hot compression process. At a high strain rate, as the temperature increased, the grains initially refined and then grew, and the proportion of high-angle grain boundaries increased. The volume fraction of the dynamic recrystallization increased. Most of the grains were randomly distributed and the proportion of recrystallized texture components first increased and then decreased. Complete dynamic recrystallization occurred at 1100 °C, where the recrystallized volume fraction and the random distribution ratios of grains reached a maximum. This study indicated that the dynamic recrystallization mechanism of the Inconel625 alloy at a high strain rate included continuous dynamic recrystallization with subgrain merging and rotation, and discontinuous dynamic recrystallization with bulging grain boundary induced by twinning. The latter mechanism was less dominant.


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