scholarly journals Femtosecond Laser Fabrication of Engineered Functional Surfaces based on Biodegradable Polymer and Biopolymer/Ceramic Composite Thin Films

Polymers ◽  
2019 ◽  
Vol 11 (2) ◽  
pp. 378 ◽  
Author(s):  
Albena Daskalova ◽  
Irina Bliznakova ◽  
Liliya Angelova ◽  
Anton Trifonov ◽  
Heidi Declercq ◽  
...  
Keyword(s):  
Thin Films ◽  
Surface Roughness ◽  
Femtosecond Laser ◽  
Surface Functionalization ◽  
Biodegradable Polymer ◽  
Photoelectron Spectroscopy ◽  
Laser Energy ◽  
Surface Characteristics ◽  
Laser Pulses ◽  
Xrd Analysis

Surface functionalization introduced by precisely-defined surface structures depended on the surface texture and quality. Laser treatment is an advanced, non-contact technique for improving the biomaterials surface characteristics. In this study, femtosecond laser modification was applied to fabricate diverse structures on biodegradable polymer thin films and their ceramic blends. The influences of key laser processing parameters like laser energy and a number of applied laser pulses (N) over laser-treated surfaces were investigated. The modification of surface roughness was determined by atomic force microscopy (AFM). The surface roughness (Rrms) increased from approximately 0.5 to nearly 3 µm. The roughness changed with increasing laser energy and a number of applied laser pulses (N). The induced morphologies with different laser parameters were compared via Scanning electron microscopy (SEM) and confocal microscopy analysis. The chemical composition of exposed surfaces was examined by FTIR, X-ray photoelectron spectroscopy (XPS), and XRD analysis. This work illustrates the capacity of the laser microstructuring method for surface functionalization with possible applications in improvement of cellular attachment and orientation. Cells exhibited an extended shape along laser-modified surface zones compared to non-structured areas and demonstrated parallel alignment to the created structures. We examined laser-material interaction, microstructural outgrowth, and surface-treatment effect. By comparing the experimental results, it can be summarized that considerable processing quality can be obtained with femtosecond laser structuring.

scholarly journals A Study of Laser Micromachining of PM Processed Ti Compact for Dental Implants Applications

Materials ◽  
2019 ◽  
Vol 12 (14) ◽  
pp. 2246 ◽  
Author(s):  
Peter Šugár ◽  
Jaroslav Kováčik ◽  
Jana Šugárová ◽  
Barbora Ludrovcová
Keyword(s):  
Surface Roughness ◽  
Laser Energy ◽  
Surface Characteristics ◽  
Xrd Analysis ◽  
Point Of View ◽  
Nanosecond Laser ◽  
Machined Surface ◽  
X Ray ◽  
Industrial Grade ◽  
Different Characteristics

The paper deals with the experimental study of laser beam micromachining of the powder metallurgy processed Ti compacts applying the industrial grade fibre nanosecond laser operating at the wavelength of 1064 nm. The influence of the laser energy density on the surface roughness, surface morphology and surface elements composition was investigated and evaluated by means of surface roughness measurement, scanning electron microscopy (SEM), energy dispersive X-Ray spectroscopy (EDS) and X-ray diffraction (XRD) analysis. The different laser treatment parameters resulted in the surfaces of very different characteristics of the newly developed biocompatible material prepared by advanced low temperature technology of hydride dehydride (HDH) titanium powder compactation. The results indicate that the laser pulse energy has remarkable effects on the machined surface characteristics which are discussed from the point of view of application in dental implantology.

scholarly journals Preparation and Properties of Superconducting thin Films by Excimer Laser Ablation

1990 ◽  
Vol 191 ◽  
Author(s):  
Michael E. Geusic ◽  
Alan F. Stewart ◽  
Larry R. Pederson ◽  
William J. Weber ◽  
Kenneth R. Marken ◽  
...  
Keyword(s):  
Thin Films ◽  
Laser Ablation ◽  
Excimer Laser ◽  
Laser Energy ◽  
Substrate Surface ◽  
Xrd Analysis ◽  
Zero Field ◽  
Superconducting Transition ◽  
X Ray Diffraction ◽  
Excimer Laser Ablation

ABSTRACTExcimer laser ablation with an in situ heat treatment was used to prepare high quality superconducting YBa2Cu3O7−x thin films on (100)-SrTiO3 and (100)-LaAlO3 substrates. A pulsed excimer laser (XeCl; 308 nm) was used to ablate a rotating, bulk YBa2Cu3O7−x target at a laser energy density of 2–3 J/cm2. Based on four-probe dc resistance measurements, the films exhibited superconducting transition temperatures (Tc, midpoint) of 88 and 87K with 2K (90–10%) transition widths for SrTiO3 and LaAlO3, respectively. Transport critical current densities (Jc) measured at 77K were 2 × 106 and 1 × 106 A/cm2 in zero field for SrTiO3 and LaAlO3, respectively. X-ray diffraction (XRD) analysis showed the films to be highly oriented, with the c-axis perpendicular to the substrate surface.

Characterization of Electrical Contacts on Silicon (100) after Ablation and Sulfur Doping by Femtosecond Laser Pulses

2013 ◽  
Vol 205-206 ◽  
pp. 358-363 ◽  
Author(s):  
Philipp Saring ◽  
Anna Lena Baumann ◽  
Stefan Kontermann ◽  
Wolfgang Schade ◽  
Michael Seibt
Keyword(s):  
Surface Roughness ◽  
Femtosecond Laser ◽  
Laser Pulses ◽  
Sample Surface ◽  
Femtosecond Laser Pulses ◽  
Electrical Contacts ◽  
Single Shot ◽  
Excess Charge ◽  
Silicon Sample ◽  
Etching Depth

This paper investigates the influence of different number of laser pulses on contact behavior and conductivity of the surface layer of femtosecond laser microstructured, sulfur-doped silicon. Single shot laser processed silicon (Pink Silicon) is characterized by low surface roughness, whereas five shot laser processed silicon (Grey Silicon) has an elevated sulfur content with a surface roughness low enough to maintain good contacting. To laterally confine the laser induced pn-junction part of the Grey Silicon sample surface is etched off. The etching depth is confirmed to be sufficient to completely remove the active n-type sulfur layer. While Pink Silicon shows little or no lateral conductivity within the laser processed layer, Grey Silicon offers acceptable conductivity, just as expected by the fact of having incorporated a higher sulfur dopant content. Recombination dominates the irradiated regions of Pink Silicon and suppresses excess charge carrier collection. Grey Silicon, while showing sufficient lateral conductivity, still shows regions of lower conductivity, most likely dominated by the laser irradiation-induced formation of dislocations. According to our results, the optimum laser pulse number for electrical and structural properties is expected to be in the range between one and five laser pulses.

scholarly journals Micromachining of Transparent Biocompatible Polymers Applied in Medicine Using Bursts of Femtosecond Laser Pulses

Micromachines ◽  
2020 ◽  
Vol 11 (12) ◽  
pp. 1093
Author(s):  
Evaldas Kažukauskas ◽  
Simas Butkus ◽  
Piotr Tokarski ◽  
Vytautas Jukna ◽  
Martynas Barkauskas ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Femtosecond Laser ◽  
Contact Lenses ◽  
Laser Pulses ◽  
Laser Micromachining ◽  
Femtosecond Laser Pulses ◽  
Intraocular Lenses ◽  
Great Promise ◽  
Biocompatible Polymers ◽  
Mechanical Methods

Biocompatible polymers are used for many different purposes (catheters, artificial heart components, dentistry products, etc.). An important field for biocompatible polymers is the production of vision implants known as intraocular lenses or custom-shape contact lenses. Typically, curved surfaces are manufactured by mechanical means such as milling, turning or lathe cutting. The 2.5 D objects/surfaces can also be manufactured by means of laser micromachining; however, due to the nature of light–matter interaction, it is difficult to produce a surface finish with surface roughness values lower than ~1 µm Ra. Therefore, laser micromachining alone can’t produce the final parts with optical-grade quality. Laser machined surfaces may be polished via mechanical methods; however, the process may take up to several days, which makes the production of implants economically challenging. The aim of this study is the investigation of the polishing capabilities of rough (~1 µm Ra) hydrophilic acrylic surfaces using bursts of femtosecond laser pulses. By changing different laser parameters, it was possible to find a regime where the surface roughness can be minimized to 18 nm Ra, while the polishing of the entire part takes a matter of seconds. The produced surface demonstrates a transparent appearance and the process shows great promise towards commercial fabrication of low surface roughness custom-shape optics.

Surface Modification Induced by Femtosecond Laser Pulses in Lithium Niobate

2011 ◽  
Vol 142 ◽  
pp. 134-137
Author(s):  
Hong Yun Chen ◽  
Zhen Zhu Wan ◽  
Yan Ling Han
Keyword(s):  
Surface Modification ◽  
Lithium Niobate ◽  
Femtosecond Laser ◽  
Laser Energy ◽  
Laser Pulses ◽  
Sample Surface ◽  
Femtosecond Laser Pulses ◽  
Two Dimensional ◽  
Damage Depth ◽  
Transparent Materials

The interaction between femtoseocnd laser and transparent materials has been studied intensively in recent years. When the femtosecond laser was focused onto the surface of the transparent materials, if the laser fluence applied to the sample exceeds the material’s fluence threshold, ablation occurs. In this paper, we study the surface ablation of lithium niobate by femtosecond laser. We produced a two-dimensional array of voids in the sample surface by varying the number of shots and laser energy, and analyze of the damage depth with the relation to the pulse energy and the number of the pulse. It has important reference on the microfabrication in such materials by femtosecond laser.

Light field characteristics of reflective thin-films irradiated by femtosecond laser pulses

Optik ◽  
2012 ◽  
Vol 123 (4) ◽  
pp. 291-294 ◽  
Author(s):  
Zhiwu Zhu ◽  
Xiang’ai Cheng ◽  
Hong Tian ◽  
Jing Bian ◽  
Zejin Liu
Keyword(s):  
Thin Films ◽  
Femtosecond Laser ◽  
Light Field ◽  
Laser Pulses ◽  
Femtosecond Laser Pulses

Pulsed laser deposition and characterization of conductive RuO2 thin films

1997 ◽  
Vol 12 (6) ◽  
pp. 1433-1436 ◽  
Author(s):  
A. Iembo ◽  
F. Fuso ◽  
E. Arimondo ◽  
C. Ciofi ◽  
G. Pennelli ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Electrical Properties ◽  
Pulsed Laser Deposition ◽  
Photoelectron Spectroscopy ◽  
Pulsed Laser ◽  
Surface Characteristics ◽  
Laser Deposition ◽  
X Ray ◽  
Substrate Interface

RuO2 thin films have been produced on silicon-based substrates by in situ pulsed laser deposition for the first time. The electrical properties, the surface characteristics, the crystalline structure, and the film-substrate interface of deposited samples have been investigated by 4-probe resistance versus temperature technique, scanning electron microscopy, x-ray photoelectron spectroscopy, x-ray diffraction, and transmission electron microscopy, respectively. The films show good electrical properties. The RuO2-substrate interface is very thin (≈3 nm), since it is not degraded by any annealing process. These two characteristics render our films suitable to be used as electrodes in PZT-based capacitors.

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