scholarly journals Hygromechanical Performance of Polyamide Specimens Made with Fused Filament Fabrication

Polymers ◽  
2021 ◽  
Vol 13 (15) ◽  
pp. 2401
Author(s):  
Roberto Spina ◽  
Bruno Cavalcante

The material performance of polyamide (PA) samples made with fused filament fabrication (FFF) was analyzed. The authors implemented a well-structured framework to identify the filaments main properties before processing them and characterizing the printed samples. Unfilled and glass-fiber reinforced PA were investigated, focusing on moisture absorption and its effects on dimensional stability and mechanical performance. The properties were collected using differential scanning calorimetry and Fourier-transform infrared spectroscopy, whereas the specimens were characterized by employing compression tests. This framework allowed for the moisture determination, as well as the influence of the moisture absorption. A significant impact was detected for the glass-fiber reinforced PA, with a decrease in the dimensional and mechanical performance. The novelty of this study was to define a well-structured framework for testing the moisture influence of FFF components.

2021 ◽  
pp. 073168442110140
Author(s):  
Hossein Ramezani-Dana ◽  
Moussa Gomina ◽  
Joël Bréard ◽  
Gilles Orange

In this work, we examine the relationships between the microstructure and the mechanical properties of glass fiber–reinforced polyamide 6,6 composite materials ( V f = 54%). These materials made by thermocompression incorporate different grades of high fluidity polyamide-based polymers and two types of quasi-UD glass fiber reinforcement. One is a classic commercial fabric, while the other specially designed and manufactured incorporates weaker tex glass yarns (the spacer) to increase the planar permeability of the preform. The effects of the viscosity of the polymers and their composition on the wettability of the reinforcements were analyzed by scanning electron microscopy observations of the microstructure. The respective influences of the polymers and the spacer on the mechanical performance were determined by uniaxial tensile and compression tests in the directions parallel and transverse to the warp yarns. Not only does the spacer enhance permeability but it also improves physical and mechanical properties: tensile longitudinal Young’s modulus increased from 38.2 GPa to 42.9 GPa (13% growth), tensile strength increased from 618.9 MPa to 697 MPa (3% growth), and decrease in ultimate strain from 1.8% to 1.7% (5% reduction). The correlation of these results with the damage observed post mortem confirms those acquired from analyses of the microstructure of composites and the rheological behaviors of polymers.


2022 ◽  
Vol 7 (1) ◽  
Author(s):  
Tao Jiang ◽  
Xinfeng Wu ◽  
Yuan Gao ◽  
Ying Wang ◽  
Ke Yang ◽  
...  

2020 ◽  
pp. 096739112096510
Author(s):  
Pan Wang ◽  
Qing Lin ◽  
Yaming Wang ◽  
Chuntai Liu ◽  
Changyu Shen

This work aims to perform a systematic investigation on the crystallization behavior and morphologies of carbon and glass fiber reinforced PEEK. The nonisothermal and isothermal crystallization behavior was investigated by differential scanning calorimetry (DSC). The resultant morphologies were assessed by wide angle X-ray diffraction (WAXD), small angle X-ray scattering (SAXS), and polarized optical microscopy (POM) to provide details on spherulitic level, crystalline structure at unit cell, and lamellar levels. It was found that the crystallization ability of carbon fiber filled PEEK was better than that of neat PEEK, while the behavior of glass fiber filled PEEK was in an opposite trend. The incorporation of carbon fiber (or glass fiber) led to a looser packing of the unit cell or a less crystal perfection of PEEK but did not change its crystal form as well as its long period of lamellae. The isothermal crystallization kinetics was analyzed by the Avrami model, suggesting that the crystallization mechanism of carbon fiber filled PEEK was different from that of neat PEEK and its glass fiber filled composites. Nevertheless, the POM results showed that fiber-induced transcrystallization in PEEK matrix was not evidenced for either carbon or glass fiber filled PEEK. Finally, the effect of carbon and glass fiber on the crystallization of PEEK matrix was discussed to some extent.


e-Polymers ◽  
2017 ◽  
Vol 17 (2) ◽  
pp. 159-166 ◽  
Author(s):  
Hyeong Min Yoo ◽  
Dong-Jun Kwon ◽  
Joung-Man Park ◽  
Sang Hyuk Yum ◽  
Woo Il Lee

AbstractA lab scale structural reaction injection molding (S-RIM) piece of equipment was designed and used to fabricate glass fiber reinforced polydicyclopentadiene (p-DCPD) composites for three different fiber contents. In order to obtain information regarding the optimal process temperature (>80°C) and the curing time (<30 s), differential scanning calorimetry (DSC) was used to investigate the curing behavior of DCPD resin under isothermal conditions. Further, a norbornene-based silane treatment was used to improve the interfacial adhesion between the glass fibers and DCPD as confirmed by the micro-droplet pull-out test and scanning electron microscopy (SEM). Fabrication of glass fiber/p-DCPD composites with improved mechanical properties was carried out based on the optimized process conditions and surface treatment of glass fiber.


2013 ◽  
Vol 750-752 ◽  
pp. 176-185
Author(s):  
Yun Hae Kim ◽  
Jun Mu Park ◽  
Jin Woo Lee ◽  
Jae Hyun Jeong ◽  
Kyung Man Moon

Generally, the moisture absorbed in the composites plasticizes the resin. And it makes the composites expansion in volume and generates the cracking at the same time, So, the fracture is often generated in the composites by those reason. Therefore, in this study, the change of mechanical properties due to the moisture-absorption for the carbon fiber reinforced composites in comparison with basalt fiber and glass fiber reinforced composites are investigated. The specimens for the carbon, basalt, and glass fiber reinforced composites manufactured with the ASTM standard. The specimens immersed in distilled water at 80°C during 100 days and the coefficient of moisture was measured in according to the Fick's law. In addition, after drying process, the humidity-absorbed specimen under 80°C for 1 day, the recovery rate was measured. As a result, the coefficient of moisture-absorption of carbon fiber reinforced composite material was the lowest at approximately 3 % because the interface coherence with the fiber and resin are the most strong. Also, after drying process, the recovery rate was 20 percent higher than the others.


2016 ◽  
Vol 51 (16) ◽  
pp. 2301-2313 ◽  
Author(s):  
B Stankiewicz

Modern bridge structures need light decks with long durability and promising technical parameters. Glass fiber-reinforced polymer orthotropic bridge deck creates unconventional possibilities in bridge designing. Parallel identification of glass fiber-reinforced polymer deck panel by differential thermal analysis, spectroscopy analysis, scanning and optical microscope monitoring, dynamic mechanical analysis and differential scanning calorimetry analysis, tensile and flexural tests will be presented in the paper. Differential thermal analysis was carried out for estimation of the physical and chemical transformation of glass fiber. The differential scanning calorimetry experiments were performed in the glass fiber-reinforced polymer–bridge deck material for determining the mass variation and the energy changes suffered by the materials, as a function of temperature and time. Dynamic mechanical analysis was allowed to detect thermal effects based on the changes in the modulus or damping behavior. Tensile and flexural tests allowed the observation of the decomposition process and information about the basic stress parameters of glass fiber-reinforced polymer material used in bridge applications was taken. Aforementioned analyses are necessary to examine the durability description of the composite element.


2015 ◽  
Vol 766-767 ◽  
pp. 193-198 ◽  
Author(s):  
T. Rajmohan ◽  
K. Mohan ◽  
K. Palanikumar

Natural Fiber Reinforced Composite (NFRC) are used by replacing Synthetic Fiber Reinforced Composites (SFRC) because of its poor reusability, recycling, bio degradability. Even though NFRC are lack in thermal stability, strength degradation, water absorption and poor impact properties. The hybridization and nanoparticles mixed in different polymers are used to improve mechanical and wear properties of the polymer composites. In the present investigation Multi wall carbon nanotubes (MWCNT) dispersed in Epoxy resin using ultrasonic bath sonicator are used as matrix face for hybrid banana-Glass Fiber Reinforced Plastics composite materials which is manufactured by compression molding processes. As per ASTM standards tensile, compression tests are carried out by using Universal Testing Machine. Microstructure of samples are investigated by scanning electron microscope (SEM) with Energy dispersive X-ray (EDS). SEM shows the homogeneous distribution of the fiber in the modified polymer matrix. The results indicated that the increase in weight % of MWCNT improves the mechanical properties of MWCNT filled hybrid natural fiber composites.


Sign in / Sign up

Export Citation Format

Share Document