Characterization of Heat-Resistant Geocement Based on Potassium Silica Solution

2013 ◽  
Vol 378 ◽  
pp. 230-234
Author(s):  
Tomáš Kovářík ◽  
Jaroslav Kadlec ◽  
Michal Pola ◽  
Pavel Novotný ◽  
Stanislava Podmanická ◽  
...  

The aim of this paper is detailed description of synthesis geocement composite material based on K2O-Al2O3-SiO2 system and characterization its thermal properties. The series of analytic tools were used (XRF, XRD, SEM, BET, particle-size distribution) for accurate identification of chemical and physical properties of raw material. Optimum technological prescription was determined and geocement specimens were tested for identification of mechanical and thermal properties. Three series of specimens were heated up to 1000, 1100 and 1230°C and flexural strength was determined. The thermal analysis TMA and DMA were used for characterization of heat-resistant properties. The maximum shrinkage in the range 30-1000°C was for the first run in temperature rate 20°C/min. only 3%. The heating exposure at slower rate (3°C/min.) caused reduction of shrinkage up to 1.5% at 1000°C. Geocement represents attractive thermal properties.

2019 ◽  
pp. 089270571987822
Author(s):  
Saud Aldajah ◽  
Mohammad Y Al-Haik ◽  
Waseem Siddique ◽  
Mohammad M Kabir ◽  
Yousef Haik

This study reveals the enhancement of mechanical and thermal properties of maleic anhydride-grafted polypropylene (PP- g-MA) with the addition of nanocrystalline cellulose (NCC). A nanocomposite was manufactured by blending various percentages of PP, MA, and NCC nanoparticles by means of a twin-screw extruder. The influence of varying the percentages of NCC on the mechanical and thermal behavior of the nanocomposite was studied by performing three-point bending, nanoindentation, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), and Fourier-transform infrared (FTIR) spectroscopy tests. The novelty of this study stems on the NCC nanoparticles and their ability to enhance the mechanical and thermal properties of PP. Three-point bending and nanoindentation tests revealed improvement in the mechanical properties in terms of strength, modulus, and hardness of the PP- g-MA nanocomposites as the addition of NCC increased. SEM showed homogeneity between the mixtures which proved the presence of interfacial adhesion between the PP- g-MA incorporated with NCC nanoparticles that was confirmed by the FTIR results. DSC and TGA measurements showed that the thermal stability of the nanocomposites was not compromised due to the addition of the coupling agent and reinforced nanoparticles.


Polymers ◽  
2021 ◽  
Vol 13 (5) ◽  
pp. 754
Author(s):  
Jantrawan Pumchusak ◽  
Nonthawat Thajina ◽  
Watcharakorn Keawsujai ◽  
Pattarakamon Chaiwan

This work aims to explore the effect of organo-modified montmorillonite nanoclay (O-MMT) on the mechanical, thermo-mechanical, and thermal properties of carbon fiber-reinforced phenolic composites (CFRP). CFRP at variable O-MMT contents (from 0 to 2.5 wt%) were prepared. The addition of 1.5 wt% O-MMT was found to give the heat resistant polymer composite optimum properties. Compared to the CFRP, the CFRP with 1.5 wt% O-MMT provided a higher tensile strength of 64 MPa (+20%), higher impact strength of 49 kJ/m2 (+51%), but a little lower bending strength of 162 MPa (−1%). The composite showed a 64% higher storage modulus at 30 °C of 6.4 GPa. It also could reserve its high modulus up to 145 °C. Moreover, it had a higher heat deflection temperature of 152 °C (+1%) and a higher thermal degradation temperature of 630 °C. This composite could maintain its mechanical properties at high temperature and was a good candidate for heat resistant material.


2015 ◽  
Vol 820 ◽  
pp. 497-502 ◽  
Author(s):  
Danubia Lisbôa da Costa ◽  
Rosiane Maria da Costa Farias ◽  
Aluska Nascimento Simões Braga ◽  
Romualdo Rodrigues Menezes ◽  
Gelmires de Araujo Neves

Several years ago the study on modification of existing materials that have enhanced properties has gained prominence. In this scenario, the geopolymeric binders, currently widely used in the construction industry have emerged. Thus, this study aimed to evaluate the influence of alumina addition on the mechanical and thermal properties of metakaolin in geopolymer binder. The geopolymers were synthesized from mixtures of metakaolin/alumina and sodium hydroxide, pressed and characterized by diffraction of X-ray and differential thermal analysis and thermogravimetric. Two types of alumina were used in different amounts (14% and 7%) in order to evaluate the effect of the load binder obtained. It can be seen that the incorporation of alumina into the system caused an increase in strength of products obtained as well as a reduction in total mass loss of the sample , especially when the use of fine alumina.


2014 ◽  
Vol 343 (1) ◽  
pp. 88-95 ◽  
Author(s):  
Reinaldo Yoshio Morita ◽  
Juliana Regina Kloss ◽  
Ronilson Vasconcelos Barbosa

2012 ◽  
Vol 9 (3) ◽  
pp. 450-458
Author(s):  
Baghdad Science Journal

In this study , Iraqi Bentonite clay was used as a filler for polyvinyl chloride polymer. Bentonite clay was prepared as a powder for some certain particle size ,followed by calcinations process at (300,700,900) OC ,then milled and sieved. The selected sizes were D ~75 µm and D ~150. After that polyvinyl Al-Cohool solution prepared and used as a coated layer covered the Bentonite powder before applied as a filler ,followed by drying , milling and sieving for limited recommend sizes. polyvinyl chloride solutions were prepared and adding of modified Bentonite power at certain quantities were followed .Sheet of these variables on the mechanical and thermal properties of the prepared reinforced particular polyvinyl chloride composite Experimentally, it was found that the composite prepared by adding modified Iraqi Bentonite powder , that calcined at 700 oC as a filler have an advantage in heating insulator properties by 30 from that found for PVC as it is ,and the value of stress strength exceed by three times as that for original value.


2016 ◽  
Vol 694 ◽  
pp. 34-38
Author(s):  
Zaleha Mustafa ◽  
Zurina Shamsudin ◽  
Radzali Othman ◽  
Nur Fashiha Sapari ◽  
Jariah Mohd Juoi ◽  
...  

Glass-composite materials were prepared from the soda lime silicate (SLS) waste glass; ball clay and charcoal powder were fired to temperature of 850 °C as an effort for recycling waste glass. Various carbon contents, i.e., 1, 5, 10, 20 and 30 wt.% C were used to evaluate the effect of carbon contents on the hardness and thermal properties of glass composites. In addition, five different particles size (d0.5) of 1, 5, 20, 40 and 75 μm were used to observe the influence of particle size on the physical and mechanical properties of the glass composites. Phase analysis studies revealed the presence of quartz (ICDD: 00001-0649, 2θ = 25.6° and 35.6°), cristobalite (ICDD 00004-0379, 2θ = 22.0° and 38.4°) and wollastonite (ICDD 00002-0689, 2θ = 30.1° and 26.9°). The results showed that the optimised properties is at 1 wt.% of carbon content containing average pore size of 10 μm, with lowest porosity percentage of 1.76 %, highest Vickers microhardness of 4.6 GPa and minimum CTE. The percentage of porosity and hardness value also increased with reduction in carbon particle size.


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