Ammonia Leaching Study on Carbonate Oxidised Copper Ores in Yunnan

2015 ◽  
Vol 723 ◽  
pp. 644-647
Author(s):  
Ke Jun Bi ◽  
Jian Jun Fang ◽  
Tai Guo Jiang ◽  
Guo Dong Li

The effects of oxidized copper ores which came from Yunnan province were carried out by using ammonialeaching methods in the laboratory.In order to seek the optimum leaching conditions under normal temperature and pressure,we conducted a series of validation experiments. Theoptimum conditions were obtained as follows: ammonia concentration 2.5mol/L, ammonium sulfateconcentration 2.5mol/L,grinding fineness about 80% -0.074mm, liquid-solid ratio 2.5:1and leaching time was 2.5h. Under these experimental conditions, the copper leaching rate could reach 69.91%.

2014 ◽  
Vol 563 ◽  
pp. 53-56
Author(s):  
Tie Min Zhang ◽  
Zhi Cong Wei ◽  
Ying Bo Mao

Ammonia leaching research is carried out on a certain oxidised copper ores. The effects of oxidized copper ores which came from Yunnan Province were studied in laboratory in order to find out the optimum leaching conditions under normal temperature and pressure. The ores belonged to typical high binding rate minerals. The optimum conditions obtained were as follows: granding fineness about 90% -0.074mm, ammonia concentration 2 mol/l, ammonium fluoride concentration 1.5mol/l , leaching time 2h, and liquid-solid ratio 3:1.The leaching rate of this ore could reach 86%.


2013 ◽  
Vol 785-786 ◽  
pp. 1076-1080
Author(s):  
Xiao Dong Jia ◽  
Zhi Cong Wei ◽  
Dian Wen Liu ◽  
Jing Jie Yuan

The effects of refractory zinc oxide ore which came from Lanping of Yunnan Province were studied using agitation leach method in laboratory in order to find out the optimum leaching conditions. The optimum conditions obtained are as follows: ammonia concentration 3mol/L, ammonium bicarbonate 1.5mol/L, granularity (-0.074mm) about 85%, solid to liquid ratio 4:1, and leaching time 2h. On this condition, the test obtained the better index of the zinc leaching rate 74.4%.


Author(s):  
Shiwei Li ◽  
Haoyu Li ◽  
Weiheng Chen ◽  
Jinhui Peng ◽  
Aiyuan Ma ◽  
...  

AbstractIrradiated roast treatment and the ammonia leaching processing were conducted to deal with the low-grade oxide zinc ores. The ZnCO3phase was hard to be attended, which was the reason for the low leaching rate of the complicated zinc ores. The mineral phase transformation of the ZnCO3phase was generated after the ores irradiated in the microwave at the temperature of 673 K. The irradiated ores generated more small particles, it was the reason that the leaching rate of the complicated zinc ores was increased. When the leaching processing of the irradiated roasted ores was conducted under the conditions of the total ammonia concentration of 6 mol/L, the liquid to solid phase ratio of 11:1, the leaching temperature of 298 K, the leaching time of 150 min and the stirring speed of 400 rpm, 88.3 % of zinc could be achieved, which was the maximum leaching rate of the irradiated ores.


2013 ◽  
Vol 634-638 ◽  
pp. 3454-3459
Author(s):  
Ya Wen ◽  
Jian Jun Fang ◽  
Ying Bo Mao ◽  
Shan Wang ◽  
Zhi Cong Wei ◽  
...  

The experiments of refractory copper oxide ore which comes from Tangdan of Yunnan Province were studied in laboratory using bulk flotation process and a new process that Ammonia leaching-Extraction-Electrode position-Residue flotation under normal temperature and pressure respectively. The results show that new process, compared with bulk flotation, had an effect to add 10.8 percent points to recovery. And then it is confirmed by industry experiment. So it is successfully applied to industry production and technology indicators were improved dramatically.


2015 ◽  
Vol 1094 ◽  
pp. 415-418
Author(s):  
Fei Wang Wang ◽  
Yi Qi Cui ◽  
Xiong Tong ◽  
Dan Dan Xie

In this research, a fine disseminated gold ore in Yunnan, After four ore exploration tests of chemical pretreatment, get a reasonable oxidation-leaching process that: W-1 (60 kg/t) and M-3 (45 kg/t) used in conjunction with inflated amount of 0.5 m3/h, under the condition of 75°C, stirring pretreated for 24 h, the ore sample after pretreatment was filtered to take a certain amount ,at the condition of normal temperature and pressure, NH4SCN 0.6 mol/L, KMnO4 10 g/L, slurry solid ratio of pulp is 4:1, stirring time is 5 h, pH value is 3. Under these conditions, the gold leaching rate up to 82.26%.


2012 ◽  
Vol 95 (3) ◽  
pp. 845-849 ◽  
Author(s):  
Mohammad Mirzaei ◽  
Atieh Karimi Naeini ◽  
Mansoureh Behzadi

Abstract A simple and sensitive method has been developed for preconcentration and determination of genistein in soybeans. This method is based on cloud point extraction (CPE) of genistein from soybeans using ethylene glycol monoalkyl ether (Genapol X-080) as a nonionic surfactant. The concentration of extracted genistein was determined by HPLC with a UV detector. Optimum experimental conditions were established. With 5% Genapol X-080 (v/v), a liquid/solid ratio of 25:1 mL/g, and ultrasonic-assisted extraction at 40°C for 45 min, the extraction percentage of genistein reached its highest value. The preconcentration factor for genistein was about 16.5. The RSD for seven replicate measurements and the LOD were ±4.45% and 15.0 ng/mL, respectively. CPE is simple, inexpensive, and suitable for extraction of genistein from soybean. It uses environmentally friendly surfactants and offers a convenient alternative to more conventional extraction systems.


2013 ◽  
Vol 734-737 ◽  
pp. 1033-1036
Author(s):  
Gui Fang Zhang ◽  
Peng Yan ◽  
Qing Rong Yang

Based on the benefication of the complex silicate ore containing scandium, the research about aid-leaching agent used in the leaching of the scandium concentrate was been conducted. And the suitable leaching agent and aid-leaching agent which the useful ions entered into leaching liquid and the harmful ions were kept in leaching residue were been found according to the experiment results. For the scandium of sample existed various complex silicate ore as isomorphism form, the research has adopted hydrochloric acid with aid-leaching agent to dissociate the silicate ore and make scandium entering into solution. The research results has shown that the scandium leaching rate could reach 92.06% under the optimal conditions which the hydrochloric acid concentration is 22.8%, the dosage of aid leaching agent is 6%, liquid solid ratio is 4:1, particle size of leaching material totally is less than 0.15mm and leaching time is 8h.


2013 ◽  
Vol 591 ◽  
pp. 122-125
Author(s):  
Li Jiao Yang ◽  
Si Chen ◽  
Yan Zhang ◽  
Nan Chun Chen ◽  
Jun Gao ◽  
...  

Extracting indium from water quenching slag, which contains poor indium, by two process of leaching, the effect of different oxidants and dosages on the leaching rate of indium in water quenching slag were studied. The leaching conditions: temperature 80 °C, leaching time 2 h, the liquid to solid ratio of neutral leaching 8︰1, the liquid to solid ratio of acid leaching 2︰1, initial concentration of sulfuric acid 500 g·L-1, adding different oxidants, the concentration was detected by crystal violet spectrophotometry. Test results showed that the leaching rate of indium was significantly improved by adding hydrogen peroxide and potassium permanganate. Compared with the effect of different oxidants, the effect of potassium permanganate was significantly higher than that of hydrogen peroxide on the leaching rate of indium.


In previous papers the results of investigations into the influence of varying initial pressures up to 15-20 atmospheres on the spontaneous ignition of mixtures with air of butane, iso -butane, pentane, and hexane were described. On the attainment of a critical pressure, which varied both with the hydrocarbon concerned and the composition of its mixture with air, the ignition points were always found to fall sharply from a higher temperature range above 500°C to a lower range at about 300°C. At pressures just exceeding the critical transition pressures ignition occurred at first only within limited temperature ranges which widened and ultimately merged with increasing pressure. The striking relationship between the behaviours of the hydrocarbons referred to under the experimental conditions and their “knocking” propensities in an engine was also indicated. While the data available were inadequate for drawing any final con­clusion as to the character of the phenomena referred to, a tentative hypothesis was advanced that while ignition in the higher temperature range pertains mainly to the thermal decomponents of intermedially formed compounds, ignition in the lower system occurs when temperature and pressure conditions favour the survival and further oxidation of such bodies, particularly aldehydes.


2009 ◽  
Vol 71-73 ◽  
pp. 409-412
Author(s):  
Wen Qing Qin ◽  
Yan Sheng Zhang ◽  
Shi Jie Zhen ◽  
Jun Wang ◽  
Jian Wen Zhang ◽  
...  

The effects of several variables on the column bioleaching of copper sulphide ore have been investigated. The copper ore contained chalcopyrite as the main sulfide minerals and bornite and chalcocite as the minor minerals. The experiment was carried out using bench-scale column leach reactors designed in Key Lab of Biometallurgy of Ministry of Education, which were inoculated with the pure mesophile bacteria (Acidithiobacillus ferrooxidans) and thermophile bacteria (Sulfobacillus), respectively, and the mixed bacteria which contain both iron- and sulfur-oxidizing bacteria. The results show that the mixed cultures were more efficient than the pure cultures alone and the maximum copper recovery 53.64% was achieved using the mixed cultures after 85 days. The leaching rate of chalcopyrite tended to increase with the increased dissolved ferric iron concentration. The effect of particle size on the rate of the copper leaching was also investigated, and it was shown that the copper bioleaching rate decreases as the amount of fines increase, which limits the permeability, thus decreases leaching rate. Jarosite and elemental sulphur formed in the column were characterized by the X-ray and EDS.


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