Recycled Applications of a Single Crystal Superalloy

2011 ◽  
Vol 239-242 ◽  
pp. 1422-1427 ◽  
Author(s):  
Jin Jiang Yu ◽  
Xiao Feng Sun ◽  
Jiang Xin Lou ◽  
Hai Xia Lang ◽  
Heng Rong Guan ◽  
...  

The effects of application of recycled scraps on the composition, microstructure and mechanical properties of SRR99 alloy were studied. The compositions of recycle master alloy are similar to that of the fresh alloy. However, nitrogen content, the size and amount of microporosity increase significantly with the recycle material proportion. Granular, lamellar and strip-like MC particles mainly represent in the interdendritic regions of the revert alloy. With the addition of the recycled material proportion, the amount of the granular ones rapidly drop and the lamellar ones gently enhance. The stress rupture life decline with the addition of the recycled material proportion. The oxide and sulphide inclusions in revert superalloy can be effectively captured and removed by a foam ceramic filter so that the tensile and stress rupture property has been significantly improved.

2016 ◽  
Vol 849 ◽  
pp. 549-556
Author(s):  
Pin Pin Hu ◽  
Qi Dong Gai ◽  
Qing Li ◽  
Xin Tang

The effect of Microcast-X fine grain casting on the microstructure and mechnical property K492M alloy at 760°C of was investigated. The results indicated that Microcast-X fine grain casting decreased grain size and dendrite space of γ′ phase and γ/γ′ eutectic. In addition, the element segregation decreased significantly compared to conventional casting technique. Also, the size and distribution of MC carbide were improved. By Microcast-X fine grain casting, the tensile strength increased from 934MPa of conventional casting alloy to 1089MPa and the elongation increased from 1.9% to 5.7%. In addition, the stress-rupture life increased from 28.8h of conventional casting alloy to 72.5h. And the fracture mechanism for the alloys by Microcast-X fine grain casting is trans-granular fracture toughness.


2016 ◽  
Vol 849 ◽  
pp. 570-579
Author(s):  
Qiang Huang ◽  
Jin Xia Song ◽  
Qing Li ◽  
Wei Peng Ren ◽  
Xin Guang Guan ◽  
...  

The microstructures and mechanical properties of superalloy K465 under different heat treatment, including as as-cast, solution treatment and aging, were investigated. The results showed that γ' precipitates in as-cast condition exhibited two kinds of morphologies of fine regular cuboidal shape at dendritic arm and coarse irregular form in interdendritic region. MC carbides decomposed into M6C carbides partly after 1210°C/4h solution treatment. The high temperature stress-rupture life can be improved obviously with the increasing cooling rate. When cooling rate was lower than 70°C/min, the room temperature tensile elongation increased with cooling rate increasing. When cooling rate was higher than 90°C/min the room temperature tensile elongation decreased with cooling rate increasing. The proper cooling rate of 70oC/min~90oC/min is advantageous for the achievement of excellent comprehensive properties. When aging treatments continued the regularization of γ' resulted in the improvement of stress-rupture life and the reduction of tensile elongation. The mechanical property gap between the solution treatment and aging can be decreased with increasing cooling rate.


2014 ◽  
Vol 788 ◽  
pp. 493-497
Author(s):  
Xiang Hui Li ◽  
Lian Li ◽  
Xin Tang ◽  
Qi Dong Gai

The microstructure, tensile and stress rupture properties of K492Malloy have been investigated in the present study. The results revealed that γ matrix, γ′ phase, carbide and eutectic in the interdendritic region within grain interior and along grain boundary were observed after solidification. After heat treatment, γ' precipitates with two obviously distinct size existed in the dendrite core and interdendritic region, respectively. Meanwhile, the chain-like (W, Mo)6C and Cr23C6carbides precipitated along grain boundary. The investigation of mechanical properties suggested that the tensile strength was initially increased but then decreased with increasing the temperature from 25oC to 760oC. The stress rupture life was 68.2h and 35.8h at 760oC / 655MPa and 870oC / 365MP, respectively. The columnar grain and carbide along grain boundary resulted in intergranular brittle fracture in both test conditions. As a result, the elongation under the conditions of 760oC/655MPa and 870oC/365MP was 1.5% and 1.4%, respectively.


2018 ◽  
Vol 37 (3) ◽  
pp. 271-276
Author(s):  
P. C. Xia ◽  
K. Xie ◽  
H. Z. Cui ◽  
J. J. Yu

AbstractThe effects of heat treatment process on microstructure and properties of a nickel base superalloy are investigated. The size of γ´ phase decreases and the stress rupture life of alloy at 1100 °C/60 MPa drops with the rise of cooling rate. The hardness at room temperature also increases. The size of cuboidal γ´ precipitate and the volume of spherical γ´ precipitate increase with the rise of aging temperature. With higher aging temperature, the alloy exhibits bimodal γ´ phase. A reasonable combination of the size and volume fraction of cuboidal and spherical γ´ phase can obtain better stress rupture property at 1100 °C/60 MPa.


2007 ◽  
Vol 546-549 ◽  
pp. 1443-1446 ◽  
Author(s):  
Zhi Gang Kong ◽  
Lei Ji ◽  
Shu Suo Li ◽  
Ya Fang Han ◽  
Hui Bin Xu

The effect of heat treatment on microstructures and stress rupture property of a Ni3Al base single crystal alloy DDIC6 was studied in the present investigate. The single crystal specimens were produced by screw selection crystal method. The heat treatment for the alloy was 1300°C/10h+1120°C/4h+870°C/32h and 1300°C/10h+870°C/32h.The microstructures were examined by SEM, TEM and X-ray EDS techniques. The stress rupture tests were carried out in air by constant load creep machines under 1100°C/130MPa with the specimens size of φ5×25 mm. The experimental results showed that the as-cast large size γ′ phases entirely dissolved after 1300°C/10h, and secondary fine γ′ phases precipitated by following aging at 1120°C and 870°C for certain periods of time. The stress rupture life under 1100°C/130MPa increased from 20~30hrs for as-cast condition to 60~100hrs for heat treatment condition. The improvement of the creep resistance of the alloy may attribute to the decrement of the elements segregation at dendrite and interdendritic areas, and the proper size and distribution of γ′ phases.


2007 ◽  
Vol 546-549 ◽  
pp. 1467-1470
Author(s):  
Shu Suo Li ◽  
Chun Xiao Zhang ◽  
Yong Wang Kang ◽  
Ya Fang Han

The effect of NiCr-CrAl coating on the microstructure, oxidation and corrosion resistance, as well as mechanical properties of Ni3Al base alloy IC6AE has been studied in the present investigation. NiCr-CrAl coating for alloy IC6AE was prepared by the powder pack cementation method. The oxidation resistance tests were carried out under the condition of 1050°C/100h, while the hot corrosion resistance tests were under 900°C/100h. The tensile tests at the room temperature and the stress rupture life tests under 1050°C/90Mpa have been also conducted. The experimental results showed that NiCr-CrAl as-coated specimens had excellent oxidation and hot corrosion resistance compared with the alloy IC6AE blank specimens, and NiCr-CrAl coating has no obvious effect on the mechanical properties of alloy IC6AE. It may be concluded that NiCr-CrAl coating is suitable for the alloy IC6AE.


2017 ◽  
Vol 898 ◽  
pp. 401-406
Author(s):  
Qun Gong He ◽  
Jun Liu ◽  
Lin Xu Li ◽  
Zhen Huan Gao ◽  
Xiao Yan Shi ◽  
...  

The microstructures and mechanical properties of IN738LC superalloy made by investment castings followed by Hot Isostatic Pressing (HIP) treatment have been investigated. The results revealed that after HIP treatment, the microporosities have been almost removed and the density rose by 0.21%. The eutectic size became smaller and the fraction decreased. The γ' phase was more regular and also increased in size, while a large number of secondary γ' phase appeared. With HIP treatment, the impact toughness increased from 5.0J ~ 7.0J to 8J ~ 9J and tensile strength at 200°C ~ 800°C was improved by approximately 3.2%~19.7%. In addition, the ductility and the stress rupture life have also been greatly improved as well.


2016 ◽  
Vol 849 ◽  
pp. 520-525
Author(s):  
Zhen Rui Li ◽  
Ning An

This study aims to explore the influence of morphology and distribution characteristic of carbides on stress rupture property at high temperature. The stress rupture life at 850°C/325MPa was tested. Meanwhile, microstructure and fracture morphology of stress rupture specimens were observed by scanning electron microscopy. The types of carbides were identified and the carbide size was also measured. The results show that the alloys with small size, uniformly distribution and moderate number of carbides present a high stress rupture performance.


2017 ◽  
Vol 898 ◽  
pp. 498-504
Author(s):  
Hui Fen Li ◽  
Li Jun Liu ◽  
Ming Xue ◽  
La Mei Cao

The microstructure of a third generation single crystal superalloy DD10 with 0°~15° grain boundary and stress rupture property at 980°C/280MPa and 1100°C/140MPa have been studied and compared in the present investigation. The results showed that the primary dendritic stems at either side of low angle boundary indicated angular differences as compared with structure of principal [001] crystal. After thermal treatment, the grain boundary changed from irregular chain structure of γ’ and γ to flat and thin γ layer. Under the condition of 980°C/280MPaand 1100°C/140MPa, stress rupture life of the DD10 alloy with 7° low angle boundary decreased little compared with [001] crystal. The rupture was non-intergranular fracture. The 9° low angle boundary did not have a remarkable effect on stress rupture property of the DD10 alloy.


2010 ◽  
Vol 650 ◽  
pp. 205-209 ◽  
Author(s):  
Ming Li ◽  
Jin Xia Song ◽  
Shu Suo Li ◽  
Ya Fang Han

The effect of long-term aging at 1070°C on microstructure and mechanical properties of Ni3Al-base equiaxed superalloy IC6E was investigated. The microstructure change during aging for periods of 100 to 1500h was examined by SEM . Results showed that alloy IC6E underwent following microstructure changes during aging: γ' phases coalesced and grew, γ phases became disconnected and coarsened, the content of Mo (the solution-hardening element of γ and γ' phases) in γ' phases decreased, Y-NiMo phases precipitated from γ phases both at grain boundaries and within grains, and γ' bands and large γ phases emerged along grain boundaries. The tensile and stress rupture properties after aging were determined. The results showed that the yield strength of alloy IC6E at room temperature decreased obviously after aging for 100 h, and reduced slowly during further aging. The stress rupture life under 1070°C, 80MPa also had no essential change during aging.


Sign in / Sign up

Export Citation Format

Share Document