Optical Properties of CulnSi Nanocomposite Thin Film Deposited by Magnetron Co-Sputtering

2011 ◽  
Vol 403-408 ◽  
pp. 1089-1093
Author(s):  
Jian Sheng Xie ◽  
Jin Hua Li ◽  
Luan Ping

Thin CuInSi nanocomposite films were prepared by magnetron co-sputtering. The structures of CuInSi nanocomposite films were detected by X-ray diffraction(XRD); XRD studies of the annealed films indicate the presence of CuInSi, the main crystal phase peak is at 2θ=42.400°. The transmittance (T) spectra of the films were measured by Shimadzu UV-2450 double beam spectrophotometer. The band gap has been estimated from the optical absorption studies and found to be about 1.40 eV, but changes with purity of CuInSi.

2011 ◽  
Vol 110-116 ◽  
pp. 3289-3292
Author(s):  
Jian Sheng Xie ◽  
Jin Hua Li ◽  
Ping Luan

Thin CuInSi nanocomposite films were prepared by magnetron co-sputtering. The structures of CuInSi nanocomposite films were detected by X-ray diffraction (XRD); XRD studies of the annealed films indicate the presence of CuInSi, a peak at about 2θ=42.400°. The morphology of the film surface was studied by SEM. The nanocrystallization with needle shape of CuInSi could be seen clearly. The grain size is a few hundred angstroms.


2013 ◽  
Vol 313-314 ◽  
pp. 254-257
Author(s):  
Ling Fang Jin ◽  
Hong Zhuang

Nonepitaxially grown FePt (x)/FePt:C thin films were synthesized, where FePt (x) (x=2, 5, 8, 11, 14 nm) layers were served as underlayers and FePt:C layer was nanocomposite with thickness of 5 nm. The effect of FePt underlayer on the ordering, orientation and magnetic properties of FePt:C thin films has been investigated by adjusting FePt underlayer thicknesses from 2 nm to 14 nm. X-ray diffraction (XRD), together with transmission electron microscopy (TEM) confirmed that the desired L10 phase was formed and films were (001) textured with FePt underlayer thickness decreased less 5 nm. For 5 nm FePt:C nanocomposite thin film with 2 nm FePt underlayer, the coercivity was 8.2 KOe and the correlation length of FePt:C nanocomposite film was 67 nm. These results reveal that the better orientation and magnetic properties for FePt:C nanocomposite films can be tuned by decreasing FePt underlayer thickness.


2011 ◽  
Vol 403-408 ◽  
pp. 1094-1098
Author(s):  
Jian Sheng Xie ◽  
Ping Luan ◽  
Jin Hua Li

Thin Nano-CuInSi films have been prepared by multilayer synthesized method using magnetron sputtering technology, and followed by annealing in N2 atmosphere at different temperatures. The structures of CuInSi films were detected by X-ray diffraction(XRD); X-ray diffraction studies of the annealed films indicate the presence of CuInSi, the peak of main crystal phase is at 2θ=42.450°; the morphology of the film surface was studied by SEM. The SEM images show that the crystalline of the film prepared by multilayer synthesized method was granulated. The transmittance (T) spectra of the films were measured by Shimadzu UV-2450 double beam spectrophotometer. The calculated absorption coefficient is larger than 105 cm−1 when the wavelength is shorter than 750 nm. The band gap has been estimated from the optical absorption studies and found to be about 1.47 eV, but changes with purity of CuInSi. CuInSi thin film is a potential absorber layer material applied in solar cells and photoelectric automatic control.


2012 ◽  
Vol 433-440 ◽  
pp. 302-305
Author(s):  
Jian Sheng Xie ◽  
Jin Hua Li ◽  
Ping Luan

Thin CuInSi films have been prepared by magnetron co-sputtering, and followed by annealing in N2 atmosphere at different temperatures. The structures of CuInSi films were detected by X-ray diffraction(XRD); X-ray diffraction studies of the annealed films indicate the presence of CuInSi, In2O3 and other peaks. The morphology of the film surface was studied by SEM. The band gap has been estimated from the optical absorption studies and found to be about 1.40 eV, but changes with purity of CuInSi. CuInSi thin film is a potential absorber layer material applied in solar cells and photoelectric automatic control.


2014 ◽  
Vol 989-994 ◽  
pp. 656-659
Author(s):  
Ping Cao ◽  
Yue Bai

Al co-doped ZnCoO thin film has been prepared by a sol-gel method. The structural and optical properties of the sample were investigated. X-ray diffraction and UV absorption spectroscopy analyses indicate that Al3+ and Co2+ substitute for Zn2+ without changing the wurtzite structure. With the Al doping, the visible emission increased and the UV emission decreased, which is attributed to the increase of O vacancies and Zn interstitials.


2021 ◽  
Author(s):  
aimane guedri ◽  
Mourad ZAABAT ◽  
Boubekeur BOUDINE ◽  
Abdelkader HAFDALLAH

Abstract Considered Technique spin coating of the most important techniques used to prepare thin films because it is easy to use and inexpensive since it is closely dependent on the number of layers deposited. This work aims to study the effect of samples thickness for nanocomposites of polyvinyl chloride doped with zinc oxide nanoparticles on the structural, optical properties, and photocatalytic activities. Nanocomposite films of polyvinyl chloride (PVC) - zinc oxide (ZnO) with a different number of the deposited layers (15, 20, 25, and 30 layers) were synthesized by a sol-gel method (spin coating) using tetrahydrofuran as a solvent, and investigated by various techniques. X-ray diffraction measurements indicated in the case of 15, 20, and 25 layers do not clearly show the presence of diffraction peaks. On the other hand, in the case of 30 layers, the presence of several peaks is observed, which testify to the presence of ZnO crystallites of wurtzite structure in PVC films. The size of the crystallites is almost equal to 32 nm depending on the working conditions. Raman and infrared spectra confirmed the result of X-ray diffraction on the incorporation of ZnO crystallites in the films produced by showing peaks corresponding to the modes of vibration of the crystal lattice of the ZnO doping semiconductor. Optical transmittance spectra have shown that The layers obtained have an optical transmission varying from 75 to 86% in the visible region of the spectrum. The values of the band gap energies, determined from the transmission spectra for the films deposited on glass, vary between 3.45 and 3.94 eV. The Photoluminescence spectra of ZnO/PVC nanocomposites studied revealed a strong ultraviolet and green luminescence, attributed to structural defects in the zinc oxide. The photocatalytic reaction has been shown using MB in the UV irradiation action of films stacked in an MB solution. The result showed that the 30-layer (PVC / ZnO) sample gave an efficiency to remove MB of 79% at 60 min, Similar to other samples which gave a lower efficiency.


2015 ◽  
Vol 727-728 ◽  
pp. 280-283
Author(s):  
Ping Cao ◽  
Yue Bai ◽  
Zhi Qu

Al doped ZnO thin film have been prepared by a sol-gel method. The structural, and optical properties of the sample were investigated. X-ray diffraction and X-ray absorption spectroscopy analyses and UV absorption spectroscopy analyses indicate that Al3+ substitute for Zn2+ without changing the wurtzite structure. With the Al doping, the visible emission increased and the UV emission decreased, which is attributed to the increase of O vacancies and Zn interstitials.


2009 ◽  
Vol 152-153 ◽  
pp. 253-256 ◽  
Author(s):  
Elena E. Shalygina ◽  
G.V. Maximova ◽  
M.A. Komarova ◽  
A.N. Shalygin ◽  
L.V. Kozlovskii

Results on the investigation of magnetic and magneto-optical properties of nanocrystalline Fe/Zr and Fe/Zr, Mo/Fe thin-film systems are presented. The examined samples were prepared by DC magnetron sputtering technique. The structural investigations of the samples were performed by X-ray diffraction analysis. The hysteresis loops and spectral dependencies of the transverse Kerr effect were measured employing the magneto-optical magnetometer and the magneto-optical spectrometer, respectively. The influence of the Zr and Mo layer thickness on the magnetic and magneto-optical properties of the examined samples was observed.


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