Effect of VC Content on Microstructure and Mechanical Properties of VC/Fe-Based Composites

2012 ◽  
Vol 583 ◽  
pp. 219-222
Author(s):  
Rui Feng Wang ◽  
Zhi Ping Sun ◽  
Guo Jun Zhang ◽  
Li Yan Zou

VC/Fe-based composite samples were fabricated with different volume fraction of VC in vacuum, and the content are 40%, 55%, and 70% respectively. The relationship between microstructure and mechanical properties for VC/Fe based composite with various VC content were studied. The results indicated VC content had a significant effect on the performance and organization of the VC/Fe-based composites and the effect of VC content on the mechanical properties are varied. With ratio of VC powders increased, the volume fraction of V8C7 particles formed additionally, while the fraction of Fe particles slightly decreased. The flexural strength, fracture toughness, relative density and wear resistant increased with increase of VC content in the range of 0 to 55vol. %, and then decreased with further increase of VC content, while the Vickers hardness increased with the increase of VC content. By comparing the material with 55vol.%VC would show the best combination of properties in the prepared samples.

2012 ◽  
Vol 583 ◽  
pp. 215-218
Author(s):  
Rui Feng Wang ◽  
Zhi Ping Sun ◽  
Li Yan Zou ◽  
Guo Jun Zhang

Ti(C,N)/Fe composites samples were fabricated in vacuum and Ti(C,N) content was respectively 20vol.%, 30vol.% and 40vol.%. The relationship of microstructure and mechanical properties for Ti(C,N)/Fe composites with various Ti(C,N) content were studied. The results indicated that the flexural strength and wear resistant increased with increasing the content of Ti(C,N)in the range of 0 to 30vol.%, then decreased with further increase of Ti(C,N) content, and the fracture toughness decreases with increasing Ti(C,N) content integrally, while the Vickers hardness increased with the increase of Ti(C,N) content. The microstructure of Ti(C,N)/Fe composites is uniform, fine grains, and grains combine more closely with Ti(C,N) 30vol.%. By comparing the properties of the material was relatively good with Ti(C,N) 30vol.% at 1300°C.


2010 ◽  
Vol 105-106 ◽  
pp. 27-30 ◽  
Author(s):  
Wei Ru Zhang ◽  
Feng Sun ◽  
Ting Yan Tian ◽  
Xiang Hong Teng ◽  
Min Chao Ru ◽  
...  

Silicon nitride ceramics were prepared by gas pressure sintering (GPS) with different sintering additives, including La2O3, Sm2O3 and Al2O3. Effect of sintering additives on the phase-transformation, microstructure and mechanical properties of porous silicon nitride ceramics was investigated. The results show that the reaction of sintering additives each other and with SiO2 had key effects on the phase-transformation, grain growing and grain boundaries. With 9MPa N2 atmosphere pressure, holding 1h at 1850°C, adding 10wt% one of the La2O3, Sm2O3, Al2O3, porous silicon nitride was prepared and the relative density was 78%, 72%, 85% respectively. The flexural strength was less than 500MPa, and the fracture toughness was less than 4.8MPam1/2. Dropping compounds sintering additives, such as La2O3+Al2O3, Sm2O3+Al2O3 effectively improves the sintering and mechanical properties. The relative density was 99.2% and 98.7% with 10wt% compounds sintering additives. The grain ratio of length to diameter was up to 1:8. The flexural strength was more than 900MPa, and the fracture toughness was more than 8.9MPam1/2.


2008 ◽  
Vol 368-372 ◽  
pp. 1764-1766 ◽  
Author(s):  
Yu Jin Wang ◽  
Lei Chen ◽  
Tai Quan Zhang ◽  
Yu Zhou

The ZrC-W composites with iron as sintering additive were fabricated by hot-press sintering. The densification, microstructure and mechanical properties of the composites were investigated. The incorporation of Fe beneficially promotes the densification of ZrC-W composites. The relative density of the composite sintered at 1900°C can attain 95.3%. W2C phase is also found in the ZrC-W composite sintered at 1700°C. The content of W2C decreases with the increase of sintering temperature. However, W2C phase is not identified in the composite sintered at 1900°C. The flexural strength and fracture toughness of the composites are strongly dependent on sintering temperature. The flexural strength and fracture toughness of ZrC-W composite sintered at optimized temperature of 1800°C are 438 MPa and 3.99 MPa·m1/2, respectively.


2012 ◽  
Vol 723 ◽  
pp. 233-237 ◽  
Author(s):  
Tong Chun Yang ◽  
Chuan Zhen Huang ◽  
Han Lian Liu ◽  
Bin Zou ◽  
Hong Tao Zhu ◽  
...  

TiB2-(W,Ti)C composites with (Ni,Mo) as sintering additive have been fabricated by hot-pressing technique, and the microstructure and mechanical properties of the composites have been investigated. (Ni,Mo) promotes grain growth of the composites. In the case of 7vol.% (Ni,Mo), the grain size decreases consistently with an increase in the content of (W,Ti)C. When the proper content of (W,Ti)C is added to TiB2 composites, the growth of matrix grains is inhibited and the mechanical properties of the composites are improved. The best mechanical properties of the composites are 1084.13MPa for three-point flexural strength, 7.80MPa•m 1/2 for fracture toughness and 17.92GPa for Vickers hardness.


2012 ◽  
Vol 723 ◽  
pp. 353-357
Author(s):  
Guo Jun Zhang ◽  
Zhi Ping Sun ◽  
Li Yan Zou

The microstructure and mechanical properties of samples were examined, and the relationship of structure and mechanical properties for VC/Fe composite sintered at different holding time were studied. Holding time can influence the mechanical properties, with the holding time rising, when the holding time is 80 min, the hardness is Max, it’s 10.71 GPa, the enhancing range is 37.66%; The relative density changes slower from 60 to 100 min; when the holding time is 60 minutes, fracture toughness and bending strength of material is 16.17 MPa•m 1/2 and 1070 MPa, it’s better than before.


2001 ◽  
Vol 702 ◽  
Author(s):  
L.M. Peng ◽  
K. Noda ◽  
H. Kawamoto

ABSTRACTThe present study aimed to investigate the microstructure and mechanical properties of aluminum matrix composites reinforced with high volume fraction of Si3N4 fabricated by the pressure casting technique, with variations in the composition of matrix alloy and microstructure of preforms. Characterization was carried out by a combination of metallography, flexural and load-controlled fatigue tests to study the flexural strength, fracture toughness and fatigue behavior in the composites. The findings indicated that increasing matrix strength resulted in an increase in flexural strength and fatigue resistance of composites. The fracture toughness of composites increased with the volume fraction of infiltrated tough Al phase. The CIP pressure exerted a significant effect on mechanical properties of composites. The improvement in mechanical properties of composites is associated with the load transfer effect from matrix to the stiffer reinforcement.


2002 ◽  
Vol 11 (6) ◽  
pp. 096369350201100 ◽  
Author(s):  
I. J. Davies ◽  
G. Pezzotti ◽  
A. Bellosi ◽  
D. Sciti ◽  
S. Guicciardi

The microstructure and mechanical properties of hot-pressed alumina (Al2O3) matrix composites containing 20, 35, or 50 vol% of nickel aluminide (NiAl) were investigated. The mean Al2O3 grain size was found to decrease from approximately 2.0 μm (monolithic Al2O3) to 1.0 μm for the composite containing 50 vol% NiAl. Composite flexural strength values were lower than both the monolithic Al2O3 and NiAl and attributed to the weakly bonded NiAl particles acting as flaw origins. In contrast to this, the fracture toughness increased with NiAl volume fraction to a maximum of 4.90 MPa·m1/2, thus confirming the toughening effect of NiAl addition on Al2O3 ceramics, with the slope of the rising R-curve for the composite being approximately 8 times that of monolithic Al2O3.


2012 ◽  
Vol 724 ◽  
pp. 278-281 ◽  
Author(s):  
Lan Ye ◽  
Jian Feng Zhu

The Ti3AlC2/Al2O3 in situ composites were successfully synthesized from the system of Ti-TiC-Al-TiO2 by reactive hot pressing at 1350 °C. The effect of TiC content on the phase composition, microstructure and mechanical properties were investigated in detail. The results indicate that the fabricated products possess the highest purity as the TiC contents reduce to 90 % of its theoretical content. This deviation is mainly attributed to the decomposition of Ti3AlC2 and vaporization of Al at high temperatures. The effect of TiC content on the fracture toughness, flexural strength, Vickers hardness of Ti3AlC2/Al2O3 composites was also discussed in detail.


2021 ◽  
Vol 1 (4) ◽  
pp. 216-222
Author(s):  
Sheida Haji Amiri ◽  
Nasser Pourmohammadie Vafa

The Ti3SiC2 used in this project has been purchased ready-made. This study aimed to investigate the effect of sintering temperature on samples' microstructure and mechanical properties, including three-point flexural strength, Vickers hardness, and fracture toughness. Therefore, Ti3SiC2 samples were sintered under a vacuum atmosphere at a pressure of 35 MPa for 30 minutes at two temperatures of 1500 °C and 1550 °C by hot pressing. The microstructure obtained from the fracture cross-section of the samples shows that by increasing the sintering temperature to 1550 °C, the microstructure of this sample becomes larger than the sintered sample at 1500 °C. Also, increasing the sintering temperature to 1550 °C causes the decomposition of Ti3SiC2 to TiC, which can be seen in the X-ray diffraction pattern (XRD). In addition, the relative density of the sintered sample at 1550 °C is 98.08% which is higher than that of the sintered sample at 1500 °C with the result of 89%. On the other hand, the three-point flexural strength (227.5 MPa), the Vickers hardness (~9 GPa), and the fracture toughness (8.6 MPa.m1/2) of the sintered sample at 1500 °C are higher due to the fine-grained structure.


2014 ◽  
Vol 788 ◽  
pp. 580-587
Author(s):  
Yuan Lu ◽  
Jing Long Li ◽  
Jian Feng Yang ◽  
Qiang Zheng Jing ◽  
Jing Jing Li ◽  
...  

The co-continuous AlN composites with different Al contents were fabricated through the squeeze casting of porous AlN preform with varied porosities obtained by carbothermal reduction. The effects of volume fraction of Al phase and the heat treatment temperature on the mechanical properties of composites were investigated. The change of the mechanical properties of composites with the Al content was in line with the mixed rule. With an increase in the Al content, the fracture toughness increased, the Vickers hardness and the flexural strength decreased. The toughen mechanism of composites included ductile rupture and microcrack toughening. The avoiding of excessive interface reaction between AlN and Al was beneficial to the mechanical properties of composites. With an increase in the heat treatment temperature, the stress and the dislocation due to mismatch in the coefficients of thermal expansion increased, the fracture toughness decreased, the vickers hardness and the flexural strength increased.


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