High-Temperature Ultrasonic Fatigue Testing at 1000°C

2014 ◽  
Vol 891-892 ◽  
pp. 1413-1418
Author(s):  
Yoshiyuki Furuya ◽  
Kazuo Kobayashi ◽  
Masao Hayakawa ◽  
Masao Sakamoto ◽  
Yutaka Koizumi ◽  
...  

A high-temperature ultrasonic fatigue testing system was developed to evaluate the gigacycle fatigue properties of single-crystal superalloys used in aircraft engine turbine blades. In this development, a commercial ultrasonic fatigue testing machine was considerably modified to achieve high-temperature fatigue testing. The developed system took account of temperature dependency of Youngs modulus, and also had a function to evaluate the Youngs modulus. In order to protect the testing system from the heat of a specimen, straight and round rods were inserted between the testing system and the specimen. Other modifications achieved accurate control of temperature, edge displacement and resonance frequency, which were necessary for accurate control of stress amplitude. The testing system was first applied to a heat-resistant steel at 650 °C to check its accuracy, and next to SC superalloy samples at 1000 °C. In the conventional fatigue tests on the heat-resistant steel, the results were coincident in a frequency range from 1 Hz to 800 Hz, suggesting that comparable results would be obtained in ultrasonic fatigue testing at 20 kHz. In case of the SC superalloy samples, conventional fatigue tests were conducted at only 10 Hz, so the frequency effects were not clarified. In both cases, ultrasonic fatigue testing showed good agreement with conventional fatigue testing. The accuracy of the developed system is therefore high, even at 1000 °C. In these results, the SC superalloys showed no fatigue limit, indicating gigacycle fatigue tests to be necessary.

2019 ◽  
Vol 33 (14n15) ◽  
pp. 1940034
Author(s):  
Il Heon Jeong ◽  
Yeong Min Park ◽  
Mun Ki Bae ◽  
Chi Hwan Kim ◽  
Tae Gyu Kim

The purpose of this study is to examine the low-cycle fatigue (LCF) characteristics of high-chrome heat-resistant steel, which is used in a high-temperature environment, at both ambient and high temperature. High-chrome heat-resistant steel, which is used for the turbine blades of a nuclear power plant, can be subject to plastic deformation due to overloading conditions at startup and shutdown. It is therefore very important to evaluate the damage caused by LCF, which is considered as fatigue damage due to plastic deformation. To examine the mechanical properties of high-chrome heat-resistant steel, the tensile strength was tested under different heat treatment conditions. In addition, the LCF characteristics were tested at ambient temperature and [Formula: see text].


2016 ◽  
Vol 17 ◽  
pp. 14-30 ◽  
Author(s):  
Okechukwu P. Nwachukwu ◽  
Alexander V. Gridasov ◽  
Ekaterina A. Gridasova

This review looks into the state of gigacycle fatigue behavior of some structural materials used in engineering works. Particular attention is given to the use of ultrasonic fatigue testing machine (USF-2000) due to its important role in conducting gigacycle fatigue tests. Gigacycle fatigue behavior of most materials used for very long life engineering applications is reviewed.Gigacycle fatigue behavior of magnesium alloys, aluminum alloys, titanium alloys, spheroid graphite cast iron, steels and nickel alloys are reviewed together with the examination of the most common material defects that initiate gigacycle fatigue failures in these materials. In addition, the stage-by-stage fatigue crack developments in the gigacycle regime are reviewed. This review is concluded by suggesting the directions for future works in gigacycle fatigue.


2019 ◽  
Vol 814 ◽  
pp. 157-162
Author(s):  
You Yang ◽  
Xiao Dong Wang ◽  
Wei Feng Tang

The high temperature creep test of heat-resisting steel 30Cr25Ni20 for automobile exhaust manifolds was carried out, and the creep strain-time curves at 650°C and 700°C in the different loads were obtained. The effects of different creep temperature and stress on creep life of materials were studied. The microstructure of the fracture after creep was observed by scanning electron microscopy. Microstructures before and after creep at different temperatures were compared by optical microscopy. The results show that the creep fracture life of heat-resistant steel decreases with the increase of stress at the same temperature. The creep fracture life decreases with the increase of temperature at the same stress, too. The fracture of heat-resistant steel shows good high temperature plasticity and a ductile fracture after creep. The fracture dimples become deeper with the increase of stress. At 650°Cand 700°C, the stress exponent is 8.6 and 6, respectively. When the sample was subjected to high temperature creep at 700°C, the precipitates increase obviously and the reticular structure became very large. At this point, the internal structure of the material is destroyed, and the matrix structure becomes unevenly distributed. The failure of the internal structure leads to the dramatic increase of the creep strain, and the failure of the internal structure will be more serious with the deformation of the sample.


2020 ◽  
Vol 861 ◽  
pp. 83-88
Author(s):  
You Yang ◽  
Xiao Dong Wang

High temperature oxidation dynamic behaviors and mechanisms for 30Cr25Ni20Si heat-resistant steel were investigated at 800, 900 and 1000°C. The oxide layers were characterized by scanning electron microscopy (SEM-EDS), X-ray diffractometer (XRD). The results showed that the oxidation rate of test alloys is increased with increasing the oxidation time. The oxidation dynamic curves at 800 and 900°C follow from liner to parabolic oxidation law. The transition point is 10 h. At 1000°C, the steel exhibits a catastrophic oxidation, and the oxidation mass gain value at 50 h is 0.77 mg/cm2. This suggests that the steel at 900°C has formed a dense protective surface oxidation film, effectively preventing the diffusion of the oxygen atoms and other corrosive gas into the alloy. Therefore, at the first stage of oxidation, chemical adsorption and reaction determine the oxide film composition and formation process. At the oxide film growth stage, oxidation is controlled by migration of ions or electrons across the oxide film. When the spinel scale forms, it acts as a compact barrier for O element and improving the oxidation resistance.


2019 ◽  
Vol 25 (4) ◽  
pp. 394-400
Author(s):  
Hong LI ◽  
Chengzhi ZHAO ◽  
Tao YAN ◽  
Chao DING ◽  
Hexin ZHANG ◽  
...  

The research is focused on a novel aluminum and copper-containing heat-resistant steel. The steel was designed by the material performance simulation software JmatPro, performed high-temperature oxidation tests at 650 °C and 700 °C atmospheric conditions, and analyzed the high-temperature oxidation processes and its mechanisms.The phase transtions and surface morphology of the oxide films were studied using X-ray diffraction (XRD), electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). The results showed that the equilibrium phase of the test steel is composed of γ phase and δ phase at 1050 °C and tranforms to tempered martensite and δ-Fe mixed structure after heat treatment. The preferential oxidation of Fe and Cr and the internal oxidation of Al occurred during the high temperature oxidation of the test steel. The oxide films were formed with various shape and weak bonding properties after high-temperature oxidation at 650℃. To the contrary, the oxide films more regular and evenly distributed, and has a certain protective effect after high-temperature oxidation at 700 ℃. The oxide films were divided into two layers, Fe2O3 is main element in the outer layer, the inner layer is mainly consisting the oxide of Cr. However, the addition of Cu element can promote the diffusion of Al and Si elements, which is beneficial to the formation of Al2O3 and SiO2 protective oxide films and excellent in high temperature oxidation resistance.


2015 ◽  
Vol 664 ◽  
pp. 246-254 ◽  
Author(s):  
Tilmann Beck ◽  
Stephan A. Kovacs ◽  
Fabian Ritz

Low-pressure steam turbine blades undergo VHCF-loadings induced by inhomogenous flow behind the vanes resulting in excitation frequencies of ≈ 2 kHz for rotational speeds of 50 Hz and a typical number of stator vanes of ≈ 60. The VHCF loading is superimposed by considerable mean stresses caused by centrifugal forces. In the present study, the VHCF-behavior of the ferritic-martensitic turbine blade steel X10CrNiMoV12-2-2 is investigated using an ultrasonic fatigue testing system up to cycle numbers of 5∙109 at stress ratios from R = -1 up to 0.7, i.e. up to very high mean stresses. Generally, crack initiation changes from the surface to internal inclusions at fatigue lives around 4∙107. The transition between fatigue failure and run-outs is shifted to higher lifetime with increasing R, and fine grained areas (FGAs) at the crack initiation sites only occur at R < -0.1. However, the fracture mechanics approach proposed by Murakami consistently describes the lifetime behavior for all load ratios over 4 decades of lifetime. At R up from 0.5 considerable cyclic creep occurs, even for lifetimes above 108 cycles, resulting in cyclic hardening which was proved by microhardness measurements at longitudinal sections. This effect at least partially explains the high maximum stresses close to the tensile strength of the material occurring in the VHCF regime at load ratios ≥ 0.5.


2018 ◽  
Vol 37 (6) ◽  
pp. 539-544
Author(s):  
Chengzhi Zhao ◽  
Ning Li ◽  
Yihan Zhao ◽  
Hexin Zhang

AbstractA new kind of martensitic ZG1Cr10MoWVNbN heat-resistant steel has been attracted more attentions in recent years, which is mainly applied in ultra-supercritical steam turbines. The ageing property for ZG1Cr10MoWVNbN heat-resistant steel is very important because it often serves for long-time at high-temperature environment. Herein, a long-term ageing heat treatment was conducted on ZG1Cr10MoWVNbN steel at 600 °C heat for 17,000 hours. The microstructure evolution and property variation of the ZG1Cr10MoWVNbN steel were analysed before and after ageing, and also the effect of the precipitates on the mechanical properties was studied. The result showed that strength, the plastic index and impact power of the ZG1Cr10MoWVNbN steel were gradually decreased after long-term and high-temperature ageing at 600 °C due to the changes of martensite morphology and the coarsening of M23C6 carbide precipitation phase. Furthermore, fine precipitation of matrix MX carbide can also attribute to the change of mechanical properties at high temperature.


2012 ◽  
Vol 78 (789) ◽  
pp. 718-727 ◽  
Author(s):  
Yoshiyuki FURUYA ◽  
Kazuo KOBAYASHI ◽  
Masao HAYAKAWA ◽  
Masao SAKAMOTO ◽  
Yutaka KOIZUMI ◽  
...  

2011 ◽  
Vol 217-218 ◽  
pp. 958-963
Author(s):  
Xue Qin Jin ◽  
Da Sen Bi ◽  
Jian Zhang ◽  
Xiao Lan Wang ◽  
Jian Hua Song ◽  
...  

In power station big caliber thick wall seamless tube typical steel P91for example, The hot deformation behavior and heat flow stress-strain curve of the heat resistant steel P91was investigated with a compression test on Gleeble3500 simulator at a temperature range of 1050°C~1200°C and strain rate range of 10-4~5s-1. The test curve shows that P91 materials have the dynamic recrystallization and recovery behavior in high temperature and deformation. With the rise of temperature and strain rate of decreased, flow stress is lower and the dynamic recrystallization phenomenon is easier to occur. By metalloscope observed, in the high temperature and low strain rate conditions, the dynamic recrystallization area and new nucleation grain size are larger, and microstructure is more uniformly distributed.


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