Smoothing of GaN Substrate by Ultraviolet Assisted Polishing in KOH Solution

2015 ◽  
Vol 656-657 ◽  
pp. 446-449
Author(s):  
Takahiro Takita ◽  
Hiroaki Ando ◽  
Akihisa Kubota ◽  
Mutsumi Touge

In this study, we investigated the possibility of smoothing a GaN substrate utilizing ultraviolet (UV) assisted polishing method in potassium hydroxide (KOH) solution. In this polishing method, GaN substrate was excited by an UV radiation, and then an oxide layer on the GaN substrate was formed by photochemical reaction. Simultaneously, generated oxide layer was removed by synthetic quartz tool and chemically etched by KOH solution. Finally, smoothed GaN surface could be realized. The surface quality and removal depth were measured and evaluated using a scanning white light interferometer and Normalski type differential interference microscopy. Obtained results show that the surface morphology and the removal rate are strongly dependent on the existence of the UV irradiation. Moreover, the processed surface has revealed that many scratches on the preprocessed GaN surface could be completely removed. The microroughness of the processed GaN surface profile was improved to be 0.18 nm (Rms), 1.06 nm (Rz).

2012 ◽  
Vol 523-524 ◽  
pp. 24-28 ◽  
Author(s):  
Akihisa Kubota ◽  
Kazuya Kurihara ◽  
Mutsumi Touge

In this study, we investigated the possibility of removing and smoothing a single-crystal silicon carbide (SiC) surface under ultraviolet (UV) irradiation in hydrogen peroxide (H2O2) solution. In this method, a SiC substrate was excited by UV irradiation that transmitted synthetic quartz, and then an oxide layer on the SiC substrate was formed by photochemical reaction. Simultaneously, hydroxyl radical (OH*) was generated by the decomposition of H2O2 solution by UV irradiation. OH* plays an important role of oxidation of SiC surface. With these chemical reactions, oxide layer was effectively formed on the SiC surface. Finally, the oxide layer generated on a SiC substrate was chemically and/or mechanically removed by synthetic quartz and solutions. The polishing characteristics of this method were investigated by controlling the process parameters. Additionally, surface quality and removal depth were measured and evaluated by a phase-shift interference microscopy. Obtained results show that the surface morphology and the removal rate are strongly dependent on the existence of the UV irradiation. Moreover, it is shown that the removal characteristics of the SiC substrate depend on the process parameters such as the process time, reciprocating speed, and contact load. The processed surface has revealed that many scratches on the preprocessed surface was completely removed. The microroughness of the processed surface was improved to 0.15 nm (Rms) and 1.62 nm (p-v), respectively. These results provide useful information for obtaining an atomically smooth SiC surface.


2020 ◽  
Vol 10 (5) ◽  
pp. 1667 ◽  
Author(s):  
Basem M. A. Abdo ◽  
Abdualziz El-Tamimi ◽  
Emad Abouel Nasr

Pocket milling has been regarded as one of the most widely used operations in machining. The surface quality of the machined pockets is an essential aspect of any engineering and medical applications. In the current study, rotary ultrasonic machining (RUM) was applied for milling micro-pockets on alumina (Al2O3) ceramic. The objective of this research was to analyze the effect of the tool overlapping parameters on the surface roughness, surface morphology and the profiles of the machined pockets. Subsequently, the effect of different tool path strategies was analyzed on the surface quality and the material removal rate (MRR) of the machined pockets. A scanning electron microscope is used for analyzing the tool wear mechanisms. The experimental results provide evidence that the surface roughness, surface morphology and the MRR have been significantly affected by the considered tool overlapping and the tool path strategies. Furthermore, among the selected tool overlapping parameters (5–25%) and the tool path strategies, the best surface roughness (Ra = 0.155 μm and Rt = 1.432 µm) of the machined pockets can be found at 20% of the tool overlapping with a mix of uni-directional and zigzag tool path strategy.


2021 ◽  
Vol 34 (1) ◽  
Author(s):  
Xu Zhao ◽  
Yadong Gong ◽  
Guiqiang Liang ◽  
Ming Cai ◽  
Bing Han

AbstractThe existing research on SiCp/Al composite machining mainly focuses on the machining parameters or surface morphology. However, the surface quality of SiCp/Al composites with a high volume fraction has not been extensively studied. In this study, 32 SiCp/Al specimens with a high volume fraction were prepared and their machining parameters measured. The surface quality of the specimens was then tested and the effect of the grinding parameters on the surface quality was analyzed. The grinding quality of the composite specimens was comprehensively analyzed taking the grinding force, friction coefficient, and roughness parameters as the evaluation standards. The best grinding parameters were obtained by analyzing the surface morphology. The results show that, a higher spindle speed should be chosen to obtain a better surface quality. The final surface quality is related to the friction coefficient, surface roughness, and fragmentation degree as well as the quantity and distribution of the defects. Lower feeding amount, lower grinding depth and appropriately higher spindle speed should be chosen to obtain better surface quality. Lower feeding amount, higher grinding depth and spindle speed should be chosen to balance grind efficiently and surface quality. This study proposes a systematic evaluation method, which can be used to guide the machining of SiCp/Al composites with a high volume fraction.


Author(s):  
Barnabás Zoltán Balázs ◽  
Márton Takács

Micro-milling is one of the most essential technologies to produce micro components, but due to the size effect, it has many special characteristics and challenges. The process can be characterised by strong vibrations, relatively large run-out and tool deformation, which directly affects the quality of the machined surface. This paper deals with a detailed investigation of the influence of cutting parameters on surface roughness and on the special characteristics of micro-milled surfaces. Several systematic series of experiments were carried out and analysed in detail. A five-axis micromachining centre and a two fluted, coated carbide micro-milling tool with a diameter of 500 µm were used for the tests. The experiments were conducted on AISI H13 hot-work tool steel and Böhler M303 martensitic corrosion resistance steel with a hardness of 50 HRC in order to gain relevant information of machining characteristics of potential materials of micro-injection moulding tools. The effect of the cutting parameters on the surface quality and on the ratio of Rz/ Ra was investigated in a comprehensive cutting parameter range. ANOVA was used for the statistical evaluation. A novel method is presented, which allows a detailed analysis of the surface profile and repetitions, and identify the frequencies that create the characteristic profile of the surface. The procedure establishes a connection between the frequencies obtained during the analysis of dynamics (forces, vibrations) of the micro-milling process and the characterising repetitions and frequencies of the surface.


Author(s):  
Zhichao Geng ◽  
Ping Zhou ◽  
Lei Meng ◽  
Ying Yan ◽  
Dongming Guo

Abstract Lapping has a history of hundreds of years, yet it still relies on the experience of workers. To improve the automaticity and controllability of the lapping process, a modeling method of friction and wear is developed to predict the surface profile evolution of the workpiece and lapping plate in the lapping process. In the proposed method, by solving the balance equations of resultant force and moment, the inclination angles of the workpiece can be calculated, thus more accurate contact pressure distribution of the workpiece/lapping plate interface can be calculated. Combined with the material removal rate model, the continuous evolution process of the workpiece and lapping plate can be predicted in the lapping process. The modeling method was validated by a lapping test of a flat optical glass (Φ 100 mm) with a composite copper plate. The results show that the proposed method can predict the evolution of the surface profile of the workpiece and lapping plate with high accuracy. Consequently, the lapping plate can be dressed at the right time point. Benefit from this, in the validation test the PV value of the workpiece (with 5 mm edge exclusion) was reduced from 5.279 μm to 0.267 μm in 30 min. The proposed surface profile evolution modeling method not only improves the lapping efficiency but also provides an opportunity to understand the lapping process.


Author(s):  
Debtanay Das ◽  
Swarup Bag ◽  
Sukhomay Pal ◽  
M. Ruhul Amin

Abstract Friction stir welding (FSW) is widely accepted by industry because of multiple advantages such as low-temperature process, green technology, and capable of producing good quality weld joints. Extensive research has been conducted to understand the physical process and material flow during FSW. The published works mainly discussed the effects of various process parameters on temperature distribution and microstructure formation. There are few works on the prediction of defect formation from a physics-based model. However, these models ignore chip formation or surface morphology and material loss during the FSW process. In the present work, a fully coupled 3D thermo-mechanical model is developed to predict the chip formation and surface morphology during welding. The effects of various process parameters on surface morphology are also studied using the current model. Coupled Eulerian-Lagrangian (CEL) technique is used to model the FSW process using a commercial software ABAQUS. The model is validated by comparing the results in published literature. The current model is capable of predicting the material flow out of the workpiece and thus enables the visualization of the chip formation. The developed model can extensively be used to predict the surface quality of the friction stir welded joints.


Author(s):  
Greg Pasken ◽  
J. Ma ◽  
Muhammad P. Jahan ◽  
Shuting Lei

Abstract The most common problem when machining titanium using traditional metal cutting processes is that tools rapidly wear out and need to be replaced. This study examines the ability of a pure water jet to machine Ti-6Al-4V via simulations using ABAQUS’s Smoothed Particle Hydrodynamics (SPH). These simulations are then validated experimentally at two pressures, 138 MPa and 317 MPa. Using a Maxiem water jet built by Omax, experiments are conducted by creating a series of 5 lines that are 5 inches (127 mm) long placed 0.5 inches (12.7 mm) apart on a 1 mm thick Ti-6Al-4V workpiece. Predictive modeling is also conducted using the two additional pressures 400 MPa and 621 MPa as well as three orifice diameters 0.254 mm, 0.3556 mm, and 0.4572 mm. The simulations are validated at both pressures and had a percent error less than 2.6% which were within the standard deviation of the experimental results. The predictive modeling indicates that the pressures above 317 MPa create a near identical percent increase from the orifice diameter but the kerf has a more noticeable decrease in width of cut as the pressure increases. The 138 MPa has the smoothest surface profile compared to the other pressures. The volume of removed material decreases as the pressure increases but the material removal rate (MRR) increases as the pressure increases. This is due to the velocity of the water increasing as the pressure increases causing a lower run time. The 621 MPa is the best pressure to machine Ti-6Al-4V as it has a better MRR than the other pressures used in the predictive modelling.


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