scholarly journals Preparation, Characterization and Tribological Properties of Diamond-Like Carbon Film on AZ31 Magnesium Alloy

2019 ◽  
Vol 804 ◽  
pp. 69-74
Author(s):  
Bei Bei Han ◽  
Dong Ying Ju ◽  
Susumu Sato ◽  
Hui Jun Zhao

In this study, DLC films were deposited using IBED with various CH4/H2 ratio, gas flow rates and accelerating voltages. The composition and mechanical properties of the DLC coatings were characterized using SEM, Raman spectroscopy and nanoindentor. The tribological properties of the coating were also investigated using a frictional surface microscope with an in situ observation system and friction force measurements. The DLC films were characterized by a lower ID/IG, higher hardness, and improved tribological properties when deposited at a lower accelerating voltage (6 kV). At the CH4/H2 ratio of 1:99 and 6 sccm/6 kV, minimum ID/IG values of 0.62, relatively low friction coefficient of 0.12 , and a maximum hardness of 4056 HV were attained respectively.

Author(s):  
K. Fukushima ◽  
N. Kohyama ◽  
A. Fukami

A film-sealed high resolution environmental cell(E.C) for observing hydrated materials had been developed by us(l). Main specification of the E.C. is as follows: 1) Accelerated voltage; 100 kV. 2) Gas in the E.C.; saturated water vapour with carrier gas of 50 Torr. 3) Thickness of gas layer; 50 μm. 4) Sealing film; evaporated carbon film(20 nm thick) with plastic microgrid. 5) Resolving power; 1 nm. 6) Transmittance of electron beam; 60% at 100 kV. The E.C. had been successfully applied to the study of hydrated halloysite(2) (3). Kaolin minerals have no interlayer water and are basically non-expandable but form intercalation compounds with some specific chemicals such as hydrazine, formamide and etc. Because of these compounds being mostly changed in vacuum, we tried to reveal the structure changes between in wet air and in vacuum of kaolin minerals intercalated with hydrazine and of hydrated state of montmori1lonite using the E.C. developed by us.


Polar Biology ◽  
2021 ◽  
Author(s):  
Philipp Neitzel ◽  
Aino Hosia ◽  
Uwe Piatkowski ◽  
Henk-Jan Hoving

AbstractObservations of the diversity, distribution and abundance of pelagic fauna are absent for many ocean regions in the Atlantic, but baseline data are required to detect changes in communities as a result of climate change. Gelatinous fauna are increasingly recognized as vital players in oceanic food webs, but sampling these delicate organisms in nets is challenging. Underwater (in situ) observations have provided unprecedented insights into mesopelagic communities in particular for abundance and distribution of gelatinous fauna. In September 2018, we performed horizontal video transects (50–1200 m) using the pelagic in situ observation system during a research cruise in the southern Norwegian Sea. Annotation of the video recordings resulted in 12 abundant and 7 rare taxa. Chaetognaths, the trachymedusaAglantha digitaleand appendicularians were the three most abundant taxa. The high numbers of fishes and crustaceans in the upper 100 m was likely the result of vertical migration. Gelatinous zooplankton included ctenophores (lobate ctenophores,Beroespp.,Euplokamissp., and an undescribed cydippid) as well as calycophoran and physonect siphonophores. We discuss the distributions of these fauna, some of which represent the first record for the Norwegian Sea.


1995 ◽  
Vol 81 (6) ◽  
pp. 607-612 ◽  
Author(s):  
Takayuki NARUSHIMA ◽  
Naoki KIKUCHI ◽  
Makoto MARUYAMA ◽  
Haruo ARASHI ◽  
Yuichiro NISHINA ◽  
...  

2021 ◽  
Author(s):  
Jean-Michel Lellouche ◽  
Romain Bourdalle-Badie ◽  
Eric Greiner ◽  
Gilles Garric ◽  
Angelique Melet ◽  
...  

<p>The GLORYS12V1 system is a global eddy-resolving physical ocean and sea ice reanalysis at 1/12° resolution covering the 1993-present altimetry period, designed and implemented in the framework of the Copernicus Marine Environment Monitoring Service (CMEMS). All the essential ocean physical variables from this reanalysis are available with free access through the CMEMS data portal.</p><p>The GLORYS12V1 reanalysis is based on the current CMEMS global real-time forecasting system, apart from a few specificities that are detailed in this manuscript. The model component is the NEMO platform driven at the surface by atmospheric conditions from the ECMWF ERA-Interim reanalysis. Ocean observations are assimilated by means of a reduced-order Kalman filter. Along track altimeter sea level anomaly, satellite sea surface temperature and sea ice concentration data and in situ temperature and salinity (T/S) vertical profiles are jointly assimilated. A 3D-VAR scheme provides an additional correction for the slowly-evolving large-scale biases in temperature and salinity.</p><p>The performance of the reanalysis is first addressed in the space of the assimilated observations and shows a clear dependency on the time-dependent in situ observation system, which is intrinsic to most reanalyses. The general assessment of GLORYS12V1 highlights a level of performance at the state-of-the-art and the reliability of the system to correctly capture the main expected climatic interannual variability signals for ocean and sea ice, the general circulation and the inter-basins exchanges. In terms of trends, GLORYS12V1 shows a higher than observed  warming trend together with a lower than observed global mean sea level rise.</p><p>Comparisons made with an experiment carried out on the same platform without assimilation show the benefit of data assimilation in controlling water masses properties and their low frequency variability. Examination of the deep signals below 2000 m depth shows that the reanalysis does not suffer from artificial signals even in the pre-Argo period.</p><p>Moreover, GLORYS12V1 represents particularly well the small-scale variability of surface dynamics and compares well with independent (non-assimilated) data. Comparisons made with a twin experiment carried out at ¼° resolution allows characterizing and quantifying the strengthened contribution of the 1/12° resolution onto the downscaled dynamics.</p><p>In conclusion, GLORYS12V1 provides a reliable physical ocean state for climate variability and supports applications such as seasonal forecasts. In addition, this reanalysis has strong assets to serve regional applications and should provide relevant physical conditions for applications such as marine biogeochemistry. In a near future, GLORYS12V1 will be maintained to be as close as possible to real time and could therefore provide a relevant reference statistical framework for many operational applications.</p>


Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 917 ◽  
Author(s):  
Shimizu ◽  
Kobayashi ◽  
Vorholt ◽  
Yang

: To investigate the underlying mechanism of the effects of surface texturing on lubricated sliding friction in the metal forming operation, an in-situ observation system using transparent silica glass dies and a high speed recording camera was newly developed. To correlate the dimensional parameters of micro-dimple textured structures and tribological properties in the metal forming operation, the in-situ observation was performed during bending with the ironing process of the stainless steel sheet with a thickness of 0.1 mm. The lubrication behavior were compared between the different lubricant viscosities and the micro-dimple textures with different diameters of 10 µm, 50 µm, 100 µm fabricated by using femto-/pico-second laser processing. As a result, the textured die with dimple diameters of 10 µm and 50 µm showed the lubricant flow transferred from one to the other dimples owing to the lubricant reservoir effect, while that of 100 µm indicated the less supply of the lubricant. However, the textured die with a dimple diameter of 10 µm demonstrated higher ironing force than that of 50 µm, due to the severe adhesion of work materials inside the dimple structures. Based on these experimental findings, the dimple size dependencies on lubricant reservoirs effects and the generation of the hydrodynamic pressure were discussed by correlating with the in-situ observation results, a fluid-flow analysis and a laminar two-phase flow analysis using the finite element method.


2014 ◽  
Vol 627 ◽  
pp. 361-364 ◽  
Author(s):  
Yasuhiro Yamazaki

In this paper, an in-situ measurement of crack size as a function of applied indentation load during indentation test was conducted. To perform the in-situ measurement, an instrumented indentation test machine with the in-situ observation system was developed and used. The joints of transparent ceramics by diffusion bonding were prepared as the specimen used in this study. The indentations were performed at the interface of the joints, and in the monolithic transparent ceramics by means of the instrumented indenter with the in-situ observation system. The relationship between crack shape and indentation load, as well as, the effect of the indenter shape on it were discussed.


Author(s):  
Tatsuya OKAMOTO ◽  
Hidenori NISHIMURA ◽  
Noritsugu UMEHARA ◽  
Motoyuki MURASHIMA ◽  
Takayuki TOKOROYAMA

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