Extraction of Essential Oil from Sedap malam Flower (Polianthes tuberosa) Using Methanol Solvent

2021 ◽  
Vol 872 ◽  
pp. 67-71
Author(s):  
Suharno Rusdi ◽  
Farida Imtiyaz ◽  
Nopia Denvil Wulandari ◽  
Achmad Chafidz
Keyword(s):  
Essential Oil ◽  
Chemical Properties ◽  
Extraction Process ◽  
Physical And Chemical Properties ◽  
Simple Distillation ◽  
Infra Red ◽  
Ft Ir ◽  
Ir Analysis ◽  
Physical And Chemical ◽  
And Chemical Properties

The objectives of this study are to obtain essential oil from Sedap Malam (Tuberose) flower via extraction method and to characterize the physical and chemical properties of the essential oil produced, such as density, rendement, and chemical composition. The extraction process was carried out by using methanol solvent. The ratio between Sedap Malam flower and the methanol solvent was 1:5. After the extraction process of the essential oil finished, the essential oil and the solvent were separated via a simple distillation process. The collected essential oil was then characterized using Gas Chromatography-Mass Spectrophotometry (GC-MS) apparatus and Fourier Transform Infra-Red (FT-IR) analysis to investigate the content of the essential oil extracted from Sedap Malam flower. The physical characterization results showed that the essential oil has average rendement value of 12.605 % and density value of 1.0905 g/mL. Additionally, organoleptic test was carried to test the response of respondents toward the color and odor/fragrance of the essential oil extracted from Sedap Malam flower. Most of the responses were included in categories of “Like” and “Really like”. Additionally, for the fragrance, most of response of the respondents for all the four samples of essential oil were in category of “Really like”.

Effect of dextrose equivalent on physical and chemical properties of lime essential oil microparticles

2017 ◽  
Vol 102 ◽  
pp. 105-114 ◽  
Author(s):  
Pedro Henrique Campelo ◽  
Eloá Lourenço do Carmo ◽  
Rosana Domingues Zacarias ◽  
Maria Irene Yoshida ◽  
Vany Perpétua Ferraz ◽  
...  
Keyword(s):  
Essential Oil ◽  
Chemical Properties ◽  
Physical And Chemical Properties ◽  
Dextrose Equivalent ◽  
Physical And Chemical ◽  
And Chemical Properties

scholarly journals Spling of slots in chaff as an effect of using mixtures with a regulated composite related basis in the bathroom in gas structures

2018 ◽  
pp. 50-56
Author(s):  
V Kamkin ◽  
S Tokarev ◽  
A Mishalkin ◽  
R Ankudinov ◽  
O Bezshkurenko
Keyword(s):  
Carbon Content ◽  
Disperse Material ◽  
Chemical Properties ◽  
Component Composition ◽  
Extraction Process ◽  
Slag Formation ◽  
Physical And Chemical Properties ◽  
Natural Minerals ◽  
Physical And Chemical ◽  
And Chemical Properties

The purpose of the work is to select a rational mode of slag formation in oxygen converters and chipboard. It should be based on the study of the influence of the chemical and component composition on the physical and chemical properties of slag, which determine its refining capacity. The physicochemical substantiation of the rational component and chemical composition of fluxes for the formation of a slag phase with given physical and chemical properties during the smelting of electric steel is given. It has been shown that when reducing the oxidation intensity of carbon in a metal melt and in the conditions of the extraction process for the formation of a stable gas-slag foam, the use of complex slag-forming mixtures containing natural minerals and man-made wastes on the basis of carbon and iron oxides is used. Increasing the efficiency of applying slag-forming mixtures with an adjustable CaO: CaCO3: C: FexOy ratio is achieved by implementing a method for introducing a disperse material into a carrier gas stream with an oxidizing potential, depending on the carbon content in the metal. It is established that the most rational for conditions of oxygen-converter melting is the use of materials intended for use, which contain lime with cigarette butter 15 - 20%. The material is fed to the bath at the end of the oxidation period with a decrease in carbon content to 0.15-0.2% with a significant increase in the temperature of the liquid steel. For conditions of steel smelting in the chipboard, the cigarette can be 40 60%.

Synthesis of Fe3O4 Magnetic Nanoparticles in a Helical Microreactor

2020 ◽  
Vol 842 ◽  
pp. 174-181
Author(s):  
Dan Wang ◽  
Mudassir Iqbal ◽  
Ming Qiao Zhu
Keyword(s):  
Magnetic Nanoparticles ◽  
Saturation Magnetization ◽  
Chemical Properties ◽  
Precipitation Method ◽  
Physical And Chemical Properties ◽  
Reaction Conditions ◽  
Ft Ir ◽  
Co Precipitation ◽  
Physical And Chemical ◽  
And Chemical Properties

Fe3O4 nanoparticles (NPs) have previously been employed in various fields owing to their unique physical and chemical properties. In this paper, Fe3O4 NPs are prepared by co-precipitation method in a helical microreactor under different reaction conditions which affect the size of Fe3O4 NPs. The product is characterized by FT-IR and XPS. Also, VSM characterization shows that Fe3O4 exhibits typical superparamagnetic behavior and the saturation magnetization of NPs is 53 emu/g.

scholarly journals Preparation of Poly (N-4-Antipyrinyl or Procainyl Methyl Nadamic Acids) as Drug Polymers

2014 ◽  
Vol 5 (1) ◽  
pp. 42-53
Author(s):  
Dr. Firyal M. Ali AL-Salami ◽  
Abbas N. M. AL-Sharify ◽  
Khudheyer Jawad Kadhem
Keyword(s):  
Room Temperature ◽  
Uv Spectroscopy ◽  
Chemical Properties ◽  
Physical And Chemical Properties ◽  
Release Rates ◽  
Ph Values ◽  
Ft Ir ◽  
Physical And Chemical ◽  
And Chemical Properties ◽  
Ostwald Viscometer

Two new monomers of N-4-antipyrinyl methyl nadamic acid M1 and N-Procaienyl methyl nadamic acid M2 were synthesized from reaction of 4-Aminoantipyrine or procaine with methyl nadic anhydride at room temperature with dioxane as a solvent. The prepared monomers M1 and M2 were polymerized free radically with AIBN as initiator to corresponding polyamic acids P1 and P2, Which were converted to their sodium salt polymers P3 and P4 to enhanced their solubility's in water. The physical and chemical properties were studied for monomers and polymers, also FT-IR ,1H-NMR  and UV. Spectroscopy was characterized of M1or M2. The intrinsic viscosity was measured by  Ostwald viscometer at 30 0C  .The swelling %was measured and the controlled release rates of drug polymers were studied in different pH values at 37 0C.

scholarly journals Correlation and modelling of the penetration and softening point tests of bitumen binders with a variety of physical and chemical properties

2021 ◽  
Vol 76 ◽  
pp. 57
Author(s):  
Marvy Girgis ◽  
Jérémie Barbier ◽  
Alain Quignard ◽  
Isabelle Merdrignac ◽  
João Marques
Keyword(s):  
Softening Point ◽  
Good Accuracy ◽  
Chemical Properties ◽  
The Other ◽  
Proton Nuclear Magnetic Resonance ◽  
Physical And Chemical Properties ◽  
H Nmr ◽  
Ft Ir ◽  
Physical And Chemical ◽  
And Chemical Properties

Studying bitumen has always posed a challenge to researchers owing to its extreme complexity and unique properties. To classify it commercially and to determine bitumen grade, two standard empirical tests have been adopted within the European standardized bitumen binders system [EN 12591:2009 (2009) Bitumen and bituminous binders – Specifications for paving grade bitumens]: Softening Point (SP) and Penetration (PEN). The relationship between these two tests and the physical or chemical properties of bitumen is not well understood. For the first time, this study represents an attempt to build more understanding of such a relationship through a comprehensive study of the correlation between the two standard tests and many physical and chemical properties of bitumen. A second goal is to propose some predictive models for these two tests and compare their predictive accuracy. Therefore, 13 Straight Run Vacuum Residues (SRVR) samples from different geographical origins were analyzed to measure the following parameters: Dynamic Viscosity (VisDy), Conradson Carbon Residue (CCR), C5 Asphaltenes Content (AspC5), C7 Asphaltenes Content (AspC7), Elemental Analysis (including C, H, O, N, S, Ni, and V content), Simulated Distillation (SD), Fourier-Transform Infrared Spectroscopy (FT-IR), and proton nuclear magnetic resonance spectroscopy (H-NMR). Results of studying correlations using correlation matrix and Principal Component Analysis (PCA) have emphasized the prominent effect of asphaltenes content on the other properties and the results of SP and PEN. It has also shown the potential importance of the aliphaticity/aromaticity of bitumen. Then, four models were proposed for the prediction of SP and PEN: viscosity, FT-IR, H-NMR, and multi-parameter models. Partial least squares (PLS) regression was used for building all models, except viscosity ones. All SP models, except H-NMR model, exhibited very good accuracy compared to the standard method. On the other hand, PEN was more difficult to predict than SP and only the multi-parameter model of PEN showed relatively good accuracy of prediction.

scholarly journals Characteristics of Sodium Alginate Extracted from Turbinaria sp. and Sargassum sp.

2018 ◽  
Vol 13 (2) ◽  
pp. 79 ◽  
Author(s):  
Rinta Kusumawati ◽  
Jamal Basmal ◽  
Bagus Sediadi Bandol Utomo
Keyword(s):  
Water Content ◽  
Sodium Alginate ◽  
Raw Materials ◽  
Chemical Properties ◽  
Brown Seaweed ◽  
Extraction Process ◽  
Physical And Chemical Properties ◽  
Physical And Chemical ◽  
And Chemical Properties

Characterization of sodium alginate extracted from two species of brown seaweed (Turbinaria sp. and Sargassum sp.) has been conducted. The aim of the study was to evaluate physical and chemical properties of the two different types of sodium alginates produced from this extraction process. Extraction was conducted in alkaline solution followed by acid treatment with the following steps: sortation of seaweed, washing, alkaline extraction, bleaching, alginic acid and sodium alginate conversion, dehydration using isopropyl alcohol (IPA), drying, chopping and grinding. Each extraction was conducted in duplicate using approximately 1 kg of the raw materials. The physical and chemical properties of the final products (sodium alginate powders) were analyzed. The results of the analysis were as follows: the yield of alginate powder from Turbinaria sp. was 14.77% having water content of 13.48%; whiteness degree of 23.77%; and viscosity of 133.67 cPs while the yield of sodium alginate powder extracted from Sargassum sp. was 24.56% with water content of 12.69%; whiteness degree of 43.80%; and viscosity of 217.50 cPs. Both alginate powders had better physical characteristics compared to commercial grade alginate which had water content of 16.07%, whiteness degree of 29.37%, and viscosity of 102.67cPs.

Physical Characteristics and Organoleptic Test of Essential Oil Extracted from Sedap malam Flower (Polianthes tuberosa) Using N-Hexane Solvent

2021 ◽  
Vol 882 ◽  
pp. 191-199
Author(s):  
Suharno Rusdi ◽  
Farida Imtiyaz ◽  
Nopia Denvil Wulandari ◽  
Achmad Chafidz
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Essential Oil ◽  
Extraction Method ◽  
Soxhlet Extraction ◽  
Extraction Process ◽  
Gas Chromatography Mass Spectrometry ◽  
Infra Red ◽  
Ft Ir ◽  
Ir Analysis

In this work, an essential oil was extracted from from Sedap Malam (Tuberose) flower using n-hexane as the solvent. The extraction process was performed using simple soxhlet extraction method with the ratio between Sedap Malam flower and n-hexane solvent was 1:5. The physical properties, such as density and rendement values of the extracted essential oil were analyzed. The analysis results exhibited that the essential oil has average rendement value of 9.91 % and density value of 0.9275 g/mL. Additionally, organoleptic testing was also carried out to test the response of respondents toward the color and odor/fragrance of the extracted essential oil. The results showed that the responses of the respondents about the color and fragrance of the extracted essential oil were quite satisfactory. The highest responses for both color and the fragrance were belong to “Really Like” category. The extracted essential oil was also characterized using Gas Chromatography - Mass Spectrometry (GC-MS) apparatus and Fourier Transform Infra-Red (FT-IR) analysis.

scholarly journals SOME PHYSICAL PROPERTIES OF ESSENTIAL OIL OF BARAKASEED NIGELLA SATIVA L. IMPACTED BY BAT GUANO Otonycteris hemprichii Camd AND SEAWEED EXTRACT

2016 ◽  
Vol 47 (4) ◽  
Author(s):  
Al-mohammedi & et al.
Keyword(s):  
Refractive Index ◽  
Essential Oil ◽  
Nigella Sativa ◽  
Chemical Properties ◽  
Seaweed Extract ◽  
Physical And Chemical Properties ◽  
Oil Density ◽  
Physical And Chemical ◽  
And Chemical Properties ◽  
Bat Guano

Some fertilizers practices could be used to improve Baraka seed Nigella sativa L. as a medicinal crop like organic farmyard manure which efficiently applied to enhance growth and yield. Thus, a field experiment was conducted out at Research Station in Tikrit-Iraq during 2012/2013 season to estimate the impact of bat guano (0, 75, 125 and 175 kg.ha-1), seaweed extract as kelpak (0, 1, 2 and 3ml.l-1) on some physical and chemical essential oil components. Two factors were arranged in factorial experiment in randomized complete block design with three replicates. Thus, results revealed that application of bat guano at 125 kg.ha-1 was superior in enhancement of essential oil and its some physical and chemical properties as essential oil% of 1.53%, specific gravity of 0.95 g.cm-3, refractive index of 1.82, essential oil density of 0.93, dithymohydroquinone of 37.44µg.µl-1 and thymol of 25.73 µg.µl-1. Moreover, kelpak (3ml.l-1) significantly improved physical and chemical properties of essential oil which were essential oil% of 1.52%, specific gravity of 0.93 g.cm-3, refractive index of 1.72, and essential oil density of 0.94 and thymol of 25.92 µg.µl-1. Whereas, the main component dithymohydroquinone effected by application of 2 ml.l-1kelpak of 37.04 µg.µl-1. It could be recommended to use bat guano as alternative to chemical fertilizer fortified with foliar application of seaweed extract as kelpak so as to improve physical and chemical properties of essential oil.

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