Interlaboratory Comparison (Round Robin) of the Application of the Rietveld Method to Quantitative Phase Analysis by X-Ray and Neutron Diffraction

2001 ◽  
Vol 378-381 ◽  
pp. 124-131 ◽  
Author(s):  
B. Peplinski ◽  
Dietrich Schultze ◽  
J. Wenzel
Keyword(s):  
Neutron Diffraction ◽  
Phase Analysis ◽  
Interlaboratory Comparison ◽  
Rietveld Method ◽  
Round Robin ◽  
Quantitative Phase Analysis ◽  
X Ray ◽  
Quantitative Phase

scholarly journals The effect of data quality and model parameters on the quantitative phase analysis of X-ray diffraction data by the Rietveld method

2021 ◽  
Vol 54 (3) ◽  
Author(s):  
Matthew R. Rowles
Keyword(s):  
Phase Analysis ◽  
Diffraction Data ◽  
Rietveld Method ◽  
Quantitative Phase Analysis ◽  
Model Parameters ◽  
Case Scenario ◽  
X Ray ◽  
Quantitative Phase ◽  
Two Samples ◽  
Using Data

The quality of X-ray powder diffraction data and the number and type of refinable parameters have been examined with respect to their effect on quantitative phase analysis (QPA) by the Rietveld method using data collected from two samples from the QPA round robin [Madsen, Scarlett, Cranswick & Lwin (2001). J. Appl. Cryst. 34, 409–426]. From the analyses of these best-case-scenario specimens, a series of recommendations for minimum standards of data collection and analysis are proposed. It is hoped that these will aid new QPA-by-Rietveld users in their analyses.

scholarly journals Evaluation via multivariate techniques of scale factor variability in the rietveld method applied to quantitative phase analysis with X ray powder diffraction

2006 ◽  
Vol 9 (4) ◽  
pp. 369-374 ◽  
Author(s):  
Terezinha Ferreira de Oliveira ◽  
Roberto Ribeiro de Avillez ◽  
Eugenio Kahn Epprecht ◽  
Joaquim Carlos Barbosa Queiroz
Keyword(s):  
Phase Analysis ◽  
Powder Diffraction ◽  
Rietveld Method ◽  
Scale Factor ◽  
Quantitative Phase Analysis ◽  
Multivariate Techniques ◽  
X Ray ◽  
Quantitative Phase

Effect of Testing Factors on Rietveld Quantitative Analysis of Cement-Matrix Materials

2017 ◽  
Vol 898 ◽  
pp. 2054-2059
Author(s):  
Yan Ling Gan ◽  
Su Ping Cui ◽  
Ya Li Wang ◽  
Hong Xia Guo
Keyword(s):  
Quantitative Analysis ◽  
Phase Analysis ◽  
Rietveld Method ◽  
Cementitious Materials ◽  
Cement Matrix ◽  
Quantitative Phase Analysis ◽  
Step Size ◽  
X Ray ◽  
Quantitative Phase ◽  
Scan Time

For cement-matrix materials, the microstructure plays a vital important role in the research. Recently, quantitative phase analysis of cementitious materials can be performed using the Rietveld method by fitting the calculated X-ray diffraction (XRD) profile with the observed one. The aim of this paper is to further perform the quantitative analysis by the Rietveld method and discuss the influence of testing factors on the Rietveld quantitative phase analysis. The factors included the collection range of pattern, step size and the scan time of per step. In this study, the chemical composition of the samples was determined by X-ray fluorescence (XRF) spectrometry. And their phase composition was calculated by X-ray powder diffraction and Rietveld analysis. The results showed that the collection range of pattern depended on the tested materials , and the scanning range should include the main diffraction peak of the sample. Smaller step size and longer scan time of each step made the fitting factor smaller, also the calculated pattern coincided with the measured pattern, better enhance the precision of the analyses.

On the quantitative phase analysis and amorphous content of triacylglycerols materials by X-ray Rietveld method

2018 ◽  
Vol 212 ◽  
pp. 51-60 ◽  
Author(s):  
Guilherme A. Calligaris ◽  
Thais L.T. da Silva ◽  
Ana Paula B. Ribeiro ◽  
Adenilson O. dos Santos ◽  
Lisandro P. Cardoso
Keyword(s):  
Phase Analysis ◽  
Rietveld Method ◽  
Quantitative Phase Analysis ◽  
X Ray ◽  
Quantitative Phase ◽  
Amorphous Content

Quantitative Phase Analyses of a Slag Using X-Ray Powder Diffraction

2014 ◽  
Vol 881-883 ◽  
pp. 1241-1244
Author(s):  
Wei Jin Zeng ◽  
Chao Zeng ◽  
Wei He
Keyword(s):  
Quantitative Analysis ◽  
Phase Analysis ◽  
Powder Diffraction ◽  
Rietveld Method ◽  
Quantitative Phase Analysis ◽  
Powder Diffraction Data ◽  
X Ray ◽  
Quantitative Phase ◽  
Full Profile ◽  
Qualitative Phase

The quantitative phase analyses of a slag have been successfully carried out by using both of the full-profile Rietveld and RIR methods from X-ray powder diffraction data. The qualitative phase analysis indicates that the slag contains mayenite (CaO)12(Al2O3)7, olivine Ca2(SiO4), gehlenite Ca2Al (AlSiO7), lemite Ca2(SiO4) and hibonite CaO(Al2O3)6. The quantitative analysis from Rietveld refinement shows that the weight concentrations of mayenite, olivine, gehlenite, lemite and hibonite for the slag are 48.8(4) wt.%, 32.2(5) wt.%, 11.0(9) wt.%, 6.2(1.1) wt.% and 1.8 (1.2) wt.%, respectively. The quantitative phase analysis results obtained by Rietveld method are more precise then those by RIR method.

Quantitative phase analysis using the Rietveld method

1988 ◽  
Vol 21 (2) ◽  
pp. 86-91 ◽  
Author(s):  
D. L. Bish ◽  
S. A. Howard
Keyword(s):  
Phase Analysis ◽  
Rietveld Method ◽  
Quantitative Phase Analysis ◽  
Quantitative Phase

X-Ray Diffraction Intensity of Oxide Solid Solutions: Application to Qualitative and Quantitative Phase Analysis

1982 ◽  
pp. 119-128
Author(s):  
Ronald C. Gehringer ◽  
Gregory J. McCarthy ◽  
R. G. Garvey ◽  
Deane K. Smith
Keyword(s):  
Phase Analysis ◽  
Solid Solutions ◽  
Quantitative Phase Analysis ◽  
X Ray Diffraction ◽  
Diffraction Intensity ◽  
X Ray ◽  
Quantitative Phase ◽  
Qualitative And Quantitative

scholarly journals Quantitative Phase Analysis in Textured Steels by Continuous X-ray Diffraction Method with Energy Analysis System

1981 ◽  
Vol 67 (11) ◽  
pp. 2039-2048 ◽  
Author(s):  
Nobukatsu FUJINO ◽  
Yoshiro MATSUMOTO ◽  
Yasuhiro MAEHARA
Keyword(s):  
Phase Analysis ◽  
Energy Analysis ◽  
Diffraction Method ◽  
Quantitative Phase Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Quantitative Phase ◽  
Analysis System

Quantitative Phase Analysis by X-Ray Diffraction.

1966 ◽  
Vol 38 (12) ◽  
pp. 1741-1745 ◽  
Author(s):  
R. F. Karlak ◽  
D. S. Burnett
Keyword(s):  
Phase Analysis ◽  
Quantitative Phase Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Quantitative Phase
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