Microstructural Evolution of Synthetic Forsterite Aggregates Deformed to High Strain

2004 ◽  
Vol 467-470 ◽  
pp. 579-584 ◽  
Author(s):  
A. Kellermann Slotemaker ◽  
J.H.P. de Bresser ◽  
C.J. Spiers ◽  
M.R. Drury

Microstructures provide the crucial link between solid state flow of rock materials in the laboratory and large-scale tectonic processes in nature. In this context, microstructural evolution of olivine aggregates is of particular importance, since this material controls the flow of the Earth’s upper mantle and affects the dynamics of the outer Earth. From previous work it has become apparent that if olivine rocks are plastically deformed to high strain, substantial weakening may occur before steady state mechanical behaviour is approached. This weakening appears directly related to progressive modification of the grain size distribution through competing effects of dynamic recrystallization and syn-deformational grain growth. However, most of our understanding of these processes in olivine comes from tests on coarse-grained materials that show grain size reduction through dynamic recrystallization. In the present study we focused on fine-grained (~1 µm) olivine aggregates (i.e., forsterite/Mg2SiO4), containing ~0.5 wt% water and 10 vol% enstatite (MgSiO3), Samples were axially compressed to varying strains up to a maximum of ~45%, at 600 MPa confining pressure and a temperature of 950°C. Microstructures were characterized by analyzing full grain size distributions and textures using SEM/EBSD. We observed syndeformational grain growth rather than grain size reduction, and relate this to strain hardening seen in the stress-strain curves.

Solid Earth ◽  
2019 ◽  
Vol 10 (1) ◽  
pp. 95-116 ◽  
Author(s):  
Felix Hentschel ◽  
Claudia A. Trepmann ◽  
Emilie Janots

Abstract. Deformation microstructures of albitic plagioclase and K-feldspar were investigated in mylonitic pegmatites from the Austroalpine basement south of the western Tauern Window by polarized light microscopy, electron microscopy and electron backscatter diffraction to evaluate feldspar deformation mechanisms at greenschist facies conditions. The main mylonitic characteristics are alternating almost monophase quartz and albite layers, surrounding porphyroclasts of deformed feldspar and tourmaline. The dominant deformation microstructures of K-feldspar porphyroclasts are intragranular fractures at a high angle to the stretching lineation. The fractures are healed or sealed by polyphase aggregates of albite, K-feldspar, quartz and mica, which also occur along intragranular fractures of tourmaline and strain shadows around other porphyroclasts. These polyphase aggregates indicate dissolution–precipitation creep. K-feldspar porphyroclasts are partly replaced by albite characterized by a cuspate interface. This replacement is interpreted to take place by interface-coupled dissolution–precipitation driven by a solubility difference between K-feldspar and albite. Albite porphyroclasts are replaced at boundaries parallel to the foliation by fine-grained monophase albite aggregates of small strain-free new grains mixed with deformed fragments. Dislocation glide is indicated by bent and twinned albite porphyroclasts with internal misorientation. An indication of effective dislocation climb with dynamic recovery, for example, by the presence of subgrains, is systematically missing. We interpret the grain size reduction of albite to be the result of coupled dislocation glide and fracturing (low-temperature plasticity). Subsequent growth is by a combination of strain-induced grain boundary migration and formation of growth rims, resulting in an aspect ratio of albite with the long axis within the foliation. This strain-induced replacement by nucleation (associated dislocation glide and microfracturing) and subsequent growth is suggested to result in the observed monophase albite layers, probably together with granular flow. The associated quartz layers show characteristics of dislocation creep by the presence of subgrains, undulatory extinction and sutured grain boundaries. We identified two endmember matrix microstructures: (i) alternating layers of a few hundred micrometres' width, with isometric, fine-grained feldspar (on average 15 µm in diameter) and coarse-grained quartz (a few hundred micrometres in diameter), representing lower strain compared to (ii) alternating thin layers of some tens of micrometres' width composed of fine-grained quartz (<20 µm in diameter) and coarse elongated albite grains (long axis of a few tens of micrometres) defining the foliation, respectively. Our observations indicate that grain size reduction by strain-induced replacement of albite (associated dislocation glide and microfracturing) followed by growth and granular flow simultaneous with dislocation creep of quartz are playing the dominating role in formation of the mylonitic microstructure.


2018 ◽  
Author(s):  
Felix Hentschel ◽  
Claudia A. Trepmann ◽  
Emilie Janots

Abstract. Deformation microstructures of albitic plagioclase and K-feldspar were investigated in mylonitic pegmatites from the Austroalpine basement south of the western Tauern Window by polarized light microscopy, electron microscopy and electron backscatter diffraction to evaluate the rheologically dominant feldspar deformation mechanisms at greenschist facies conditions. The main mylonitic characteristics are alternating almost monophase quartz and albite layers, surrounding porphyroclasts of deformed feldspar and tourmaline. The dominant deformation microstructures of K-feldspar porphyroclasts are intragranular fractures parallel to the main shortening direction indicated by the foliation. The fractures are healed or sealed by polyphase aggregates of albite, K-feldspar, quartz and mica, which also occur along intragranular fractures of tourmaline and strain shadows around other porphyroclasts. Polyphase aggregates at sites of dilation indicate dissolution-precipitation creep. K-feldspar porphyroclasts are partly replaced by albite characterized by a sawtooth-shaped interface. This replacement is interpreted to be by interface-coupled dissolution-precipitation driven by a solubility difference between K-feldspar and albite and is not controlled by strain. In contrast, albite porphyroclasts are replaced at sites of shortening by fine-grained monophase albite aggregates of small strain-free new grains mixed with deformed fragments. Dislocation glide is indicated by bent, kinked and twinned albite. No indication of effective dislocation climb with dynamic recovery, for example by the presence of subgrains, a crystallographic preferred orientation or sutured grain boundaries was observed. We interpret the grain size reduction of albite at sites of shortening to be the result of coupled fracturing, dislocation glide and strain-induced grain boundary migration. This strain-induced replacement by nucleation and growth leads, together with granular flow, to the monophase albite layers. The associated quartz layers in contrast, show characteristics of dislocation creep by the presence of subgrains, undulatory extinction and sutured grain boundaries. We identified two endmember matrix microstructures that correlate with strain. Samples with lower strain are characterized by layers of a few hundreds of µm width, with coarse-grained quartz and layers with isometric, fine-grained feldspar. Higher strained samples are characterized by narrow alternating layers of some tens of µm width composed of fine-grained quartz and coarse albite grains elongated parallel to the stretching lineation, respectively. These observations indicate that grain size reduction by strain-induced replacement of albite, granular flow assisted by fracturing and dissolution-precipitation together with dislocation creep of quartz are rheologically dominant.


2021 ◽  
Vol 83 (4) ◽  
Author(s):  
S. Adam Soule ◽  
Michael Zoeller ◽  
Carolyn Parcheta

AbstractHawaiian and other ocean island lava flows that reach the coastline can deposit significant volumes of lava in submarine deltas. The catastrophic collapse of these deltas represents one of the most significant, but least predictable, volcanic hazards at ocean islands. The volume of lava deposited below sea level in delta-forming eruptions and the mechanisms of delta construction and destruction are rarely documented. Here, we report on bathymetric surveys and ROV observations following the Kīlauea 2018 eruption that, along with a comparison to the deltas formed at Pu‘u ‘Ō‘ō over the past decade, provide new insight into delta formation. Bathymetric differencing reveals that the 2018 deltas contain more than half of the total volume of lava erupted. In addition, we find that the 2018 deltas are comprised largely of coarse-grained volcanic breccias and intact lava flows, which contrast with those at Pu‘u ‘Ō‘ō that contain a large fraction of fine-grained hyaloclastite. We attribute this difference to less efficient fragmentation of the 2018 ‘a‘ā flows leading to fragmentation by collapse rather than hydrovolcanic explosion. We suggest a mechanistic model where the characteristic grain size influences the form and stability of the delta with fine grain size deltas (Pu‘u ‘Ō‘ō) experiencing larger landslides with greater run-out supported by increased pore pressure and with coarse grain size deltas (Kīlauea 2018) experiencing smaller landslides that quickly stop as the pore pressure rapidly dissipates. This difference, if validated for other lava deltas, would provide a means to assess potential delta stability in future eruptions.


2007 ◽  
Vol 551-552 ◽  
pp. 387-392 ◽  
Author(s):  
Wen Juan Zhao ◽  
Hua Ding ◽  
D. Song ◽  
F.R. Cao ◽  
Hong Liang Hou

In this study, superplastic tensile tests were carried out for Ti-6Al-4V alloy using different initial grain sizes (2.6 μm, 6.5μm and 16.2 μm) at a temperature of 920°C with an initial strain rate of 1×10-3 s-1. To get an insight into the effect of grain size on the superplastic deformation mechanisms, the microstructures of deformed alloy were investigated by using an optical microscope and transmission electron microscope (TEM). The results indicate that there is dramatic difference in the superplastic deformation mode of fine and coarse grained Ti-6Al-4V alloy. Meanwhile, grain growth induced by superplastic deformation has also been clearly observed during deformation process, and the grain growth model including the static and strain induced part during superplastic deformation was utilized to analyze the data of Ti-6Al-4V alloy.


2010 ◽  
Vol 160-162 ◽  
pp. 260-266 ◽  
Author(s):  
Tao Suo ◽  
Kui Xie ◽  
Yu Long Li ◽  
Feng Zhao ◽  
Qiong Deng

In this paper, ultra-fine grained copper fabricated by equal channel angular pressing method and annealed coarse grained copper were tensioned under both quasi-static and dynamic loading conditions using an electronic universal testing machine and the split Hopkinson tension bar respectively. The rapture surface of specimen was also observed via a Scanning Electron Microscope (SEM). The experimental results show that the ductility of polycrystalline copper decreases remarkably due to the grain refinement. However, with the increase of applied strain rate, ductility of the UFG-Cu is enhanced. The fracture morphologies also give the evidence of enhanced ductility of UFG-Cu at high strain rate. It is believed the enhanced ductility of UFG materials at high strain rate can be attributed to the restrained dislocation dynamic recovery.


Author(s):  
Sunal Ahmet Parasiz ◽  
Reid VanBenthysen ◽  
Brad L. Kinsey

Sheet metal forming often consists of bending processes in which gradients of deformation exists through the thickness of the workpiece in a localized deformation area. In microscale bending, these deformation gradients become much steeper, as the changes in the deformation occur over short distances (in the order of micrometers). In addition, with miniaturization, the number of grains that are present through the thickness decreases significantly. In this research, the effect of grain size and specimen size on the deformation distribution through the thickness of microbent sheet specimens was investigated via microhardness evaluations. It was found that the deformation distribution, i.e., hardness profile, is not affected significantly by the grain size when the sheet thickness is large (for 1.625 mm specimens) or by miniaturization of the specimen size when the grain size is fine. However, the deformation distribution of the coarse grained specimens deviates from the fine grained ones and from the 1.625 mm thick sheet specimens when the specimen size is miniaturized.


2018 ◽  
Vol 2018 ◽  
pp. 1-16
Author(s):  
Fang Xu ◽  
Wuming Leng ◽  
Rusong Nie ◽  
Qishu Zhang ◽  
Qi Yang

A new prestressed reinforcement device (PRD) consisting of two lateral pressure plates (LPPs) and a reinforcement bar is developed to strengthen soil embankments by improving the soil confining pressure and providing lateral constraint on embankment slopes. The reinforcement effects of PRDs were demonstrated by investigating the beneficial effects of increasing confining pressure on the soil behavior via the performance of a series of large-scale static and cyclic triaxial tests on a coarse-grained embankment soil. The results show that PRDs can effectively improve the soil shear strength, bearing capacity, ability to resist elastic and plastic deformation, critical dynamic stress, and dynamic shear modulus, and empirical methods were also developed to determine the critical dynamic stress and initial dynamic shear modulus of the embankment soil. Moreover, 3D finite element analyses (FEAs) with an LPP width of 1.2 m were performed to analyze the additional stress field in a prestressed heavy-haul railway embankment. The FEAs showed that the additional stress at a given external distance from the border of an LPP first increased to a maximum value and then gradually decreased with increasing depth; the additional stress was transferred to the zones where the subgrade tends to have higher stresses with peak stress diffusion angles of 34° (slope direction) and 27° (longitudinal direction); and a continuous effective reinforcement zone with a minimum additional stress coefficient of approximately 0.2 was likely to form at the diffusion surface of the train loads, provided that the net spacing of the LPPs was 0.7 m. The reinforcement zone above the diffusion surface of the train loads can act as a protective layer for the zones that tend to have higher stresses. Finally, the advantages and application prospects of PRDs are discussed in detail. The newly developed PRDs may provide a cost-effective alternative for strengthening soil embankments.


2007 ◽  
Vol 551-552 ◽  
pp. 621-626
Author(s):  
Young Gun Ko ◽  
Yong Nam Kwon ◽  
Jung Hwan Lee ◽  
Dong Hyuk Shin ◽  
Chong Soo Lee

Cavitation behavior during superplastic flow of ultra-fine grained (UFG) Ti-6Al-4V alloy was established with the variation of grain size and misorientation. After imposing an effective strainup to 8 via equal-channel angular pressing (ECAP) at 873 K, alpha-phase grains were markedly refined from 11 μm to ≈ 0.3 μm, and misorientation angle was increased. Uniaxial-tension tests were conducted for initial coarse grained (CG) and two UFG alloys (ε = 4 and 8) at temperature of 973 K and strain rate of 10-4 s-1. Quantitative measurements of cavitation evidenced that both the average size and the area fraction of cavities significantly decreased with decreasing grain size and/or increasing misorientation. It was also found that, when compared to CG alloy, cavitation as well as diffused necking was less prevalent in UFG alloys, which was presumably due to the higher value of strain-rate sensitivity. Based on the several theoretical models describing the cavity growth behavior, the cavity growth mechanism in UFG alloys was suggested.


1999 ◽  
Vol 601 ◽  
Author(s):  
V.A. Valitov ◽  
B.P. Bewlay ◽  
Sh. Kh. Mukhtarov ◽  
O.A. Kaibyshev ◽  
M.F.X. Gigliotti

AbstractThis paper will describe the generation of micro- and sub-microcrystalline structures in two Ni-based alloys that are typically strengthened by phases, such as γ′ and γ″+δ. The relationship between the superplastic behavior and microstructure will be discussed. High strain deformation processing in the temperature range of 0.9 Tm to 0. 6Tm results in reduction of the initial coarse-grained structure (>100 µm) to a range of structures including microcrystalline (MC) (grain size <10 µm) and sub-microcrystalline (SMC) (grain size <1 µm) with increasing deformation. The influence of alloy chemistry and constituent phases on dynamic and static recrystallization is considered, and their effect on grain refinement is described. Low-temperature and high strain rate superplasticity can be observed in dispersionstrengthened alloys with SMC structures. It was established that in dispersion-hardened Ni alloys with SMC structures, superplasticity can be observed at temperatures 200-250°C lower than in alloys with MC structure.


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