Effects of Rare Earth on Microstructure and Mechanical Properties of Al-3.2Mg Alloy

2015 ◽  
Vol 817 ◽  
pp. 192-197
Author(s):  
Xin Zhang ◽  
Ze Hua Wang ◽  
Ze Hua Zhou ◽  
Jian Ming Xu ◽  
Zhao Jun Zhong ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Grain Size ◽  
Tensile Strength ◽  
Rare Earth ◽  
Second Phase ◽  
Phase Precipitation ◽  
X Ray ◽  
Scanning Electron

A series of Al-3.2Mg alloys with addition of 0~1.6 wt.% rare earth (Ce and La) were prepared. The microstructure of as-cast Al-3.2Mg alloys was investigated by optical microscopy (OM), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), and the tensile strength was measured. The results indicated that the addition of rare earth elements refined grain size and secondary dendrite arm spacing (SDAS), and the tensile strength was affected by means of the second-phase precipitation and the grain boundary. Accordingly, the ductility of Al-3.2Mg alloys reduced with the increasing of RE addition due to the more second-phase formation.

Effect of Rare Earth Er on Microstructure and Mechanical Properties of Cast Al-Si-Mg Alloy

2017 ◽  
Vol 893 ◽  
pp. 202-206 ◽  
Author(s):  
Qing Lin Li ◽  
Bin Qiang Li ◽  
Jin Bao Li ◽  
Chao Fen Zhang ◽  
Ye Feng Lan
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Rare Earth ◽  
Electron Probe ◽  
Mg Alloy ◽  
Chinese Script ◽  
Eutectic Si ◽  
Scanning Electron

It is well known that Al-Si-Mg alloy can form Chinese script eutectic Mg2Si and large blocky primary Mg2Si phases. In this paper, the microstructures and mechanical properties of cast Al-18Si-10Mg-xEr (x=0, 0.3, 0.5, 0.8 and 1.0 wt.%) alloy were investigated. The as-cast samples were characterized by optical microscopy (OM), scanning electron microscopy (SEM) and electron probe microanalysis (EPMA) with wavelength dispersive spectroscopic (WDS). The results show that the morphology of primary Mg2Si changed from large block or Chinese script-like to fine block with increasing of Er contents from 0.3% to 1.0%., and the morphology of eutectic Si phases transformed into fine coral-like fibrous structure and the size of eutectic Si dramatically decrease. The mechanical properties were researched by tester with different concentration of rare earth Er. It was found that the ultimate tensile strength and hardness increased by 32.1% and 21.4%, respectively.

scholarly journals Investigating the Effect of Counter Gravity Mold Filling on Microstructure and Mechanical Properties of Cast Aluminium

2020 ◽  
Vol 5 (3) ◽  
pp. 497-506
Author(s):  
Vineet Chak ◽  
Himadri Chattopadhyay ◽  
Md. Mahfooz Alam
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Mold Cavity ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cast Aluminium ◽  
Cavity Filling ◽  
Scanning Electron

In present study an effort has been made to investigate the effect of changing the mode of mold cavity filling on mechanical properties and microstructure of cast aluminium. The pouring of the melt in mold cavity is avoided so as to check defects associated with it and instead of pouring, counter gravity filling of mold technique is utilized. The obtained properties and microstructure are compared with gravity poured (traditionally cast) aluminium. Characterization techniques like optical microscopy, scanning electron microscopy, X-Ray diffraction and mechanical testing like tensile and hardness of the cast samples is carried out. Hardness and tensile strength reported an increment of 22.37% and 26.71% respectively as compared to traditionally cast specimens. This enhancement in mechanical properties was attributed to improved microstructure obtained.

scholarly journals Effect of (Pr+Ce) Additions on Microstructure and Mechanical Properties of AlSi5Cu1Mg Alloy

2019 ◽  
Vol 9 (9) ◽  
pp. 1856
Author(s):  
Miao-Miao Fang ◽  
Hong Yan ◽  
Xian-Chen Song ◽  
Yong-Hui Sun
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Rare Earth ◽  
Ultimate Tensile Strength ◽  
Microstructure And Mechanical Properties ◽  
Eutectic Si ◽  
The Mean ◽  
Scanning Electron

The microstructure and mechanical properties of AlSi5Cu1Mg alloy with (Pr+Ce) addition were investigated by optical microscopy (OM), energy dispersive spectroscopy (EDS), and scanning electron microscopy (SEM). The results demonstrated that the rare earth (Pr+Ce) addition refined the grain. The long needle-like eutectic Si phases turned to granual. The secondary dendrite arm spacing (SADS) of the primary α-Al phase with the AlSi5Cu1Mg+0.6 wt.% (Pr+Ce) alloy reached the minimum value, which decreased by 50.2%. The mean length and the aspect ratio of the eutectic Si decreased by 78.8% and 67.4%. The ultimate tensile strength (UTS), the microhardness, and the breaking elongation of the AlSi5Cu1Mg+0.6 wt.% (Pr+Ce) alloy reached a maximum, and increased by 21.5%, 21.7%, and 8.0% compared to the AlSi5Cu1Mg alloy. The fracture examinations manifested in cleaved surfaces and brittle fracture areas, which were seen from the AlSi5Cu1Mg+0.6 wt.% (Pr+Ce) alloy. The number of dimples slightly increased.

scholarly journals STRUCTURES AND PROPERTIES OF NATURAL RUBBER/ORGANOCLAY NANOCOMPOSITES

2011 ◽  
Vol 14 (1) ◽  
pp. 30-38
Author(s):  
Hien Quang Pham ◽  
Son Thanh Thanh Do ◽  
Nieu Huu Nguyen
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Natural Rubber ◽  
Abrasion Resistance ◽  
X Ray Diffraction ◽  
X Ray ◽  
Structures And Properties ◽  
Scanning Electron

Natural rubber (NR), 30% epoxidized natural rubber (ENR30) and organoclays (Nanomer I28E and I30E) are blended in Brabender. Dispersions of the organoclay in NR are investigated by X – ray diffraction (XRD) and scanning electron microscopy (SEM). The results revealed the increase of dispersion efficiency by the addition of ENR30 as a compatibilizer. The existence of organoclay I28E reduces the vulcanization time, while torque value increases slightly and mechanical properties (abrasion resistance, modulus M100, modulus M300, tensile strength, tear strength) are improved considerably.

Investigation on the Microstructure and Mechanical Properties of New Al-Si Piston Alloys

2012 ◽  
Vol 445 ◽  
pp. 289-294 ◽  
Author(s):  
S.G. Shabestari ◽  
R. Gholizadeh
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Thermal Analysis ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Chemical Composition ◽  
Optical Microscopy ◽  
The Other ◽  
X Ray ◽  
Scanning Electron

Dense precipitation of various intermetallic compounds is a common feature in the microstructure of Al-Si piston alloys. In this investigation, microstructure of LM13 alloy and three high Cu-containing Al-Si piston alloys with different amounts of Ni, Fe, and Mn were studied by means of optical microscopy (OM) and scanning electron microscopy (SEM). Chemical composition of the phases was determined by using energy dispersive X-ray analysis (EDX). The precipitation of the phases was studied through thermal analysis of the solidifying samples. Also, tensile properties and hardness of the samples were measured. The results showed that the various intermetallics such as Al12(FeMn)3Si2, Al3Ni, Al9FeNi, and Al3CuNi precipitated during the solidification. The high Cu-containing alloy with optimum levels of Ni (1.8 wt.%), Fe (0.75 wt.%), and Mn (0.3 wt.%) has the highest tensile strength (250 MPa) and hardness (110 BHN) among the other alloys.

scholarly journals Analysis of PLA Composite Filaments Reinforced with Lignin and Polymerised-Lignin-Treated NFC

Polymers ◽  
2021 ◽  
Vol 13 (13) ◽  
pp. 2174
Author(s):  
Diana Gregor-Svetec ◽  
Mirjam Leskovšek ◽  
Blaž Leskovar ◽  
Urška Stanković Elesini ◽  
Urška Vrabič-Brodnjak
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Glassy State ◽  
Nanofibrillated Cellulose ◽  
Dynamic Mechanical Properties ◽  
Initial Modulus ◽  
Surface Modified ◽  
Scanning Electron

Polylactic acid (PLA) is one of the most suitable materials for 3D printing. Blending with nanoparticles improves some of its properties, broadening its application possibilities. The article presents a study of composite PLA matrix filaments with added unmodified and lignin/polymerised lignin surface-modified nanofibrillated cellulose (NFC). The influence of untreated and surface-modified NFC on morphological, mechanical, technological, infrared spectroscopic, and dynamic mechanical properties was evaluated for different groups of samples. As determined by the stereo and scanning electron microscopy, the unmodified and surface-modified NFCs with lignin and polymerised lignin were present in the form of plate-shaped agglomerates. The addition of NFC slightly reduced the filaments’ tensile strength, stretchability, and ability to absorb energy, while in contrast, the initial modulus slightly improved. By adding NFC to the PLA matrix, the bending storage modulus (E’) decreased slightly at lower temperatures, especially in the PLA samples with 3 wt% and 5 wt% NFC. When NFC was modified with lignin and polymerised lignin, an increase in E’ was noticed, especially in the glassy state.

Research on compatibility and surface of high impact bio-based polyamide

2021 ◽  
pp. 095400832110055
Author(s):  
Yang Wang ◽  
Yuhui Zhang ◽  
Yuhan Xu ◽  
Xiucai Liu ◽  
Weihong Guo
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Differential Scanning Calorimetry ◽  
Crystallization Behavior ◽  
High Impact ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Scanning Electron

The super-tough bio-based nylon was prepared by melt extrusion. In order to improve the compatibility between bio-based nylon and elastomer, the elastomer POE was grafted with maleic anhydride. Scanning Electron Microscopy (SEM) and Thermogravimetric Analysis (TGA) were used to study the compatibility and micro-distribution between super-tough bio-based nylon and toughened elastomers. The results of mechanical strength experiments show that the 20% content of POE-g-MAH has the best toughening effect. After toughening, the toughness of the super-tough nylon was significantly improved. The notched impact strength was 88 kJ/m2 increasing by 1700%, which was in line with the industrial super-tough nylon. X-ray Diffraction (XRD) and Differential Scanning Calorimetry (DSC) were used to study the crystallization behavior of bio-based PA56, and the effect of bio-based PA56 with high crystallinity on mechanical properties was analyzed from the microstructure.

scholarly journals Effect of Annealing Process on the Mechanical Properties of X70 Pipeline Steel

2018 ◽  
Vol 186 ◽  
pp. 02001
Author(s):  
Teng-wei Zhu ◽  
Cheng-liang Miao ◽  
Zheng Cheng ◽  
Zhipeng Wang ◽  
Yang Cui ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Tensile Strength ◽  
Annealing Temperature ◽  
Pipeline Steel ◽  
Annealing Process ◽  
X70 Pipeline Steel ◽  
Grain Sizes ◽  
Scanning Electron

The influence of the mechanical properties of X70 pipeline steel under different annealing temperature was studied. The corresponding microstructure was investigated by the Field Emission Scanning Electron Microscopy. The results showed that the yield strength and the tensile strength both experienced from rise to decline with the increase of annealing temperature. The grain sizes were coarse and a large amount of cementite precipitated due to preserving temperature above 550 °, which induced matrix fragmentation and deteriorate the -10 ° DWTT Toughness. There were little changes on the microstructure and mechanical properties when the annealing temperature was under 500 °.

The Synthesis of Cu0.81Ni0.19 Intermetallics by Mechanical Alloying

2012 ◽  
Vol 496 ◽  
pp. 379-382
Author(s):  
Rui Song Yang ◽  
Ming Tian Li ◽  
Chun Hai Liu ◽  
Xue Jun Cui ◽  
Yong Zhong Jin
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Grain Size ◽  
Mechanical Alloying ◽  
Milling Time ◽  
Elemental Powder ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scherrer Equation ◽  
Scanning Electron

The Cu0.81Ni0.19 has been synthesized directly from elemental powder of nickel and copper by mechanical alloying. The alloyed Cu0.81Ni0.19 alloy powders are prepared by milling of 8h. The grain size calculated by Scherrer equation of the NiCu alloy decreased with the increasing of milling time. The end-product was analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM)

UTILIZATION OF FLY ASH AND CONCRETE RESIDUE IN THE PRODUCTION OF GEOPOLYMER BRICKS

2017 ◽  
Vol 12 (1) ◽  
pp. 63-77 ◽  
Author(s):  
Siriporn Sirikingkaew ◽  
Nuta Supakata
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Compressive Strength ◽  
Phase Composition ◽  
Fly Ash ◽  
Industrial Waste ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

This study presents the development of geopolymer bricks synthetized from industrial waste, including fly ash mixed with concrete residue containing aluminosilicate compound. The above two ingredients are mixed according to five ratios: 100:0, 95:5, 90:10, 85:15, and 80:20. The mixture's physico-mechanical properties, in terms of water absorption and the compressive strength of the geopolymer bricks, are investigated according to the TIS 168-2546 standard. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) analyses are used to investigate the microstructure and the elemental and phase composition of the brick specimens. The results indicate that the combination of fly ash and concrete residue represents a suitable approach to brick production, as required by the TIS 168–2546 standard.

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