Effect of Sn Addition on Superplastic Properties of Zn-22mass%Al Eutectoid Alloy

2016 ◽  
Vol 838-839 ◽  
pp. 518-522 ◽  
Author(s):  
Takaomi Itoi ◽  
Fumiyasu Sato ◽  
Yuki Takabayashi ◽  
Mitsuji Hirohashi

Superplastic behavior of a Zn 22 mass % Al eutectoid alloy (SPZ) with small addition of Sn (SPZSn) was investigated. Granular grain size of about 0.3 μm was obtained by water quench after annealing SPZ and SPZ05Sn (addition of 0.05 mass % Sn into the SPZ) at 653 K for 2 h. The fundamental microstructure of the SPZ05Sn was similar to that of the SPZ, but, microstructure observation by STEM showed additive Sn was present at the α’ grain boundary in the SPZ05Sn. Excellent high strain rate superplasticity was achieved in the SPZ05Sn, with elongation of more than 1300 % at 523 K at strain rate of 10-1 S-1. Furthermore, large elongation of about 1100 % was recorded at 473 K at strain rate of 10-1 S-1. The large elongation and high strain rate sensitivity value of the SPZ05Sn tend to shift to higher strain rate region as compared to those of the SPZ. It was considered that the small addition of Sn into the SPZ effectively suppressed the grain growth of α and β phase during the superplastic deformation, because granular grains less than 2 μm is maintained after superplastic deformation at 523 K.

2007 ◽  
Vol 551-552 ◽  
pp. 481-486
Author(s):  
Yoshinobu Motohashi ◽  
H. Ishimura ◽  
Y. Kobayashi ◽  
Takaaki Sakuma

The 4mol%Sc2O3 doped ZrO2 (4ScSZ) showed a superplastic-like large elongation in a range of strain-rate at 1773K. The large elongation was caused by both of high strain-rate sensitivity and high strain hardening during the deformation. Ion conductivity of the 4ScSZ, deformed superplastically at a relatively high strain-rate region, was higher than that of non-deformed one, suggesting that superplastic deformation can improve its conductivity. These results are discussed with probable microstructural evolution.


2004 ◽  
Vol 471-472 ◽  
pp. 692-696
Author(s):  
Xiao Jing Xu ◽  
Lan Cai ◽  
Seock Sam Kim

An ingot aluminum alloy (Al-Cu-Mg-Ti-Sr) with high strength and high strain rate superplasticity has been successfully developed through a conventional manufacture route consisting of casting, heat treatment, hot extrusion with a low extrusion rate of only 10:1, hot-rolling and further cold-rolling, which is cost effective and suitable for large volume production industries. The tensile test result showed the alloy possesses not only a high ultimate strength of 513.85MPa at room temperature, but also a good high strain rate superplasticity with the tensile elongation of 174~224%, the flow stress of 17.1~33.9MPa and the strain rate sensitivity m-value of 0.174~0.293 in the initial strain rate of 3.16×10-2~1.0×10-1s-1 and at the temperature of 748K~793K. Differential scanning calorimeter (DSC) analysis showed that the superplastic deformation has no relationship with liquid phase. Scanning electron microscopy (SEM) analysis of fracture surface and surface showed that the superplastic deformation results from fine grain boundary sliding and dislocation slip.


2008 ◽  
Vol 584-586 ◽  
pp. 164-169 ◽  
Author(s):  
Krystof Turba ◽  
Premysl Malek ◽  
Edgar F. Rauch ◽  
Miroslav Cieslar

Equal-channel angular pressing (ECAP) at 443 K was used to introduce an ultra-fine grained (UFG) microstructure to a Zr and Sc modified 7075 aluminum alloy. Using the methods of TEM and EBSD, an average grain size of 0.6 1m was recorded after the pressing. The UFG microstructure remained very stable up to the temperature of 723 K, where the material exhibited high strain rate superplasticity (HSRSP) with elongations to failure of 610 % and 410 % at initial strain rates of 6.4 x 10-2 s-1 and 1 x 10-1 s-1, respectively. A strain rate sensitivity parameter m in the vicinity of 0.45 was observed at temperatures as high as 773 K. At this temperature, the material still reached an elongation to failure of 430 % at 2 x 10-2 s-1. These results confirm the stabilizing effect of the Zr and Sc additions on the UFG microstructure in a 7XXX series aluminum alloy produced by severe plastic deformation.


Metals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1153
Author(s):  
Ping Song ◽  
Wen-Bin Li ◽  
Yu Zheng ◽  
Jiu-Peng Song ◽  
Xiang-Cao Jiang ◽  
...  

This study investigated the deformation behavior of the Mo-10Ta alloy with a strain rate range of 102–105 s−1. The Split Hopkinson pressure bar (SHPB) experiments were conducted to investigate the influence of deformation conditions on the stress-strain relationship and strain rate sensitivity of the material within a strain rate range of 0.001–4500 s−1. The Shaped Charge Jet (SCJ) forming experiments under detonation loading was conducted to clarify the dynamic response and microstructure evolution of the material within an ultra-high strain rates range of 104–105 s−1. Based on the stress-strain relationship of Mo-10Ta alloy at high temperature (286–873 K) and high strain rate (460–4500 s−1), the influence of temperature and strain rate on the activation energy Q was analyzed. The results indicate that the material strain rate sensitivity increased with the increase in strain rate and strain. Meanwhile, the activation energy Q decreased as the temperature and strain rate increased. The plasticity of the Mo-10Ta alloy under the condition of SCJ forming was substantially enhanced compared with that under quasi-static deformation. The material grain was also refined under ultra-high strain rate, as reflected by the reduction in grain size from 232 μm to less than 10 μm.


Materials ◽  
2020 ◽  
Vol 13 (9) ◽  
pp. 2098 ◽  
Author(s):  
Olga Yakovtseva ◽  
Maria Sitkina ◽  
Ahmed O. Mosleh ◽  
Anastasia Mikhaylovskaya

Increasing the strain rate at superplastic forming is a challenging technical and economic task of aluminum forming manufacturing. New aluminum sheets exhibiting high strain rate superplasticity at strain rates above 0.01 s−1 are required. This study describes the microstructure and the superplasticity properties of a new high-strength Al-Zn-Mg-based alloy processed by a simple thermomechanical treatment including hot and cold rolling. The new alloy contains Ni to form Al3Ni coarse particles and minor additions of Zr (0.19 wt.%) and Sc (0.06 wt.%) to form nanoprecipitates of the L12-Al3 (Sc,Zr) phase. The design of chemical and phase compositions of the alloy provides superplasticity with an elongation of 600–800% in a strain rate range of 0.01 to 0.6/s and residual cavitation less than 2%. A mean elongation-to-failure of 400% is observed at an extremely high constant strain rate of 1 s−1. The strain-induced evolution of the grain and dislocation structures as well as the L12 precipitates at superplastic deformation is studied. The dynamic recrystallization at superplastic deformation is confirmed. The superplastic flow behavior of the proposed alloy is modeled via a mathematical Arrhenius-type constitutive model and an artificial neural network model. Both models exhibit good predictability at low and high strain rates of superplastic deformation.


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