Microstructure and Mechanical Properties of In Situ Cast Aluminum Based Composites Reinforced with TiC Nano-Particles

2020 ◽  
Vol 985 ◽  
pp. 211-217
Author(s):  
Wojciech Maziarz ◽  
Piotr Bobrowski ◽  
Anna Wójcik ◽  
Agnieszka Bigos ◽  
Łukasz Szymański ◽  
...  

This work concerns microstructure and mechanical properties investigations of aluminum based composite strengthened with the TiC particles being in nanometer size. The composites were fabricated by the casting method combined with in-situ formation of TiC particles. Applying a suitable composition of components and moderators of SHS reaction which occur during casting, it was possible to cast the samples with TiC particles of size of 150 nm and faceted shape. Microstructure investigations using scanning and transmission electron microscopy (SEM and TEM) allowed to identified the distribution of TiC particles and their preferred location in the microstructure of composites. Also the additional precipitates with different size and shape were identified in investigated samples. Significant increase of strength was observed in in-situ cast composites in comparison to Al-1000 alloy mainly due mainly due to coefficient of thermal expansion and elastic modulus mismatch between the reinforcements and the metal matrix, Hall-Pecht relation and also in minority the Orowan effect.

2016 ◽  
Vol 87 (11) ◽  
pp. 1389-1394 ◽  
Author(s):  
Yawei Niu ◽  
Hao Tang ◽  
Yanlin Wang ◽  
Xiaohua Chen ◽  
Zidong Wang ◽  
...  

Author(s):  
Ege A Diler

The effects of volume fraction, size, and type of reinforcement particles on the microstructure and mechanical properties of Al–Si–Cu–(Fe) alloy matrix composites were investigated and an analytical model was modified to predict the yield strength of the particle-reinforced nanocomposites. Nano- and micro-particle-reinforced Al–Si–Cu-(Fe) matrix composites (N-AMCs and M-AMCs) were manufactured by adding two different types and sizes of reinforcement particles to Al–Si–Cu–(Fe) alloys at different volume fractions using a two-step stir casting method combined with a high-energy ball milling process and a high-pressure die-casting method. Microstructural analyzes of N-AMCs and M-AMCs were performed using SEM, EDX, and XRD. The Brinell hardness test and the tensile test were carried out to determine the mechanical properties of the N-AMCs and M-AMCs. The hardness of the N-AMCs and M-AMCs was continuously enhanced by increasing the volume fraction of the reinforcement particles, while the yield strength and ultimate tensile strength of the N-AMCs and M-AMCs were improved up to 1.5 vol.% and 4 vol.% of nano-particles and micro-particles, respectively. An analytical model was modified to predict the yield strength of N-AMCs by integrating the effective volume ratio of nano-particles into each strengthening mechanism. The results predicted by the modified model reached nearly 98% agreement with the experimental results up to 1.5 vol.% of the reinforcement particles. Nano-particles had a much greater effect on strengthening mechanisms compared to micro-particles.


2003 ◽  
Vol 778 ◽  
Author(s):  
Rajdip Bandyopadhyaya ◽  
Weizhi Rong ◽  
Yong J. Suh ◽  
Sheldon K. Friedlander

AbstractCarbon black in the form of nanoparticle chains is used as a reinforcing filler in elastomers. However, the dynamics of the filler particles under tension and their role in the improvement of the mechanical properties of rubber are not well understood. We have studied experimentally the dynamics of isolated nanoparticle chain aggregates (NCAs) of carbon made by laser ablation, and also that of carbon black embedded in a polymer film. In situ studies of stretching and contraction of such chains in the transmission electron microscope (TEM) were conducted under different maximum values of strain. Stretching causes initially folded NCA to reorganize into a straight, taut configuration. Further stretching leads to either plastic deformation and breakage (at 37.4% strain) or to a partial elastic behavior of the chain at small strains (e.g. 2.3% strain). For all cases the chains were very flexible under tension. Similar reorientation and stretching was observed for carbon black chains embedded in a polymer film. Such flexible and elastic nature of NCAs point towards a possible mechanism of reinforcement of rubber by carbon black fillers.


2021 ◽  
Vol 212 ◽  
pp. 108681
Author(s):  
Diqiang Liu ◽  
Aijun Zhang ◽  
Jiangang Jia ◽  
Jiesheng Han ◽  
Junyan Zhang ◽  
...  

Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 422
Author(s):  
Kuai Zhang ◽  
Yungang Li ◽  
Hongyan Yan ◽  
Chuang Wang ◽  
Hui Li ◽  
...  

An Fe/FeAl2O4 composite was prepared with Fe-Fe2O3-Al2O3 powder by a hot press sintering method. The mass ratio was 6:1:2, sintering pressure was 30 MPa, and holding time was 120 min. The raw materials for the powder particles were respectively 1 µm (Fe), 0.5 µm (Fe2O3), and 1 µm (Al2O3) in diameter. The effect of sintering temperature on the microstructure and mechanical properties of Fe/FeAl2O4 composite was studied. The results showed that Fe/FeAl2O4 composite was formed by in situ reaction at 1300 °C–1500 °C. With the increased sintering temperature, the microstructure and mechanical properties of the Fe/FeAl2O4 composite showed a change law that initially became better and then became worse. The best microstructure and optimal mechanical properties were obtained at 1400 °C. At this temperature, the grain size of Fe and FeAl2O4 phases in Fe/FeAl2O4 composite was uniform, the relative density was 96.7%, and the Vickers hardness and bending strength were 1.88 GPa and 280.0 MPa, respectively. The wettability between Fe and FeAl2O4 was enhanced with increased sintering temperature. And then the densification process was accelerated. Finally, the microstructure and mechanical properties of the Fe/FeAl2O4 composite were improved.


2016 ◽  
Vol 61 (2) ◽  
pp. 761-766 ◽  
Author(s):  
A. Zieliński ◽  
M. Sroka ◽  
A. Hernas ◽  
M. Kremzer

Abstract The HR3C is a new steel for pressure components used in the construction of boilers with supercritical working parameters. In the HR3C steel, due to adding Nb and N, the compounds such as MX, CrNbN and M23C6 precipitate during service at elevated temperature, resulting in changes in mechanical properties. This paper presents the results of microstructure investigations after ageing at 650, 700 and 750 °C for 5,000 h. The microstructure investigations were carried out using scanning and transmission electron microscopy. The qualitative and quantitative identification of the existing precipitates was carried out using X-ray analysis of phase composition. The effect elevated temperature on microstructure and mechanical properties of the examined steel was described.


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