Essential Oil from Vietnamese Mandarin (Citrus reticulata Blanco) Using Hydrodistillation Extraction Process and Identification of it’s Components

2019 ◽  
Vol 298 ◽  
pp. 100-105 ◽  
Author(s):  
Thien Hien Tran ◽  
Ngo Thi Quyen ◽  
Huynh Thi Kieu Linh ◽  
Thuy Trang Le Ngoc ◽  
Phan Minh Quan ◽  
...  

In this research, the hydrodistillation extraction method has been adopted to extract the essential oil from Vietnamese Mandarin (Citrus reticulata Blanco) peel purchased from Thu Duc, Vietnam. Various extraction conditions influencing the oil yield were investigated. The obtained essential oil was evaluated for physicochemical characteristics. GC–MS studied the chemical composition of the oil. The results showed that with the ground Mandarin peel, the ratio of peel to solvent ratio 1:4 (g/mL), extraction time of 150 minutes at a temperature of 110-120°C, the highest essential oil yield was attained at 5%. Bioactive components found at high content included limonene (97.655%), were followed by β-Myrcene (1.395%), 1R-α-Pinene (0.561%), L-β-pinene (0.264%), Sabinene (0.126%).

2020 ◽  
Vol 32 (4) ◽  
pp. 965-969
Author(s):  
Ngo Thi To Quyen ◽  
Nguyen Thi Ngoc Quyen ◽  
Huynh Thi Kieu Linh ◽  
Thuy Trang Le Ngoc ◽  
Hoang Le Tuan Anh ◽  
...  

In present study, a steam distillation method has been adopted for extraction of the essential oil from Vietnamese lemon (Citrus aurantifolia) peel harvested from Tien Giang Province, Vietnam. Various extraction conditions influencing the oil yield were investigated. The resulting essential oil was evaluated for physico-chemical characteristics and antibacterial activities. The chemic al composition of oil was investigated by GC-MS. The results showed that with grinded lemon peel, a ratio of water and lemon peels of 3:1 (mL/g), extraction time of 90 min at 120 ºC, the highest essential oil yield was attained at 2.1 %. Bioactive components found at high content included limonene (64.90 %), γ-terpinene (13.70 %), β-pinene (11.89 %), α-pinene (2.11 %), β-cymene (1.80 %) and sabinen (1.52 %). The lemon essential oil in this study was found to inhibit five bacteria strains including Staphylococcus aureus, Bacillus cereus, Escherichia coli, Salmonella enterica and Pseudomonas aeruginosa.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Huimin Zhang ◽  
Hongguang Yan ◽  
Quan Li ◽  
Hui Lin ◽  
Xiaopeng Wen

AbstractThe floral fragrance of plants is an important indicator in their evaluation. The aroma of sweet cherry flowers is mainly derived from their essential oil. In this study, based on the results of a single-factor experiment, a Box–Behnken design was adopted for ultrasound- and microwave-assisted extraction of essential oil from sweet cherry flowers of the Brooks cultivar. With the objective of extracting the maximum essential oil yield (w/w), the optimal extraction process conditions were a liquid–solid ratio of 52 mL g−1, an extraction time of 27 min, and a microwave power of 435 W. The essential oil yield was 1.23%, which was close to the theoretical prediction. The volatile organic compounds (VOCs) of the sweet cherry flowers of four cultivars (Brooks, Black Pearl, Tieton and Summit) were identified via headspace solid phase microextraction (SPME) and gas chromatography–mass spectrometry (GC–MS). The results showed that a total of 155 VOCs were identified and classified in the essential oil from sweet cherry flowers of four cultivars, 65 of which were shared among the cultivars. The highest contents of VOCs were aldehydes, alcohols, ketones and esters. Ethanol, linalool, lilac alcohol, acetaldehyde, (E)-2-hexenal, benzaldehyde and dimethyl sulfide were the major volatiles, which were mainly responsible for the characteristic aroma of sweet cherry flowers. It was concluded that the VOCs of sweet cherry flowers were qualitatively similar; however, relative content differences were observed in the four cultivars. This study provides a theoretical basis for the metabolism and regulation of the VOCs of sweet cherry flowers.


Plants ◽  
2021 ◽  
Vol 10 (7) ◽  
pp. 1397
Author(s):  
William N. Setzer ◽  
Lam Duong ◽  
Trang Pham ◽  
Ambika Poudel ◽  
Cuong Nguyen ◽  
...  

Virginia mountain mint (Pycnanthemum virginianum) is a peppermint-flavored aromatic herb of the Lamiaceae and is mainly used for culinary, medicinal, aromatic, and ornamental purposes. North Alabama’s climate is conducive to growing mint for essential oils used in culinary, confectionery, and medicinal purposes. There is, however, a need for varieties of P. virginianum that can be adapted and easily grown for production in North Alabama. Towards this end, four field-grown varieties with three harvesting times (M1H1, M1H2, M1H3; M2H1, M2H2, M2H3; M3H1, M3H2, M3H3, M4H1, M4H2, M4H3) were evaluated for relative differences in essential oil yield and composition. Thirty-day-old greenhouse-grown plants of the four varieties were transplanted on raised beds in the field at the Alabama A & M University Research Station in North Alabama. The plots were arranged in a randomized complete block with three replications. The study’s objective was to compare the four varieties for essential oil yield and their composition at three harvest times, 135, 155, and 170 days after planting (DAP). Essential oils were obtained by hydrodistillation with continuous extraction with dichloromethane using a Likens–Nickerson apparatus and analyzed by gas chromatographic techniques. At the first harvest, the essential oil yield of the four varieties showed that M1H1 had a yield of 1.15%, higher than M2H1, M3H1, and M4H1 with 0.91, 0.76, and 1.03%, respectively. The isomenthone concentrations increased dramatically through the season in M1 (M1H1, M1H2, M1H3) by 19.93, 54.7, and 69.31%, and M3 (M3H1, M3H2, M3H3) by 1.81, 48.02, and 65.83%, respectively. However, it increased only slightly in M2 and M4. The thymol concentration decreased slightly but not significantly in all four varieties; the thymol in M2 and M4 was very high compared with M1 and M3. The study showed that mountain mint offers potential for production in North Alabama. Two varieties, M1 and M3, merit further studies to determine yield stability, essential oil yield, composition, and cultivation development practices.


2002 ◽  
Vol 14 (4) ◽  
pp. 243-246 ◽  
Author(s):  
Katja S. Rissanen ◽  
Abbas Aflatuni ◽  
Päivi H. Tomperi ◽  
Jorma E. Jalonen ◽  
Kari M. Laine

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