scholarly journals The influence of air temperature for solvent evaporation on bonding of self-etch adhesives to dentin

2014 ◽  
Vol 08 (02) ◽  
pp. 205-210 ◽  
Author(s):  
Sandra Kiss Moura ◽  
Cintia Gaio Murad ◽  
Alessandra Reis ◽  
Celso Afonso Klein-Júnior ◽  
Rosa Helena Miranda Grande ◽  
...  
Keyword(s):  
Bond Strength ◽  
Silver Nitrate ◽  
Air Temperature ◽  
Nitrate Uptake ◽  
Water Storage ◽  
Solvent Evaporation ◽  
Adhesive Systems ◽  
Post Hoc ◽  
Self Etch ◽  
Scanning Electron

ABSTRACT Objective: This study evaluated the effect of air temperature (warm or cold) for solvent evaporation on bonding and nanoleakage of self-etching adhesives to dentin. Materials and Methods: The adhesives Clearfil 3S Bond [S3], OptiBond All-In-One [OB], Adper SE Plus [AD], and Silorane adhesive [SI] were applied on dentin surfaces, and a warm (60 ± 2°C) or cold air (20 ± 1°C) was applied and light-cured. After water storage (24 h), the teeth were sectioned into sticks (0.8 mm2) and tested in tensile. Then, they were immersed in a 50% solution of silver nitrate, photo-developed and the nanoleakage observed in a scanning electron microscope. The bond strength and nanoleakage pattern were analyzed by two-way analysis of variance and post hoc Tukey´s test (α =0.05). Results: Higher bond strength and lower silver nitrate uptake were observed for the adhesives under warm condition (P < 0.05). AD and SI showed better adhesive results than S3 and OB (P < 0.05). Conclusion: The use of a warm air was useful to improve the bonding and diminish the nanoleakage of adhesive systems to dentin.

Interfacial Nanoleakage and Bonding of Self-Adhesive Systems Cured with a Modified-Layering Technique to Dentin of Weakened Roots

2013 ◽  
Vol 38 (5) ◽  
pp. E154-E165 ◽  
Author(s):  
E Mobarak ◽  
R Seyam
Keyword(s):  
Bond Strength ◽  
Repeated Measures ◽  
Adhesive Systems ◽  
Root Canals ◽  
Root Region ◽  
Modes Of Failure ◽  
Group A ◽  
Post Hoc ◽  
Vertise Flow ◽  
Self Etch

SUMMARY Objective The purpose of the study was to evaluate the nanoleakage and bond strength of different self adhesive systems cured with a modified-layering technique (MLT) to dentin of weakened roots. Methods Twenty-one maxillary incisors were decoronated and then root canals were instrumented and obturated with the cold lateral compaction technique. Weakened roots were simulated by flaring root canals until only 1 mm dentin thickness remained. Teeth were distributed into three groups. The canals were backfilled with Vertise Flow (VF group), a self-adhering system, following a modified-layering technique using two light-transmitting posts, sizes 6 and 3. DT Light Post size 2 was cemented using the same material. Remaining roots were prepared and cured in the same way as the VF group. However, in the TS/MF group, Clearfil Tri-S Bond (TS) adhesive and Clearfil Majesty Flow (MF) composite were used, while in the ED/PF group, ED primer II (ED)/Panavia F2.0 (PF) were used. After one week of storage, each root was sectioned to obtain six slices (two slices from each root third: coronal, middle and apical) of 0.9 ± 0.1 mm thickness. Interfacial nanoleakage expression was analyzed using a field emission scanning electron microscope (FEG-SEM), and the micro push-out bond strength (μPOBS) was measured at different root regions. Modes of failure were also determined using SEM. Data were statistically analyzed using two-way analysis of variance with repeated measures and Tukey post hoc test (p≤0.05). Results With MLT, all adhesive systems showed nanoleakage. For μPOBS, there was a statistically significant effect for adhesive systems (p&lt;0.001) but not for root region (p&lt;0.64) or for their interaction (p=0.99). Tukey post hoc test revealed that the bond strength of the VF group was significantly higher than the TS/MF and ED/PF groups for all root regions. Conclusion All of the tested self-adhesive systems cured using MLT had slight nanoleakage and were not sensitive to root regional differences. Self-adhering systems had higher bond strength than self-etch adhesives.

Effect of Different Adhesive Systems Used for Immediate Dentin Sealing on Bond Strength of a Self-Adhesive Resin Cement to Dentin

2018 ◽  
Vol 43 (4) ◽  
pp. 391-397 ◽  
Author(s):  
RC Ferreira-Filho ◽  
C Ely ◽  
RC Amaral ◽  
JA Rodrigues ◽  
J-F Roulet ◽  
...  
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Water Storage ◽  
Resin Cement ◽  
Control Group ◽  
Adhesive Systems ◽  
Adhesive Resin ◽  
Etch And Rinse ◽  
Adhesive Resin Cement ◽  
Self Etch

SUMMARY Objective: The purpose of this study was to investigate the immediate and three-month water storage behavior of adhesives when used for immediate dentin sealing (IDS). Methods and Materials: Four adhesive systems were used to perform IDS: a one-step self-etch (Xeno V), a two-step self-etch (Clearfil SE Bond), a two-step etch-and-rinse (XP Bond), and a three-step etch-and-rinse (Optibond FL). For the control group, IDS was not performed. The self-adhesive resin cement RelyX Unicem was used for the luting procedures. After seven days of water storage, specimens (n=6) were sectioned into beams (n=5) with an approximately 1-mm2 cross-sectional area. Half of the specimens were tested in tension after seven days of water storage at 37°C, while the other half was stored for three months prior to testing in tension using a universal testing machine (1 mm/min). The failure pattern was determined using a stereomicroscope and scanning electron microscopy. Microtensile bond strength (μTBS) data were statistically analyzed by two-way analysis of variance and Tukey post hoc test (α=0.05). Results: After seven days, the control group presented the lowest μTBS but did not differ from XP Bond and Clearfil SE Bond. After three months, there was no μTBS difference between the IDS groups and the control. Conclusions: After seven days of water storage, the groups with IDS presented higher μTBS values than the control group, although XP Bond and Clearfil SE Bond did not present significant differences. However, after three months of storage in water, IDS groups did not differ significantly from control group, which did not receive IDS.

scholarly journals The Use of Warm Air Stream for Solvent Evaporation: Effects on the Durability of Resin-dentin Bonds

2010 ◽  
Vol 35 (1) ◽  
pp. 29-36 ◽  
Author(s):  
A. Reis ◽  
C. A. Klein-Junior ◽  
F. H. Coelho de Souza ◽  
R. Stanislawczuk ◽  
A. D. Loguercio
Keyword(s):  
Bond Strength ◽  
Silver Nitrate ◽  
Clinical Relevance ◽  
Nitrate Uptake ◽  
Solvent Evaporation ◽  
Bonding Interface ◽  
Air Stream ◽  
Water Based ◽  
Bond Strengths ◽  
Over Time

Clinical Relevance In terms of silver nitrate uptake, the use of a warm air stream may improve bonding interface resistance to degradation over time. In terms of bond strength values, a warm air stream only improved the resin-dentin bond strengths of the ethanol/water-based system.

Effect of Bur Roughness on Bond to Sclerotic Dentin With Self-etch Adhesive Systems

2013 ◽  
Vol 38 (1) ◽  
pp. 39-47 ◽  
Author(s):  
IV Luque-Martinez ◽  
A Mena-Serrano ◽  
MA Muñoz ◽  
V Hass ◽  
A Reis ◽  
...  
Keyword(s):  
Bond Strength ◽  
Composite Resin ◽  
Relative Number ◽  
Control Group ◽  
Adhesive Systems ◽  
Tukey Test ◽  
Tensile Forces ◽  
Adhesive Application ◽  
Self Etch ◽  
Scanning Electron

ABSTRACT Purpose: To evaluate the effect of bur roughness on bond strength values and conditioner pattern of two-step self-etch adhesives applied on sclerotic dentin. Methods: The roots of 48 bovine incisors were removed and the crowns were divided into four groups: the control group (CO) teeth were left untreated or the teeth were slightly roughened with coarse-, medium-, or fine-grit diamond burs. Next, the teeth were subdivided and Clearfil SE Bond (CSE) and Adper SE Bond (ASE) were applied according to the manufacturers' instructions. Composite resin (Opallis) buildups were incrementally constructed on the bonded surfaces. After storage for 24 hours in distilled water at 37°C, the teeth were sectioned into sticks (area of 0.8 mm2). The sticks were stressed until failure by tensile forces (0.5 mm/min). Additionally, eight bovine teeth were treated as previously described, and after adhesive application, the surface was rinsed off and examined by scanning electron microscopy to measure the relative number of open tubules (OT). Data (MPa) were analyzed by two-way analysis of variance and Tukey test (p=0.05). Results: CO showed the highest bond strength values (p&lt;0.05). As regards OT, the lowest mean was observed for CO (p&lt;0.05) and the highest was found after application of CSE or ASE (p&lt;0.05).

scholarly journals Durability of bond strength to dentin using two universal adhesives in different etching modes

2021 ◽  
Vol 20 ◽  
Author(s):  
Amany A. Salem ◽  
Mohamed S. Nassif ◽  
Dalia I. El-Korashy
Keyword(s):  
Bond Strength ◽  
Water Storage ◽  
Shear Mode ◽  
Etch And Rinse ◽  
Microscopic Evaluation ◽  
Significant Difference ◽  
Universal Adhesives ◽  
Microshear Bond Strength ◽  
Self Etch ◽  
Scanning Electron

Aim. To evaluate the bond durability of two universal adhesives; mild and ultra-mild in both etch-and-rinse and self-etch modes after simulated in-vitro degradation by long-term water storage or thermocycling. Methods. A total of 144 specimens were used in this study; 120 specimens (prepared from 30 teeth) for microshear bond strength testing and fracture mode assessment, and 24 specimens for scanning electron microscopic evaluation (prepared from 24 teeth). Specimens were prepared from 54 recently extracted caries free third molars and randomly divided into 12 groups, according to the adhesive treatment (All Bond or Scotchbond Universal), etching mode (etch-andrinse or self-etch) and aging method (thermocycling or water storage). Each tooth was sectioned mesio-distally into two halves exposing free dentin surface for bonding where dentin substrate 1 mm below the dentino-enamel junction was used. After adhesive application and composite build up, specimens were tested in shear mode after storing in distilled water at 37˚C for 24 hours or 1 year, or after being thermocycled between 5 and 55 °C for 10,000 cycles (n=10). Microshear bond strength (μSBS) was tested using a universal testing machine. Adhesive-dentin interface was examined using scanning electron microscope (SEM) (n=2). Data were analyzed using 3 way AN0VA and pairwise comparisons was performed using Bonferroni correction at significance level of α ≤0.05. Results. Statistical analysis revealed non-significant difference for etching mode in both adhesives (p=0.596). After aging, the bond strength was only reduced in Scotchbond Universal after one year of water storage in both modes (p<0.001). SEM evaluation revealed intact hybrid layer and longer resin tags for etch-and-rinse mode than selfetch mode of both adhesives. Conclusion. The bond strength of universal adhesives is not affected by the etching mode, however its durability was shown to be material dependent.

scholarly journals Application Modes Affect Two Universal Adhesive Systems’ Nanoleakage Expression and Shear Bond Strength

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
A. S. Bakry ◽  
M. A. Abbassy
Keyword(s):  
Bond Strength ◽  
Silver Nitrate ◽  
Shear Bond Strength ◽  
The Self ◽  
Bonding Layer ◽  
Adhesive Systems ◽  
Hybrid Layer ◽  
Adhesive Interface ◽  
Bonding Systems ◽  
Self Etch

Objectives. The aim of this study was to evaluate the shear bond strength and the nanoleakage expression of CLEARFIL Universal Bond Quick and Tetric N-Bond adhesive systems bonded to dentin. Materials and Methods. 100 freshly extracted human premolar teeth were utilized. The teeth were sectioned to expose dentin. All dentin specimens were assigned into 4 experimental groups; 2 groups had Universal Bond Quick (Universalself group) and Tetric N-Bond (Tetricself group) applied in the self-etch mode, while 2 groups had Universal Bond Quick (Universaltotal group) and Tetric N-Bond (Tetrictotal group) applied in the total-etch mode. n = 15 for shear bond strength and n = 10 for nanoleakage experiment. One-way ANOVA and Kruskal-Wallis test were utilized to analyze the shear bond strength test and the nanoleakage expression, respectively. Results. The highest significant bond strength value was recorded by the Tetricself specimens ( p < 0.05 ) when compared to the remaining three groups. There were no statistically significant differences between the shear bond strength values recorded in the Tetrictotal, Universalself, and Universaltotal groups ( p < 0.05 ). Both bonding systems applied in the self-etch mode (Universalself, Tetricself) had no silver nitrate deposits in the hybrid layer and the hybrid layer-adhesive interface ( p < 0.001 ); however, both bonding systems applied in the total-etch mode (Universaltotal, Tetrictotal) had silver nitrate deposits in the hybrid layer, the hybrid layer-adhesive interface, and the bonding layer ( p < 0.001 ). Conclusion. Applying the Universal Bond Quick and Tetric N-Bond in the self-etch mode exhibited better results in terms of nanoleakage expression. Universal Bond Quick showed the stability of the shear bond strength to dentin when applied using the total-etch or self-etch modes. Tetric N-Bond showed significant deterioration in bond strength when applied in the total-etch mode and exhibited the highest bond strength when applied in the self-etch mode.

scholarly journals Influence of Organic Acids from the Oral Biofilm on the Bond Strength of Self-Etch Adhesives to Dentin

2015 ◽  
Vol 26 (5) ◽  
pp. 497-502 ◽  
Author(s):  
Cristiane Mariote Amaral ◽  
Danielly de Sá Correa ◽  
Luciana Meirelles Miragaya ◽  
Eduardo Moreira da Silva
Keyword(s):  
Lactic Acid ◽  
Bond Strength ◽  
Propionic Acid ◽  
Resin Composite ◽  
Water Storage ◽  
Distilled Water ◽  
Adhesive Systems ◽  
Oral Biofilm ◽  
Microtensile Bond Strength ◽  
Self Etch

Abstract: The aim of this study was to evaluate the microtensile bond strength of self-etch adhesive systems to dentin after storage in acids from oral biofilm. Three adhesive systems were used in the study: a two-step self-etch adhesive for use with a silorane-based resin composite (Filtek P90 adhesive system - P90), a two-step self-etch adhesive (Clearfil SE Bond - CSE) and a one-step self-etch adhesive (Adper Easy One - AEO). The bond strength of these products was evaluated by bonding resin composite (Filtek Z350 for CSE and AEO; and Filtek P90 for P90) to 90 bovine dentin tooth fragments, according to the manufacturer's instructions. After 24 h of water storage at 37 °C, the specimens were sectioned into beams (1 mm2) divided and stored in distilled water, lactic acid and propionic acid, for 7 and 30 days. After storage, the specimens were tested for microtensile bond strength. Data were analyzed by three-way ANOVA and Tukey´s test (α=0.05). CSE presented the highest microtensile bond strength after storage in distilled water for 7 and 30 days. The microtensile bond strength of all adhesive systems was lower after storage in lactic acid and propionic acid than after water storage. Significant difference was not found between storage times.

Degradation of Multimode Adhesive System Bond Strength to Artificial Caries-Affected Dentin Due to Water Storage

2018 ◽  
Vol 43 (2) ◽  
pp. E92-E101 ◽  
Author(s):  
AC Follak ◽  
LL Miotti ◽  
TL Lenzi ◽  
RO Rocha ◽  
FZM Soares
Keyword(s):  
Bond Strength ◽  
Repeated Measures ◽  
Water Storage ◽  
Adhesive System ◽  
Adhesive Systems ◽  
Universal Adhesive ◽  
Etch And Rinse ◽  
Influence Of Water ◽  
Microtensile Test ◽  
Post Hoc

SUMMARY The purpose of this study was to evaluate the influence of water storage on bond strength of multimode adhesive systems to artificially induced caries-affected dentin. One hundred twelve sound bovine incisors were randomly assigned to 16 groups (n=7) according to the dentin condition (sound; SND, artificially induced caries-affected dentin; CAD, cariogenic challenge by pH cycling for 14 days); the adhesive system (SU, Scotchbond Universal Adhesive; AB, All-Bond Universal; PB, Prime & Bond Elect; SB, Adper Single Bond 2; and CS, Clearfil SE Bond), and the etching strategy (etch-and-rinse and self-etch). All adhesive systems were applied under manufacturer's instructions to flat dentin surfaces, and a composite block was built up on each dentin surface. After 24 hours of water storage, the specimens were sectioned into stick-shaped specimens (0.8 mm2) and submitted to a microtensile test immediately (24 hours) or after six months of water storage. Bond strength data (MPa) were analyzed using three-way repeated-measures analysis of variance and post hoc Tukey test (α=5%), considering each substrate separately (SND and CAD). The etching strategy did not influence the bond strength of multimode adhesives, irrespective of the dentin condition. Water storage only reduced significantly the bond strength to CAD. The degradation of bond strength due to water storage was more pronounced in CAD, regardless of the etching strategy.

Durability of Enamel Bonding Using Two-step Self-etch Systems on Ground and Unground Enamel

10.2341/07-42 ◽  
2008 ◽  
Vol 33 (1) ◽  
pp. 79-88 ◽  
Author(s):  
A. D. Loguercio ◽  
S. K. Moura ◽  
A. Pellizzaro ◽  
K. Dal-Bianco ◽  
R. T. Patzlaff ◽  
...  
Keyword(s):  
Bond Strength ◽  
Clinical Relevance ◽  
Water Storage ◽  
Surface Preparation ◽  
The Self ◽  
Self Etch ◽  
Effect Of Surface

Clinical Relevance The effect of surface preparation was adhesive-dependent. Improvements in resin-enamel bond strength after enamel preparation were observed only for AdheSE and Optibond Solo plus Self-Etch Primer. Among the self-etch systems, mild, self-etch Clearfil SE Bond showed the highest bond strength values. No degradation of resin-enamel bonds was observed after 12 months of water storage, regardless of the adhesive tested.

The Effect of Dentin Desensitizer on Shear Bond Strength of Conventional and Self-adhesive Resin Luting Cements After Aging

2011 ◽  
Vol 36 (5) ◽  
pp. 492-501 ◽  
Author(s):  
B Stawarczyk ◽  
R Hartmann ◽  
L Hartmann ◽  
M Roos ◽  
M Özcan ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Water Storage ◽  
Acrylic Resin ◽  
Luting Cements ◽  
Relyx Unicem ◽  
Aging Conditions ◽  
Post Hoc ◽  
The Impact ◽  
Panavia 21

SUMMARY This study tested the impact of Gluma Desensitizer on the shear bond strength (SBS) of two conventional (RelyX ARC, Panavia 21) and two self-adhesive (RelyX Unicem, G-Cem) resin luting cements after water storage and thermocycling. Human third molars (N=880) were embedded in acrylic resin. The buccal dentin was exposed. Teeth were randomly divided into four main groups, and the following cements were adhered: 1) RelyX ARC, 2) Panavia 21, 3) RelyX Unicem, and 4) G-Cem. In half of the teeth in each group, dentin was treated with Gluma Desensitizer. In the conventional cement groups, the corresponding etchant and adhesive systems were applied. SBS of the cements was tested after 1 hour (initial); at 1, 4, 9, 16, and 25 days of water storage; and at 1, 4, 9, 16, and 25 days of thermocycling. SBS data were analyzed by one-way analysis of variance (ANOVA); this was followed by the post hoc Scheffé test and a t-test. Overall, the highest mean SBS (MPa) was obtained by RelyX ARC (ranging from 14.6 ± 3.9 to 17.6 ± 5.2) and the lowest by Panavia 21 in combination with Gluma Desensitizer (ranging from 0.0 to 2.9 ± 1.0). All tested groups with and without desensitizer showed no significant decrease after aging conditions compared with baseline values (p&gt;0.05). Only the Panavia 21/Gluma Desensitizer combination showed a significant decrease after 4 days of thermocyling compared with initial values and 1 day thermocycling. Self-adhesive cements with Gluma Desensitizer showed increased SBS after aging conditions (ranging from 7.4 ± 1.4 to 15.2 ± 3) compared with groups without desensitizer (ranging from 2.6 ± 1.2 to 8.8 ± 2.9). No cohesive failures in dentin were observed in any of the test groups. Although self-adhesive cements with and without desensitizer presented mainly adhesive failures after water storage (95.8%) and thermocyling (100%), conventional cement (RelyX ARC) showed mainly mixed failures (90.8% and 89.2%, after water storage and thermocyling, respectively). Application of the Gluma Desensitizer to dentin before cementation had a positive effect on the SBS of self-adhesive cements.

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