scholarly journals Comparison of Color Change to pH Range and Acid-Base Titration Indicator Precision Test of Multiple Ethanol Extracts

2021 ◽  
Vol 19 (1) ◽  
pp. 1446
Author(s):  
Lilis Tuslinah ◽  
Anna Yuliana ◽  
Dian Arisnawati ◽  
Lina Rahmawati Rizkuloh

Natural indicators using anthocyanin compounds can be an alternative to synthetic indicators on acid-base titration because anthocyanin is an organic compound that is unstable with changes in pH. The extraction was carried out with ethanol because the compounds of anthocyanin were polar. This study was to ensure an ethanol extract of some plants could be used as an acid-base indicator that had a pH range of color change and the value of the equality parameter was not significantly different from the phenolphthalein indicator. The research method is to collect research journals on making natural indicators from ethanol extracts of various plants compared to phenolphthalein indicators so that secondary data from these journals can be processed statistically. Research results and conclusions: Based on the results of statistical data processing using the t-test there was no difference in the average pH of the phenolphthalein indicator with the average pH of ethanol extracts of adam air leaves (Rheo discolor), white frangipani flowers and Clitoria teratea L., with a significance value > 0.05 and the equality test (precision) had the requirements of good equality. HIGHLIGHTS Natural indicators are needed as a substitute for synthetic indicators in determining acid-base titrations; one of them is anthocyanin dye Research journals on making natural indicators from ethanol extracts of various plants compared to phenolphthalein indicators so that secondary data from these journals can be processed statistically There was no significant difference between the average pH of the phenolphthalein indicator and the average pH of the ethanol extract of Adam's Eve Leaves, ethanol extracts of white Cambodia flowers and ethanol extracts of Telang flowers in producing color changes GRAPHICAL ABSTRACT

2018 ◽  
Vol 2 (3) ◽  
pp. 139 ◽  
Author(s):  
Sukemi Sukemi ◽  
Usman Usman ◽  
Boyfanie Ivan Putra ◽  
Widya Purwati ◽  
Nindy Nur Rahmawati ◽  
...  

Experiment on natural acid-base indicators is usually done by extracting the natural sources with certain solvent, testing the extract with acid, base and neutral solutions, observing the color changes, making conclusion and discharging the remaining extract at the end of the experiment. Production of long-lasting natural acid-base indicator is needed to reduce the discharged of chemicals excessively. This research was carried out to produce natural acid-base indicator from extract of shoot leaves of <em>Syzygium oleana</em> (SLS). The extraction was done by maceration technique using ethanol 95% for 13 h. The extract of SLS (SLS indicator solution) is then used to produce SLS indicator paper by soaking the filter paper in SLS indicator solution and followed by drying under shade. Both of the solution and paper indicators were tested for their color changes in pH solutions range of 1-13. Durability and performance of the indicator was investigated for 6 d. Absorbance of the indicator solution was measured under wavelength of 200-700 nm by using UV-Vis spectrophotometer. The results showed that, both of the indicators can be used as acid-base indicator; even it can be used to determine the pH range of solution. The color changes of SLS indicator in solution pH of 1-13 were pink-fade green-moss green-brown. Both of the indicators showed a good performance in their color change for 6 d of storage. Thus, the ethanol extract of SLS can be used as raw material to produce acid-base indicator.


2021 ◽  
Vol 1 (2) ◽  
pp. 176-182
Author(s):  
ENDANG RIYAYANTI

Learning Natural Sciences (IPA) is not only taught by means of lectures or memorization, but by experimental or demonstration methods, so that it is more active for students. In the experiment of acid-base solutions in science class VII SMP/MTs, natural indicators were used as a test solution to replace synthetic indicators. In addition to making students active, it also minimizes practicum costs. This experiment used leaf extracts of ornamental plants such as miana, butterfly and red purslane which were made together with students and teachers. After comparing the test results between synthetic indicators (litmus paper and phenolphthalein) with homemade natural indicators, it can be concluded that the extract can be used as an alternative to the solution test. Because there are different changes when dropped into an acid and alkaline solution. When tested the pH of the solution using the extract indicator, there was a change in the pH range in an acid solution of 3.2 and a base solution of 10.8. By observing the color change, it can be concluded that ornamental plant extracts can be used as an alternative to acid-base indicators to replace synthetic indicators. For miana the color changes from orange (acidic) – brownish yellow – light green (alkaline), red purslane from pink (acidic) – dark red to dark brown (alkaline) and butterfly from red (acid) – purple - to green (base). ABSTRAKPembelajaran Ilmu Pengetahuan Alam (IPA) tidak hanya diajarkan dengan cara ceramah atau menghafal saja melainkan dengan metode eksperimen atau demonstrasi, sehingga lebih mengaktifkan siswa. Pada percobaan larutan asam-basa dalam IPA kelas VII SMP/MTs digunakan indikator alamiah sebagai uji larutan menggantikan indikator sintetis. Selain membuat siswa aktif juga meminimalisir biaya praktiku=m. Percobaan ini digunakan ekstrak daun tanaman hias seperti miana, kupu-kupu dan krokot merah yang dibuat bersama-sama siswa dengan guru. Setelah membandingkan hasil uji antara indikator sintetis (kertas lakmus dan fenolftalein) dengan indikator alamiah buatan sendiri dapat disimpulkan bahwa ekstrak tersebut dapat digunakan sebagai alternatif untuk uji larutan. Karena terdapat perubahan yang berbeda saat diteteskan ke dalam larutan asam dan basa. Saat diuji pH larutan dengan menggunakan indikator ekstrak tersebut terdapat perubahan rentang pH dalam larutan asam 3,2 dan larutan basa 10,8. Dengan mengamati perubahan warna dapat diambil kesimpulan bahwa ekstrak tanaman hias dapat digunakan sebagai alternatif indikator asam basa menggantikan indikator sintetis. Untuk miana perubahan warna dari oranye (asam) – kuning kecoklatan – hijau muda (basa), krokot merah dari merah muda (asam) – merah tua menjadi coklat tua (basa) dan kupu-kupu dari merah (asam) – ungu - menjadi hijau (basa).


INDIAN DRUGS ◽  
2019 ◽  
Vol 56 (03) ◽  
pp. 77-79
Author(s):  
G Vambhurkar ◽  
A. Jagtap ◽  
A. Gavade ◽  
M Kengar ◽  
M Bhutkar ◽  
...  

In acid-base titration or acid-base neutralization reaction the change in color due to change pH of the solution is caused due to a third substance which is termed as acid-base indicator or pH indicator. Every indicator shows different range of colors at different pH ranges. Synthetic indicators have been widely employed as indicators in acid-base titrations; however, due to environmental pollution, availability and cost, natural compounds are best alternates. Natural pigments in plants are highly colored substances and may show sharp color changes with variation in pH. In the present study an attempt has been made to extract natural indicator from flower of Aristolochia bracteolate. The equivalence points of the titrations namely strong acid-strong base, strong acid-weak base, weak acid-strong base and weak acid weak base titrations, using flower extract of A. bracteolate were coincident with the equivalence points obtained by the synthetic indicator phenolpthalein. From the results of the study, it may be concluded that ethanolic extract of A. bracteolate flower as an indicator for acid-base titration could be effectively employed as a substitute to the synthetic acid-base indicators.


KOVALEN ◽  
2017 ◽  
Vol 3 (3) ◽  
pp. 292
Author(s):  
Khairunnisa Khairunnisa ◽  
Khairuddin Khairuddin ◽  
Dwi Juli Puspitasari

The acid-base bioindicator is an alternative substitute for the synthetic indicator. The study about ethanol extract of Ketepeng Cina crown flowers as an acid-base bioindicator source has been done. The research about utilization of ethanol extract of Ketepeng Cina crown flower was aimed to study compound group, pH range and acid-base titration which is suitable as bioindicator. This research was performed with gradual extraction by maceration method with three solvents. The results showed that ethanol extract from Ketepeng Cina crown flowers contained flavonoid, polyphenol, alkaloid, and tannin. Extract of Ketepeng Cina crown flower was yellow in acid and orange in the base with the pH range of 7-9.Keywords: Ketepeng Cina, Bioindicator, Acid-Base, Titration.


2020 ◽  
Vol 14 (01) ◽  
pp. 085-091
Author(s):  
Sedighe Sadat Hashemikamangar ◽  
Farnoosh Hoseinpour ◽  
Nazanin Kiomarsi ◽  
Mehrzad Gholampour Dehaki ◽  
Mohammad Javad Kharazifard

Abstract Objectives This study aimed to assess the effect of an optical whitening toothpaste on color stability of microhybrid, nanofilled, and microfilled composite resins and resin-modified glass ionomer (RMGI) cement in comparison of two other toothpastes. Materials and Methods In this experimental study, disc-shaped composite samples were fabricated. The samples were then polished using silicon carbide papers. Twenty-seven samples of each material were fabricated and subjected to colorimetry using a spectrophotometer. Each group of material was then divided into three subgroups for the application of conventional whitening and whitening containing blue covarine toothpastes. One operator brushed the samples with an electric soft toothbrush with circular motion twice a day, each time for 30 seconds. Colorimetry was performed at 0, 1, 7, 30, and 90 days. Statistical Analysis Two-way analysis of variance (ANOVA), one-way ANOVA, and Tukey’s honestly significant difference (HSD) test were used for statistical analysis. Results The interaction effect of type of restorative material and time on ∆E was not significant at baseline or 1 day (p > 0.05). The effect of type of toothpaste on ∆E was not significant at baseline or 1 day (p = 0.78) but the effect of type of material was significant (p < 0.05). The toothpastes had significantly different effects on ∆E of Z250 at all time points (p < 0.05) except for ∆E0–30 (p = 0.106). The toothpastes had significantly different effects on ∆E of Z350 and Gradia at all time points (p < 0.05). The same was true for RMGI except for ∆E0–7 (p = 0.43) and ∆E0–90 (p = 0.52). The majority of color changes caused by toothpastes were not clinically perceivable (∆E < 3.3), except for ∆E0–90 by the whitening toothpaste (∆E = 9), ∆E0–90 by the conventional toothpaste for Z350 (∆E = 3.9), and ∆E0–1 by the whitening toothpaste for RMGI (∆E = 3.7). Conclusion The color change of all composite samples was not clinically perceivable (<3.3) at all time points, which shows that the tested toothpastes do not cause a significant change in color of composite materials.


2018 ◽  
Vol 5 (4) ◽  
pp. 76
Author(s):  
Mone Laiz Bortoli ◽  
Cristina Von Appen ◽  
Camila Longoni ◽  
Carmen Beatriz Borges Fortes ◽  
Jefferson Tomio Sanada

Aim: This work aimed to evaluate the color stability of an acrylic resin chemically activated (ARCA) using different handling techniques, and a bisacrylic resin when exposed to different pigmentation solutions.Material and Methods: Silicon matrixes were confectioned (10x10x3mm) to be used as specimens. The groups were designed as follows: Group Pot, Group Brush, Group Manufacturer and Group Bisacrylic (n=18). Each group was exposed to three different pigmentation solutions: distilled water, coke and chlorhexidine digluconate 0.12%. Three readings were performed for each specimen using a spectrophotometer, and the evaluations were carried out in three different time. After the color reading, three averages and the standard deviation of variation were performed after 24 hours (T1), 7 days (T2) and 14 days (T3). Data were submitted to the ANOVA and 2 criteria and Tukey (P<0.05) in the statistical software SSPS 18 for Macintosh (SPSS Inc., Chicago, USA).Results: When compared the solutions in each group of material, there was no statistically significant difference, except for T3, where the group Dencor Brush and Bisacrylic demonstrated higher color variation in all the solutions, even in the control group, and the values in Chlorhexidine higher than the other, showing greater instability after 14 days.Conclusions: With the results, bisacrylic resin used as provisory prosthesis material presents greater color instability than the ARCA, when submitted to different solutions. Bisacrylic resin and Dencor Brush present significantly visible color changes in chlorhexidine solution after 14 days. All the materials in coke solution present homogeneity in the color change after 7 days exposition to the solution, with no visible color change.


2020 ◽  
Vol 9 (1) ◽  
pp. 7-15
Author(s):  
Eksari Ekasari ◽  
Purnama Ningsih

Getih sambang leaves (Hemigraphis Colorata. Hall. F) are plants that have a distinctive and unique color, namely the upper surface of the leaf is green and the bottom of the leaf is burgundy where sambang leaves contain anthocyanin compounds. Anthocyanin is the color pigment in plants that forms the basis of the use of natural indicators. This study aims to prove whether getih cucumber leaves can be used as an acid-base indicator, to determine the type of acid-base titration that is suitable for indicators of getih cucumber leaves, and to find out what the pH-changing color route of getih cucumber leaves is. The method used is extraction, namely maceration. Wee leaves are macerated by using methanol as a solvent for 24 hours. The extract was previously tested using HCl solution and NaOH solution as a test to prove the presence of anthocyanin. The results obtained in this study, getih sambang leaf extract can be used as an indicator of acid base, and also the type of acid-base titration that is suitable for use in the indicator of getih leaf extract extract precisely on the titration of strong-base strong acid, and strong weak base-acid It is best used as a substitute for the phenolphthalein indicator. In titration of strong and weak acids and bases, it is good to be used as a substitute for the indicator of methyl orange. The pH range obtained from the getih sambang leaf extract is pH 4-7 (red-purple).


2021 ◽  
Vol 11 (Suppl. 1) ◽  
pp. 81-85
Author(s):  
Firdevs Kahvecioğlu ◽  
Elçim Çoban ◽  
Hayriye Esra Ülker

Aim: The aim of this study is to evaluate the effects of whitening toothpaste applications on the color stability of different tooth-colored restorative materials (Fuji IX, GC Fuji II LC, Equia Forte, and Kerr Point 4)  Methodology: Standardized fourty disc-shaped specimens were prepared from esthetic restorative materials and polished. The baseline color values of each specimen were then measured using a spectrophotometer, according to the Commission Internationale de l'Eclairage L*, a*, and b* (CIELAB) color scale. Ten specimens from each group were then immersed in two different beverages (cherry juice and coke) for seven days. After immersion, the color value of each specimen was re-measured. Each sample was brushed with whitening toothpaste for 30 seconds using an electric toothbrush. The samples were kept in distilled water at room temperature and brushing continued twice a day for seven days. The color change value, Delta E (ΔE), was calculated. Data were analyzed by two-way ANOVA and post hoc Tukey's test. Results: When the results were evaluated, after the colored samples had been brushed with whitening toothpaste, a difference was found between the Delta E values according to the materials used (p<0.001), but no difference was found in relation to the beverages (p>0.001). When the values of the color changes were evaluated after the first brushing with whitening toothpaste and before the specimens were colored with drinks, a difference was observed in the Fuji II cola, Fuji II cherry, and Equia Forte cola groups (p<0.05). When the values of the color changes were evaluated for specimens in which brushing had been done twice a day for seven days with whitening toothpaste and before they were colored with drinks, a significant difference was observed in the Fuji II cherry and Equia Forte cola groups (p<0.05). Conclusion: Using Signal White Now whitening toothpaste for 2 min 2 times a day for seven days caused significant changes in the color of the restorative materials. The color change is dependent upon the type of restorative material that is used.   How to cite this article: Kahvecioğlu F, Çoban E, Ülker HE. The effect of optical brightening toothpaste on the color stability of esthetic restorative materials. Int Dent Res 2021;11(Suppl.1):80-4. https://doi.org/10.5577/intdentres.2021.vol11.suppl1.13   Linguistic Revision: The English in this manuscript has been checked by at least two professional editors, both native speakers of English.


bionature ◽  
2019 ◽  
Vol 19 (1) ◽  
Author(s):  
Nur R. Adawiyah Mahmud ◽  
Ihwan Ihwan ◽  
Nur Jannah

Abstract.  This study investigated a natural acid-base indicator which is extracted from plants in Kupang city. There are 14 plants that potential as a source of natural indicator for acid base titration, i.e, Kol Ungu (Brassica oleracea Capitata Group), Turi Merah flower (Sesbania grandiflora L. Pers), Belimbing Wuluh flower (Averhoa bilimbi L), Kaktus Merah fruit (Opuntia vulgaris Mill), Ruelia flower (Ruellia simplex), Flamboyan flower (Delonix regia), bugenvil flower (Bougainvillea spectabilis Willd.), Bayam Merah leaves (Amaranthus tricolor L.) Jamblang fruit (Syzygium cumini L.), Murbey fruit (Morus alba L.), Pinang fruit (Areca catechu L.), Sirih fruit (Piper betle L.), Kunyit (Curcuma longa Linn), and Nanas Kerang leaves (Rhoeo discolor). Plants extract shows a sharp color change in acid and base solution. Promising results as a natural indicator also shown in acid base titration which is have similar equivalent point to synthetic indicator. We can use these natural indicators as an alternative to synthetic indicator because they are found to be simple, very useful, cheap, easy to extract, accurate, and eco-friendly. Keywords: Plant, Natural indicator, Acid-Base


2021 ◽  
Vol 3 (2) ◽  
pp. 140-147
Author(s):  
Nana Misrochah

Through this research, it is hoped that acid-base titration learning will be more meaningful and can contribute to student creativity. PjBL model is an integrated learning that is carried out cooperatively through projects that develop student skills, so that student creativity will increase. The project given in this research is making of soap from the wrinkled oil. In the process can be attributed to the application of acid-base titration material by calculation of acid numbers and saponification numbers on the cooking oil before being processed into soap. The results of data analysis shows data significance> 0.05 which means that the data is normally distributed for pretest and posttest. The data of paired sample t-test shows that the significance obtained is 0,000 <0.05 which means that there is a significant difference between the mean value of the integrated creativity test with the acid-base titration concept before treatment is given after treatment is given. Creativity improvement were calculated using the N-Gain value resulting in an average achievement rate of 0.50 and belonging to the moderate category. Posttest results indicate that the implementation of project-based LKP is effective in improving student creativity with classically average is 81.5%.


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