FORMATION OF PHYSICAL AND MECHANICAL CHARACTERISTICS OF CARBON-CARBON MATERIALS IN ISO-STATIC TECHNOLOGY FOR PRODUCING CARBON MATRIX

Author(s):  
Sergey A. Kolesnikov ◽  
Darya S. Maximova

At certain stages of the "High Pressure-High Temperature" technology of obtaining carbon matrixes, studies were conducted to determine the level of properties of carbon-carbon structural materials during stretching, compression, and bending. The values of the modulus of elasticity were calculated from the deformation curves. The advantages of this technology are shown in the paper: constant porosity preservation in an open form, accessible for the subsequent stage of impregnation of the precursor of the carbon matrix. As a result, technically, the most efficient filling of all levels of the pore structure of carbon fibers and multidimensional structures with sizes ranging from fractions to thousands of microns is achieved. Dependences of the change in physical and mechanical properties on the porosity of the carbon matrix qualitatively changed for the three states of the composite: highly porous (lack of monolithic material); dense material (100% realization of the elastic modulus of the reinforcement); high-density material (~ 100% realization of reinforcement strength). It is shown that the strength of the composite corresponds to the notion of a "bound" and "unbound" fiber bundle according to Weibull. According to these models, the tensile strength of the carbon-carbon composite material was calculated and the results were obtained in good agreement with the experimental ones. It is established that the porosity level of ~ 0.14 and the corresponding density level of ~ 1.8 g / cm3 is the boundary for the formation of carbon-carbon composite materials with this type of carbon matrix, with the qualities of the structural material. With the provision of hydrostatic pressure in the carbonization process, there are no physical reasons for the separation of the technological scheme into "preliminary" and "finish" processes with a different set of equipment.  

Author(s):  
T. N. Antipova ◽  
D. S. Shiroyan

The system of indicators of quality of carbon-carbon composite material and technological operations of its production is proved in the work. As a result of the experimental studies, with respect to the existing laboratory equipment, the optimal number of cycles of saturation of the reinforcing frame with a carbon matrix is determined. It was found that to obtain a carbon-carbon composite material with a low cost and the required quality indicators, it is necessary to introduce additional parameters of the pitch melt at the impregnation stage.


Author(s):  
V. V. Kulakov ◽  
M. I. Pankov ◽  
V. A. Sivurova ◽  
M. S. Luchkin ◽  
A. K. Golubkov ◽  
...  

The efficiency of the pyrolytic carbon compaction process by decomposing methane in samples of a carbon-carbon composite randomly reinforced with discrete high-modulus (graphitized) carbon fibers with different densities is investigated. The analysis of the test results of samples for determining the compressive strength, determining the densities of samples after compaction with pyrocarbon and after compaction by impregnation and carbonization under pressure is carried out. Scanning electron microscopy (SEM) was used to study the structure of material samples with different initial density values.


Author(s):  
К.В. Шаньгин

Рассмотрены проблемы, возникающие при испытании на сдвиг при высоких температурах, объемно - армированных углерод - углеродных композиционных материалов, применяемых при создании ракетно-космической техники. Предложены варианты повышения точности измерения, достоверности определяемых физико-механических свойств материалов. Problems arising during shear test at high temperatures of volume - reinforced carbon - carbon composite materials used in creation of rocket and space technology are considered. Disclosed are versions of improving measurement accuracy and reliability of determined physical and mechanical properties of materials.


2018 ◽  
Vol 20 (3) ◽  
pp. 201
Author(s):  
A. Galiguzov ◽  
A. Malakho ◽  
S. Minchuk ◽  
L. Oktiabrskaia ◽  
V. Lepin

Onion-like carbon reinforced carbon-carbon composite was fabricated, and the influence of onion-like carbon (OLC) on the microstructure and mechanical and friction properties was investigated by porosity analysis, scanning electron microscopy, three-point bending test, nanoindentation test and ring-on-ring friction test. The results show that the sample containing OLC has a higher flexural strength (by 7.3%) and compressive strength (by 29.3%), hardness (by 2.1 times) and apparent density (by 1.1%) and smaller open porosity (7.9% vs 9.8%) and mesopore volume, which is confirmed by porosity analysis and is attributed to improved fiber/ matrix interface performance. The presence of OLC results in higher hardness and elastic modulus of carbon matrix under nanoindentation testing, which leads to modification of friction mechanism and a decrease in the wear rate under friction (by 3.3 times). Besides, OLC particles form self-lubricating film and show a graphitic carbon solid lubricant properties.


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