COMPARISON OF THE EFFICIENCY OF DIFFERENT DETECTORS OF THE SCANNING ELECTRONIC MICROSCOPE «MIRA-LMH» FOR STUDYING MICROSTRUCTURE OF NANOMATERIALS

На первом этапе были синтезированы объекты исследования - диоксид кремния методом Штобера, где в качестве прекурсора использовали тетраэтоксисилан, и нанокомпозит ZnO - Au золь-гель методом с использованием в качестве прекурсора 2 - водного ацетата цинка. На втором этапе, микроструктуру и морфологию полученных образцов исследовали методом растровой электронной микроскопии на сканирующем электронном микроскопе «MIRA-LMH» фирмы «Tescan» с применением как классического детектора вторичных электронов, так и дополнительных детекторов - внутрилинзового детектора вторичных электронов и детектора отраженных электронов. В результате исследований установлено, что при использовании детектора вторичных электронов получаются изображения с топографическим контрастом и практически без шумов. При использовании внутрилинзового детектора вторичных электронов создаются изображения только материального контраста, без влияния рельефа поверхности. Также использование данного детектора позволило получить высококачественные изображения с большим разрешением на расстоянии от образца 5 мм. При использовании детектора отраженных электронов с рабочим расстоянием до образца 8 мм и увеличении разрешающей способности микроскопа, полученные изображения имеют низкий контраст границ, но представляют композиционную информацию с высокой чувствительностью. Таким образом, установлено, что внутрилинзовый детектор вторичных электронов, с рабочим расстоянием до образца 5 мм, является оптимальным для получения четких изображений микроструктры поверхности наноматериалов при многократном увеличении. At the first stage, the objects of study were synthesized - silicon dioxide by the Stober method, where tetraethoxysilane was used as a precursor, and a nanocomposite ZnO - Au by the sol-gel method using the aqueous zinc acetate dihydrate as a precursor. At the second stage, the microstructure and morphology of the obtained samples were investigated by scanning electron microscopy on a «MIRA-LMH» scanning electron microscope (Tescan company) using both a classical secondary electron detector and additional detectors - intralens secondary electron detector and back-scattered electrons detector. As a result of the research, it was found that when using the secondary electron detector, practically no noise images with topographic contrast are obtained. When using the intralens secondary electron detector, images of only material contrast are created, without the influence of the surface relief. Also, the use of this detector made it possible to obtain high-quality images with a high resolution at a distance of 5 mm from the sample. When using a back-scattered electrons detector with a working distance to the sample of 8 mm and increasing the resolution of the microscope, the resulting images have low border contrast, but represent compositional information with high sensitivity. Thus, it was found that the intralens secondary electron detector with a working distance of 5 mm to the sample is optimal for obtaining clear images of the microstructure of the surface of nanomaterials at multiple magnifications.

Sequences of seismic and aseismic slip on bimaterial faults show dominant rupture asymmetry and potential for elevated seismic hazard

We perform numerical simulations of sequences of earthquake and aseismic slip on planar rate and state faults separating dissimilar material within the 2-D plane strain approximation. We resolve all stages of the earthquake cycle from aseismic slip to fast ruptures while incorporating full inertia effects during seismic event propagation. We show that bimaterial coupling results in favorable nucleation site and subsequent asymmetric rupture propagation. We demonstrate that increasing the material contrast enhances this asymmetry leading to higher slip rates and normal stress drops in the preferred rupture propagation direction. The normal stress drop, induced by the bimaterial effect, leads to strong dynamic weakening of the fault and may destabilize the creeping region on a heterogeneous rate and state fault, resulting in extended rupture propagation. Such rupture penetration into creeping patches may lead to more frequent opening of earthquake gates, causing increased seismic hazard. Furthermore, bimaterial coupling may lead to irregular seismicity pattern in terms of event length, peak slip rates,and hypocenter location, depending on the properties of the creeping patches bordering the seismogenically active part of the fault . Our results highlight robust characteristics of bimaterial interfaces that persist over long sequence of events and suggest the need for further exploration of the role of material contrast in earthquake physics and models of seismic hazard.

Bath and the Body, Bamboo and the Soul

<p>Bathing at a fundamental level is desired for two attributes cleansing the body, and cleansing the soul. Historically the act of bathing has been a combination of hot and cold water bathing; this act cleanses both the body and soul, and is seen as an enjoyable pastime for both eastern and western cultures. The priority then is to architecturally express the 'body and soul' through a careful material selection. The choice of materials reflects this, concrete and bamboo, expressing the solid (body) and the light (soul). Design precedents, material comparison, eastern and western beliefs are used to establish a rationale between the material contrast of body and soul. The location for the design reflects the natural connection between 'body and soul' in a location that references the land and water, geothermal and steam, lake and landscape. The final project includes detailing of non-penetrating fixings for the use in bamboo construction, including natural and industrial products into a public bath that compliments the body and the soul.</p>

Bath and the Body, Bamboo and the Soul

<p>Bathing at a fundamental level is desired for two attributes cleansing the body, and cleansing the soul. Historically the act of bathing has been a combination of hot and cold water bathing; this act cleanses both the body and soul, and is seen as an enjoyable pastime for both eastern and western cultures. The priority then is to architecturally express the 'body and soul' through a careful material selection. The choice of materials reflects this, concrete and bamboo, expressing the solid (body) and the light (soul). Design precedents, material comparison, eastern and western beliefs are used to establish a rationale between the material contrast of body and soul. The location for the design reflects the natural connection between 'body and soul' in a location that references the land and water, geothermal and steam, lake and landscape. The final project includes detailing of non-penetrating fixings for the use in bamboo construction, including natural and industrial products into a public bath that compliments the body and the soul.</p>

Fracture Analysis of High-Strength Screw for Highway Construction

High-strength screws represent one of the main joining or fastening components which are commonly used in the process of installation of frame constructions for information boards or signposts, relating to the traffic roads. The control of the production process may not always be a sufficient method for ensuring road safety. The backward investigation and control of the screw material processing seems to be the one of the most important procedures when there is the occurrence of any failure during the operation of the screw. This paper is mainly focused on the analysis of the failure of the high-strength screw of 10.9 grade with M diameter of 27 × 3 and a shank length of 64 mm. The mentioned and investigated screw was used as a fastener in a highway frame construction. In the paper, there is mainly the analysis of the material for a broken screw in terms of the material micropurity, the material microstructure, the surface treatment as well as chemical composition. The evaluation was based on investigation by optical microscopy, scanning electron microscopy and energy dispersive spectroscopy. Important knowledge and results were also obtained due to information on micromorphology and material contrast of the fracture surface resulting from fractographic analysis, using the method of scanning electron microscopy. In the case of the production of the high-strength screws, the tempering stands for the decisive or crucial process of heat treatment because the given process can ensure a decrease in hardness, while the required ductile properties of the material are kept and this is also reflected in the increase of strength and micromorphology of the fracture surface. From the aspect of micropurity, inclusions of critical size or distribution were not identified in the material, referring to Czech standard ČSN ISO 4967 (420471). The microstructure corresponds to tempered martensite, but the fracture surface of the broken screw was based on an intercrystalline micromechanism, which is undesirable for the given type of component. Combined with the measurement of the HV1 (Vickers hardness at a load of 1 kg) from the edge to the central area of the screw, the analysis revealed the significant drawbacks in the heat treatment of the high-strength screw.

Asymptotic approach to anti-plane dynamic problem of asymmetric three-layered composite plate

In this paper, the anti-plane shear motion of an asymmetric three-layered inhomogeneous elastic plate has been examined. An asymptotic approach is employed for the present investigation. Both the generalized and unified dispersion relations within the long-wave low-frequency range have been determined. The obtained unified dispersion relation is investigated taking into account the recently analyzed material contrast for layered plate with mixed stiff-soft layers of different material properties. Finally, we make comparison with symmetric plate being a special case of the asymmetric plate under consideration in the end.