Измерения эмиттанса газодинамического электронно-циклотронного резонансного источника ионов

Advantages of using a gasdynamic electron cyclotron ion source in a proton accelerator based compact neutron source DARIA are discussed. It is experimentally demonstrated that the gasdynamic proton source is able to provide ion beams with 100 mA current, duration from 100 microseconds and longer at repetition rate up to 1 kHz. Emittance of the ion beams produced by the gasdynamic ion source was measured using a “pepper-pot” method for two extraction electrodes geometries: “spherical” and flat parallel. It is shown that the normalized 4 rms emittance value for both electrode configurations in the range of extraction voltage from 41 t 48 kV does not exceed 2 mm mrad.

Emission Modes in Electrospray Thrusters Operating with High Conductivity Ionic Liquids

Electrospray thruster life and mission performance are strongly influenced by grid impingement, the extent of which can be correlated with emission modes that occur at steady-state extraction voltages, and thruster command transients. Most notably, we experimentally observed skewed cone-jet emission during steady-state electrospray thruster operation, which leads to the definition of an additional grid impingement mechanism that we termed “tilted emission”. Long distance microscopy was used in conjunction with high speed videography to observe the emission site of an electrospray thruster operating with an ionic liquid propellant (EMI-Im). During steady-state thruster operation, no unsteady electrohydrodynamic emission modes were observed, though the conical meniscus exhibited steady off-axis tilt of up to 15°. Cone tilt angle was independent over a wide range of flow rates but proved strongly dependent on extraction voltage. For the geometry and propellant used, the optimal extraction voltage was near 1.6 kV. A second experiment characterized transient emission behavior by observing startup and shutdown of the thruster via flow or voltage. Three of the four possible startup and shutdown procedures transition to quiescence within ∼475 μs, with no observed unsteady modes. However, during voltage-induced thruster startup, unsteady electrohydrodynamic modes were observed.

Current status of the compact 2.45 GHz ECR Ion Source at FLNR JINR

This paper describes recent results obtained with a compact 2.45 GHz ECR Ion Source at the ECR ion sources test bench. The source was tested for production of helium and hydrogen ions with different configurations of Ultra High Frequency (UHF) coupler, UHF power and frequency. At the extraction voltage about of 10 kV and UHF power about of 100 W more than 500 µA of He + ions were produced with the extraction hole of 3 mm in diameter that corresponds to the current density of 7.5mA/cm2. The future possible upgrades of the ion source are also discussed.

Development of a new high-current triode extraction system for helicon ion source: design and simulation

Three triode extraction systems are simulated by IBSimu ion optical code for Amirkabir Helicon Ion Source (AHIS). The optimized pierce and suggested parabolic electrodes are introduced for the first time in this paper. The obtained N+ beam for parabolic geometry designed for ion implantation has 66 keV energy, and 10.4 mA current. Ion beam emittance and Twiss parameters of the emittance ellipse as the function of x term index are calculated for parabolic electrode equation. The simulated triode extraction systems have been evaluated by using of optimized parameters such as the extraction voltage, gap distance, plasma electrode (PE) aperture, and ion temperature. The extraction voltage, gap distance, PE aperture, and ion temperature have been changed in the range of 58–70 kV, 35–39 mm, 4–6 mm, and 0.5–4.4 eV in the simulations, respectively.

Optimization of the flash extraction of flavonoids from the leaves ofSalix babylonicausing the response surface method and an evaluation of the leaves’ high antioxidant activity

Many biological activities ofSalix babylonicaleaves are attributed to the plants’ high total flavonoid content. Flash extraction has the advantages of high efficiency and maximum retention of the active ingredient. In this study, flash extraction was used to extract the total flavonoids, and a Box–Behnken design was used to optimize the extraction conditions for the first time. The effects of four independent variables, including ethanol concentration, extraction voltage, time, and ratio of liquid to material on flavonoid yield, was determined, and the optimal conditions for flavonoid extraction were evaluated using response surface methodology. Statistical analyses showed that the linear and quadratic terms of these four variables had significant effects. The fitted second-order model revealed that the optimal conditions consisted of an ethanol concentration of 67.91%, extraction time of 87 s, extraction voltage of 116 V and ratio of liquid to material of 42.79. Under the optimum conditions, the experimental value of 66.40±0.80% nearly coincided with that predicted by the model. In the ferric reducing antioxidant power (FRAP) and 2,2-diphenyl-1-picrylhydrazyl radical (DPPH.) assays, the extracts showed significant antioxidant and scavenging capacity for free radicals, respectively. This study helps to better exploit the resources ofSalix babylonicaleaves and provides new insights for effective extraction of flavonoids.

Homogenate Extraction of Crocins from Saffron Optimized by Response Surface Methodology

Saffron, which has many kinds of biological activities, has been widely used in medicine, cosmetics, food, and other fields of health promotion industries. Crocins are the main component of saffron (Crocus sativus L.). At present, most of the extraction methods for crocins require long time or special instruments to complete the process and some of them are not suitable for industrial production at present. In this article, homogenate extraction technology which is a convenient and efficient method was developed for crocins extraction from saffron. Firstly, the influences of extraction voltage, extraction time, ethanol concentration, and temperature on crocins yield were studied by single factor experiments; and then response surface methodology (RSM) was used to optimize levels of four variables based on the result of single factor experiments. Results showed that the optimum extraction process conditions for crocins were as follows: extraction voltage, 110 V; ethanol concentration, 70%; extraction temperature, 57°C; and extraction time, 40 s. Based on these conditions, the extraction yield of crocins can reach 22.76% which is higher than ultrasonic extraction method. Therefore, homogenate extraction is an effective way to extract crocins from saffron with higher extraction yield and shorter extraction time.