HOT DEFORMATION BEHAVIOR AND PROCESSING MAP OF A Mg-Gd-Y-Zn-Zr ALLOY

Compression tests of a Mg-13Gd-4Y-2Zn-0.5Zr alloy were carried out on a Gleeble-1500D thermo-mechanical simulator within a temperature range of 420–500 °C and strain rate of 0.001–5 s–1 so that the corresponding flow behavior was investigated. The Zener-Hollomon parameter Z was used in a hyperbolic-sine-type equation to express the relationships between the peak stress, deformation temperature and strain rate. Work hardening, dynamic recovery and dynamic recrystallization were the main characteristics affecting the plastic-deformation behaviors. The activation energy Q was calculated to be 208.2 kJ/mol and processing maps at strains of 0.3, 0.5 and 0.7 were generated based on a dynamic material model. The optimum processing parameters were obtained with a power-dissipation analysis.

Research on the Hot Deformation Behavior of the Casting NiTi Alloy

The hot deformation behavior and processing maps of the casting NiTi alloy were studied at the deformation temperature of 650–1050 °C and the strain rate of 5 × 10−3–1 s−1 by Gleeble-3800 thermal simulating tester. The variation of the strain rate sensitivity exponent m and the activation energy Q under different deformation conditions (T = 650–1050 °C, ε˙ = 0.005–1 s−1) were obtained. The formability of the NiTi alloy was the best from 800 °C to 950 °C. The constitutive equation of the casting NiTi alloy was constructed by the Arrhenius model. The processing map of the casting NiTi alloy was plotted according to the dynamic material model (DMM) based on the Prasad instability criterion. The optimal processing areas were at 800–950 °C and 0.005–0.05 s−1. The microstructure of the casting NiTi alloy was analyzed by TEM, SEM and EBSD. The softening mechanisms of the casting NiTi alloy were mainly dynamic recrystallization of the Ti2Ni phase and the nucleation and growth of fine martensite.

Hot Deformation Treatment of Grain-Modified Mg–Li Alloy

In this work, a systematic analysis of the hot deformation mechanism and a microstructure characterization of an as-cast single α-phase Mg–4.5 Li–1.5 Al alloy modified with 0.2% TiB addition, as a grain refiner, is presented. The optimized constitutive model and hot working terms of the Mg–Li alloy were also determined. The hot compression procedure of the Mg–4.5 Li–1.5 Al + 0.2 TiB alloy was performed using a DIL 805 A/D dilatometer at deformation temperatures from 250 °C to 400 °C and with strain rates of 0.01–1 s−1. The processing map adapted from a dynamic material model (DMM) of the as-cast alloy was developed through the superposition of the established instability map and power dissipation map. By considering the processing maps and microstructure characteristics, the processing window for the Mg–Li alloy were determined to be at the deformation temperature of 590 K–670 K and with a strain rate range of 0.01–0.02 s−1.

Hot Workability of Ultra-Supercritical Rotor Steel Using a 3-D Processing Map Based on the Dynamic Material Model

As a new-type of ultra-supercritical HI-IP rotor steel, X12CrMoWVNbN10-1-1 alloy steel has excellent integrative performance, which can effectively improve the power generation efficiency of the generator set. In this paper, uniaxial thermal compression tests were carried out over a temperature range of 950–1200 °C and strain rates of 0.05–5 s−1 with a Gleeble-1500D thermal simulation testing machine. Moreover, based on hot compression experimental data and the theory of processing diagrams, in combination with the dynamic material model, a three-dimensional (3-D) thermal processing map considering the effect of strain was constructed. It was concluded that optimum thermal deformation conditions were as follows: the temperature range of 1150–1200 °C, the strain rate range of 0.05–0.634 s−1. Through secondary development of the finite element (FE) software FORGE®, three-dimensional thermal processing map data were integrated into finite element software FORGE®. The distributions of instability coefficient and power dissipation coefficient were obtained over various strain rates and temperatures of the Ø 8 × 12 mm cylinder specimen by using finite element simulation. It is shown that simulation results are consistent with the microstructure photos. The method proposed in this paper, which integrates the three-dimensional processing map into the finite element software FORGE® (Forge NxT 2.1, Transvalor, Nice, France), can effectively predict the formability of X12CrMoWVNbN10-1-1 alloy steel.

Constitutive Equation and Hot Processing Map of Mg-16Al Magnesium Alloy Bars

A Gleeble-2000D thermal simulation machine was used to investigate the high-temperature hot compression deformation of an extruded Mg-16Al magnesium alloy under various strain rates (0.0001–0.1 s−1) and temperatures (523–673 K). Combined with the strain compensation Arrhenius equation and the Zener–Hollomon (Z) parameter, the constitutive equation of the alloy was constructed. The average deformation activation energy, Q, was 144 KJ/mol, and the strain hardening index (n ≈ 3) under different strain variables indicated that the thermal deformation mechanism was controlled by dislocation slip. The Mg-16Al alloy predicted by the Sellars model was characterized by a small dynamic recrystallization (DRX) critical strain, indicating that Mg17Al12 particles precipitated during the compression deformation promoted the nucleation of DRX. Hot processing maps of the alloy were established based on the dynamic material model. These maps indicated that the high Al content, precipitation of numerous Mg17Al12 phases, and generation of microcracks at low temperature and low strain rate led to an unstable flow of the alloy. The range of suitable hot working parameters of the experimental alloy was relatively small, i.e., the temperature range was 633–673 K, and the strain rate range was 0.001–0.1 s−1.

Hot Deformation Behavior of a New Al–Mn–Sc Alloy

The hot deformation behavior of a new Al–Mn–Sc alloy was investigated by hot compression conducted at temperatures from 330 to 490 °C and strain rates from 0.01 to 10 s−1. The hot deformation behavior and microstructure of the alloy were significantly affected by the deformation temperatures and strain rates. The peak flow stress decreased with increasing deformation temperatures and decreasing strain rates. According to the hot deformation behavior, the constitutive equation was established to describe the steady flow stress, and a hot processing map at 0.4 strain was obtained based on the dynamic material model and the Prasad instability standard, which can be used to evaluate the hot workability of the alloy. The developed hot processing diagram showed that the instability was more likely to occur in the higher Zener–Hollomon parameter region, and the optimal processing range was determined as 420–475 °C and 0.01–0.022 s−1, in which a stable flow and a higher power dissipation were achieved.

Extension of Experimentally Assembled Processing Maps of 10CrMo9-10 Steel via a Predicted Dataset and the Influence on Overall Informative Possibilities

Processing maps embody a supportive tool for the optimization of hot forming processes. In the present work, based on the dynamic material model, the processing maps of 10CrMo9-10 low-alloy steel were assembled with the use of two flow curve datasets. The first one was obtained on the basis of uniaxial hot compression tests in a temperature range of 1073–1523 K and a strain rate range of 0.1–100 s−1. This experimental dataset was subsequently approximated by means of an artificial neural network approach. Based on this approximation, the second dataset was calculated. An important finding was that the additional dataset contributed significantly to improving the informative ability of the assembled processing maps in terms of revealing potentially inappropriate forming conditions.

Rheological Law and Mechanism for Superplastic Deformation of Ti–6Al–4V

The behaviors of and mechanisms acting in Ti–6Al–4V alloy during low-temperature superplastic deformation were systematically studied by using a Gleeble-3800 thermocompression simulation machine. Focusing on the mechanical behaviors and microstructure evolution laws during low-temperature superplastic compression tests, we clarified the changing laws of the strain rate sensitivity index, activation energy of deformation, and grain index at varying strain rates and temperatures. Hot working images based on the dynamic material model and the deformation mechanism maps involving dislocation quantity were plotted on the basis of PRASAD instability criteria. The low-temperature superplastic compression-forming technique zone and the rheological instability zone of Ti–6Al–4V were analyzed by using hot processing theories. The dislocation evolution laws and deformation mechanisms of the grain size with Burgers vector compensation and the rheological stress with modulus compensation during the low-temperature superplastic compression of Ti–6Al–4V were predicted by using deformation mechanism maps.