The environmental fate of rare earth elements (REEs) in the Malaysian environment is limitedly known;
however, industrial emission is increasing. This study focused on the REE assessment of the surface
sediments obtained from rocky shore ecosystems along the Peninsular Malaysia coastal waters, on
deliberating interspatial variability, and on describing their partitioning. Samples were treated with
the Teflon Bomb technique, and the concentration of 14 natural REEs was measured through inductively
coupled plasma mass spectrometry (ICP-MS). Through quality control practices, the results were
verified by employing a standard reference material BCR 667. The tendency of REE distribution was
the most mutual property of particular places worldwide and in Malaysia. Among REEs present in
sediment, strong correlations were observed, which indicated REEs they behave coherently to each
other in different processes of geochemical fractionation. The contaminant metals, namely manganese,
arsenic, cadmium and copper, were strongly correlated with REEs (p < 0.01 and p < 0.05); hence,
these metals may be nonanthropogenic in origin because REEs are geogenic in origin. The enrichment
factor (EF) values of the comparative results were divided by the region-specified deficiency to minimal
enrichment in all the regions, except in the east coast region, which presented considerable enrichment,
suggesting a probability of discharge of the anthropogenic effluent. The results of the analysis
normalized to chondrite presented patterns of low atomic weight rare earth elements (LREEs)
enrichment, gradual downward pattern and depletion through high atomic weight rare earth elements
(HREEs) concentrations.