Evolution Mechanism of Differential Diagenesis Combination and Its Effect on the Reservoir Quality in the Tight Sandstone: A Case from the Lower Shihezi Formation in the Hangjinqi Area of Ordos Basin, China

The physical property heterogeneity of tight sandstones was mainly caused by complex alteration of various diagenesis combinations during burial process. However, diagenetic evolution of different diagenesis combinations which generally result in the strong difference and heterogeneity of physical property and pore structure is rarely well understood. The Middle Permian lower Shihezi Formation is one of the most important tight gas sandstone reservoirs in the Hangjinqi area of Ordos Basin, China. The reservoir heterogeneity of lower Shihezi Formation, which was caused by the differential diagenesis combination, is crucial to efficient exploration and development. Evolution mechanism of differential diagenesis combination and its effect on the reservoir quality in the tight lower Shihezi Formation sandstone in the Hangjinqi area of Ordos Basin was investigated by means of thin-section description, cathodoluminescence (CL) imaging, X-ray diffraction (XRD), scanning electron microscopy (SEM), and homogenization temperature of fluid inclusions. The lower Shihezi Formation sandstones can be divided into four diagenesis combination types according to the reservoir characteristics and diagenetic relationship. The main diagenetic sequence was mechanical compaction-chlorite rim-early pore-filling calcite cementation-dissolution-authigenic kaolinite-quartz cementation-late calcite cementation. Differential diagenesis combination was mainly controlled by the petrological characteristics, microfacies, and fault. Low content of rock fragment and high content of detrital quartz were beneficial to the compaction resistance and cementation. The moderate content of pore-filling calcite was conducive to pore space protection and feldspar dissolution. The faults control dissolution and differential diagenesis combination by influencing the migration of acid fluids. Moderate compaction-moderate cementation-moderate dissolution type (BBB type) and weak compaction-moderate cementation-strong dissolution type (CBA type) were in favour of high-quality reservoir development.

Effect of microbially induced cementation on the instability and critical state behaviours of Fraser River sand

Microbially induced calcite precipitation (MICP) is a naturally driven biological process that harnesses the natural metabolic action of bacteria to induce the precipitation of calcium carbonate and alter soil engineering properties. This paper presents the results of using MICP to improve the monotonic undrained yield and critical strengths of Fraser River sand specimens. Bacteria called “Sporosarcina ureae” are employed as a ureolytic organism to achieve MICP. The formation of calcite cementation among sand particles is confirmed using scanning electron microscopic images and X-ray compositional analysis of cemented sand clusters. The progress of MICP cementation is assessed by measuring the velocity of a shear wave (VS) traveling through the specimen. The results show that VS starts to increase just as the calcium solution is introduced into each specimen after soaking the samples with the bacterial solution. Improvement in monotonic strength of sand samples is subsequently measured in a series of direct simple shear tests. Due to the combined effects of particle cementation and densification, the sand’s undrained and drained monotonic shearing strengths are significantly enhanced.

Fluid Dynamics in a Thrust Fault Inferred from Petrology and Geochemistry of Calcite Veins: An Example from the Southern Pyrenees

Petrographic and geochemical analyses (δ18O, δ13C, 87Sr/86Sr, clumped isotopes, and elemental composition) coupled with field structural data of synkinematic calcite veins, fault rocks, and host rocks are used to reconstruct the episodic evolution of an outstanding exposed thrust zone in the Southern Pyrenees and to evaluate the fault behavior as a conduit or barrier to fluid migration. The selected thrust displaces the steeply dipping southern limb of the Sant Corneli-Bóixols anticline, juxtaposing a Cenomanian-Turonian carbonate unit against a Coniacian carbonate sequence. Successive deformation events are recorded by distinct fracture systems and related calcite veins, highlighting (i) an episodic evolution of the thrust zone, resulting from an upward migration of the fault tip (process zone development) before growth of the fault (thrust slip plane propagation), and (ii) compartmentalization of the thrust fault zone, leading to different structural and fluid flow histories in the footwall and hanging wall. Fractures within the footwall comprise three systematically oriented fracture sets (F1, F2, and F3), each sealed by a separate generation calcite cement, and a randomly oriented fracture system (mosaic to chaotic breccia), cemented by the same cements as fracture sets F1 and F2. The formation of fractures F1 and F2 and the mosaic to chaotic breccia is consistent with dilatant fracturing within the process zone (around the fault tip) during initial fault growth, whereas the formation of the latest fracture system points to hybrid shear-dilational failure during propagation of the fault. The continuous formation of different fracture systems and related calcite cementation phases evidences that the structural permeability in the footwall was transient and that the fluid pathways and regime evolved due to successive events of fracture opening and calcite cementation. Clumped isotopes evidence a progressive increase in precipitation temperatures from around 50°C to 117°C approximately, interpreted as burial increase linked to thrust sheet emplacement. During this period, the source of fluid changed from meteoric fluids to evolved meteoric fluids due to the water-rock interaction at increasing depths and temperatures. Contrary to the footwall, within the hanging wall, only randomly oriented fractures are recognized and the resulting crackle proto-breccia is sealed by a later and different calcite cement, which is also observed in the main fault plane and in the fault core. This cement precipitated from formation fluids, at around 95°C, that circulated along the fault core and in the hanging wall block, again supporting the interpretation of compartmentalization of the thrust structure. The integration of these data reveals that the studied thrust fault acted as a transverse barrier, dividing the thrust zone into two separate fluid compartments, and a longitudinal drain for migration of fluids. This study also highlights the similarity in deformation processes and mechanisms linked to the evolution of fault zones in compressional and extensional regimes involving carbonate rocks.

Diagenetic evolution of fault zones in Urgonian microporous carbonates, impact on reservoir properties (Provence – southeast France)

Microporous carbonate rocks form important reservoirs with permeability variability depending on sedimentary, structural, and diagenetic factors. Carbonates are very sensitive to fluid–rock interactions that lead to secondary diagenetic processes like cementation and dissolution capable of modifying the reservoir properties. Focusing on fault-related diagenesis, the aim of this study is to identify the impact of the fault zone on reservoir quality. This contribution focuses on two fault zones east of La Fare anticline (SE France) crosscutting Urgonian microporous carbonates. Overall, 122 collected samples along four transects orthogonal to fault strike were analyzed. Porosity values have been measured on 92 dry plugs. Diagenetic elements were determined through the observation of 92 thin sections using polarized light microscopy, cathodoluminescence, carbonate staining, SEM, and stable isotopic measurements (δ13C and δ18O). Eight different calcite cementation stages and two micrite micro-fabrics were identified. As a main result, this study highlights that the two fault zones acted as drains canalizing low-temperature fluids at their onset and induced calcite cementation, which strongly altered and modified the local reservoir properties.

Structural Diagenesis in Carbonate Rocks as Identified in Fault Damage Zones in the Northern Tarim Basin, NW China

The identification of structural diagenesis and the reconstruction of diagenetic paragenesis in fault damage zones is important for understanding fault mechanisms and fluid flow in the subsurface. Based on the examination of core and sample thin section data, we deciphered the diagenetic parasequence and their fault controls for Ordovician carbonates in the northern Tarim intracratonic basin in NW China (Halahatang area). In contrast to the uniform nature of diagenesis observed in country rocks, there is a relatively complicated style of compaction and pressure solution, multiple fracturing, and cementation and dissolution history along the carbonate fault damage zones. The relative paragenetic sequence of the structure related diagenesis suggests three cycles of fracture activities, following varied fracture enlargement and dissolution, and progressively weaker calcite cementation. These processes of structure related diagenesis are constrained to the fault damage zones, and their variation is affected by the fault activities. The results of this study suggest that the carbonate reservoir and productivity could be impacted by the structure related diagenesis locally along the fault damage zones.

Analysis of the Factors that Influence Diagenesis in the Terminal Fan Reservoir of Fuyu Oil Layer in the Southern Songliao Basin, Northeast China

The diagenesis mechanism and the physical properties of a terminal fan reservoir are determined by nuclear magnetic resonance (NMR), X-ray diffraction and scanning electron microscopy. The main provenance directions are NE and SE, and the two oppositely directed fans converge to form a small catchment basin. The mudstone color is red or purplish red, which accounts for 60% of the total rock. The sandstones are lithic-feldspar sandstones and feldspar-lithic sandstones, with a smaller quartz component relative to the adjacent sandstone formations. The reservoir mainly consists of intergranular pores (51%), intragranular pores (22%), corrosion pores (20%), micro-fractures (5%) and clay matrix pores (2%). The porosity of the reservoir is only 13%, and the throats are fine with high displacement pressure. The diagenetic processes included compaction, cementation, replacement, and dissolution, and the most influential factor on the reservoir porosity was compaction. The detrital rock cement mainly consists of clay minerals (48%), quartz (23%), carbonate (19%), feldspar (7%) and dawsonite (3%). Among them, the mixed I/S layer has the most content and the most important cementation. In addition, a small amount of dawsonite is found in the pores of the sandstone, which is a unique mineral that is related to the background of inorganic CO2. The main diagenesis factors that affected this sandstone’s porosity were compaction, early quartz overgrowth and calcite cementation, which reduced the porosity from 40% to approximately 8%. Although dissolution and fracture increased the porosity (from 8% to 26%), clay- and carbonate-mineral cementation during the late diagenesis period had a dramatic effect, forming a typical low-porosity and low-permeability reservoir.