Determination of arsenic species in oyster tissue by microwave-assisted extraction and liquid chromatography-atomic fluorescence detection

2001 ◽  
Vol 15 (8) ◽  
pp. 658-666 ◽  
Author(s):  
Marc Vilanó ◽  
Roser Rubio
Keyword(s):  
Liquid Chromatography ◽  
Fluorescence Detection ◽  
Arsenic Species ◽  
Oyster Tissue ◽  
Microwave Assisted Extraction ◽  
Atomic Fluorescence ◽  
Microwave Assisted ◽  
Assisted Extraction

scholarly journals Determination of Organochlorinated Compounds in Marine Organisms by Microwave-Assisted Extraction with Molecular Organized Systems and Liquid Chromatography with Fluorescence Detection

2002 ◽  
Vol 85 (1) ◽  
pp. 44-49
Author(s):  
Carolina Padrón Sanz ◽  
Arantza Eiguren Fernández ◽  
Zoraida Sosa Ferrera ◽  
Jose Juan Santana Rodríguez
Keyword(s):  
Liquid Chromatography ◽  
Fluorescence Detection ◽  
Soxhlet Extraction ◽  
Microwave Assisted Extraction ◽  
Chromatography Analysis ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Lauryl Ether ◽  
Microwave System

Abstract Microwave-assisted extraction methodology is used to extract different compounds from various kinds of marine solid samples, such as soils, sediments, and organisms. A new analytical method was developed to extract polychlorinated biphenyls and polychlorinated dibenzofurans by using a conventional microwave system and the nonionic surfactant, polyoxyethylene 10 lauryl ether as the extractant as a prior step to liquid chromatography analysis coupled with fluorescence detection. The method was applied to the extraction and determination of these analytes in samples of blue mussels (Mytilus galloprovincialis), cockles (Cerastoderma edule), and clams (Dosinia exoleta). Compared with the traditional Soxhlet extraction, results of the proposed method showed acceptable recovery percentages for the organochlorinated compounds under study and standard deviation values <10%.

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