Orientated crystal formation in a tungsten oxide film prepared by a sol-gel process on an amorphous quartz glass substrate

1996 ◽  
Vol 15 (13) ◽  
pp. 1149-1151 ◽  
Author(s):  
T. Nishide ◽  
F. Mizukami
Keyword(s):  
Oxide Film ◽  
Tungsten Oxide ◽  
Quartz Glass ◽  
Glass Substrate ◽  
Sol Gel ◽  
Crystal Formation ◽  
Quartz Glass Substrate ◽  
Sol Gel Process ◽  
Tungsten Oxide Film ◽  
Amorphous Quartz

Solid Phase Growth of some Metal and Metal Oxide Thin Films on Sapphire and Quartz Glass Substrates

2013 ◽  
Vol 753 ◽  
pp. 505-509
Author(s):  
Yuichi Sato ◽  
Toshifumi Suzuki ◽  
Hiroyuki Mogami ◽  
Fumito Otake ◽  
Hirotoshi Hatori ◽  
...  
Keyword(s):  
Thin Films ◽  
Quartz Glass ◽  
Glass Substrate ◽  
Solid Phase ◽  
Quartz Glass Substrate ◽  
Heteroepitaxial Growth ◽  
Phase Growth ◽  
Single Crystalline ◽  
Glass Substrates ◽  
Amorphous Quartz

Solid phase growth of thin films of copper (Cu), aluminum (Al) and zinc oxide (ZnO) on single crystalline sapphire and quartz glass substrates were tried by heat-treatments and their crystallization conditions were investigated. ZnO thin films relatively easily recrystallized even when they were deposited on the amorphous quartz glass substrate. On the other hand, Cu and Al thin films hardly recrystallized when they were deposited on the quartz glass substrate. The metal thin films could be recrystallized at only extremely narrow windows of the heat-treatment conditions when they were deposited on the single crystalline sapphire substrate. The window of the solid phase heteroepitaxial growth condition of the Al film was wider than that of the Cu film.

Synthesis and Characterization of Zn Oxide Hexagonal Nano-Pole Films on Quartz Glass Substrate

2009 ◽  
Vol 7 (1) ◽  
Author(s):  
Jie Chen ◽  
Jun Wang
Keyword(s):  
Growth Mechanism ◽  
Quartz Glass ◽  
Photoelectron Spectroscopy ◽  
Glass Substrate ◽  
Sol Gel ◽  
Layer Growth ◽  
Layer By Layer ◽  
Quartz Glass Substrate ◽  
Wurtzite Phase ◽  
X Ray

Hexagon-shaped Zn oxide nano-pole films with terraces and steps have been successfully fabricated by means of a combined approach involving sol-gel process, high-temperature heat treatment, and the hydrothermal method. The surface chemistry and morphological features of the films were characterized by means of x-ray photoelectron spectroscopy and scanning electron microcopy. All the diffraction peaks in x-ray diffraction pattern match with those of the hexagonal wurtzite phase of Zn oxide. Transmittance measurements show that the optical transmittance of the sample synthesized at 520°C on quartz glass substrate is the highest, reaching about 65% in the visible-light region. Based on the detailed structural characterization and the nucleation-growth kinetics, we find that the whole crystallization process of wurtzite Zn oxide nano-poles includes nanocatalysis and layer-by-layer growth mechanism. The present study provides an important understanding of the growth mechanism for nano-pole synthesis of Zn oxide and related materials.

PERFORMANCE OF TUNGSTEN OXIDE DOPED TITANIA via SOL-GEL PROCESS FOR PHOTO-DEGRADATION OF TRANS-CINNAMIC ACID

2016 ◽  
Vol 24 (1) ◽  
pp. 75-86
Author(s):  
Y.N. Tan ◽  
◽  
A.H.A. Malek ◽  
M.Z.A. Malek ◽  
M.T. Zainuddin ◽  
...  
Keyword(s):  
Tungsten Oxide ◽  
Cinnamic Acid ◽  
Sol Gel ◽  
Photo Degradation ◽  
Sol Gel Process ◽  
Doped Titania

Effect of Electrolyte Concentration on Electrochromic Performance of Sputtered Tungsten Oxide Film: Experiments and Simulation

2020 ◽  
pp. 137699
Author(s):  
Williams Agyei Appiah ◽  
Cyril Bubu Dzakpasu ◽  
Hyejin Lee ◽  
Hochun Lee ◽  
Yong Min Lee
Keyword(s):  
Oxide Film ◽  
Tungsten Oxide ◽  
Electrolyte Concentration ◽  
Tungsten Oxide Film

Selective formation of cubic or tetragonal zirconia thin films of transparent, with no use of metal ion stabilizer by heating molecular precursor films under mild conditions

2021 ◽  
Vol 14 (02) ◽  
pp. 2151012
Author(s):  
Natangue Heita Shafudah ◽  
Hiroki Nagai ◽  
Mitsunobu Sato
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Quartz Glass ◽  
Glass Substrate ◽  
Metal Ion ◽  
Tetragonal Zirconia ◽  
Precursor Film ◽  
Quartz Glass Substrate ◽  
Molecular Precursor ◽  
Zirconia Thin Film

Cubic or tetragonal zirconia thin films of transparent and 100 nm thickness were selectively formed on a quartz glass substrate by heat-treating the molecular precursor films involving Zr(IV) complexes of nitrilotriacetic acid, at 500[Formula: see text]C in air for 1 h. A precursor solution was prepared by a reaction of the ligand and zirconium tetrabutoxide in alcohol under the presence of butylamine. By the addition of H2O2 or H2O into the solution, the spin-coated precursor films were converted to cubic zirconia thin films by the abovementioned procedure. Further, the identical phase was produced also in the case of the electro-sprayed precursor film which was formed by an addition of H2O2 into the solution. On the other hand, the tetragonal zirconia thin film was obtained from a precursor film formed by using a solution dissolving the original Zr(IV) complex of the ligand, without H2O2 nor H2O. The crystal structure of all thin films was determined by using both the X-ray diffraction (XRD) patterns and Raman spectra. Thus, the zirconia thin films of both crystals could be facilely and selectively obtained with no use of hetero-metal ion stabilizers. The XPS spectra of the thin films show that the O/Zr ratio of the cubic phase is 1.37 and slightly larger than tetragonal one (1.29), and also demonstrate that the nitrogen atoms, which may contribute to stabilize these metastable phases at room temperature, of about 5−7 atomic% was remained in the resultant thin films. The adhesion strengths of cubic zirconia thin film onto the quartz glass substrate was 68 MPa and larger than that of tetragonal one, when the precursor films were formed via a spin coating process. The optical and surface properties of the thin films were also examined in relation to the crystal systems.

SiO2CeO2 coatings of glass substrate by sol-gel process

1997 ◽  
Vol 23 (2) ◽  
pp. 141-148 ◽  
Author(s):  
Tülay Tulun ◽  
Hilmi Akinci
Keyword(s):  
Glass Substrate ◽  
Sol Gel ◽  
Sol Gel Process

scholarly journals Anodizing of Aluminum Coated with Zirconium Oxide by a Sol-Gel Process I. Effect of Heat Treatment on the Formation of the Anodic Oxide Film

1999 ◽  
Vol 67 (12) ◽  
pp. 1243-1248 ◽  
Author(s):  
Keiji WATANABE ◽  
Masatoshi SAKAIRI ◽  
Hideaki TAKAHASHI ◽  
Katsumi TAKAHIRO ◽  
Shinji NAGATA ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Oxide Film ◽  
Zirconium Oxide ◽  
Sol Gel ◽  
Anodic Oxide ◽  
Anodic Oxide Film ◽  
Sol Gel Process
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