Effects of Heat Treatment and Severe Plastic Deformation on Microstructure, Mechanical Properties and Midsection Ultimate Strength of Shipbuilding Steel

Author(s):  
D. M. Sekban
2018 ◽  
Vol 275 ◽  
pp. 134-146
Author(s):  
Stanislav Rusz ◽  
Ondřej Hilšer ◽  
Stanislav Tylšar ◽  
Lubomír Čížek ◽  
Tomasz Tański ◽  
...  

The technology of structure refinement in materials with the aim of achieving substantial mechanical properties and maintaining the required plasticity level is becoming increasingly useful in industrial practice. Magnesium alloys are very progressive materials for utilization in practice thanks to their high strength-to-weight ratios (tensile strength/density). The presented paper analyses the effect of the input heat treatment of the AZ31 alloy on the change of structure and strength properties through the process of severe plastic deformation (SPD), which finds an increasing utilization, especially in the automotive and aviation industry. For the study of the influence of the SPD process (ECAP method) on the properties of the AZ31 alloy, two types of thermal treatment of the initial state of the structure were selected. The analysis of the structure of the AZ31 alloy was performed in the initial state without heat treatment and subsequently after heat treatment. In the next part, the influence of the number of passes on the strengthening curves was evaluated. Mechanical properties of the AZ31 alloy after ECAP were evaluated by hardness measurement and completed by structure analysis.


2012 ◽  
Vol 57 (3) ◽  
pp. 877-881 ◽  
Author(s):  
K. Wawer ◽  
M. Lewandowska ◽  
K.J. Kurzydłowski

In the present study, severe plastic deformation (SPD) processing was combined with pre- and post processing heat treatment to investigate the possibility of synergic grain size and precipitation strengthening. Samples of 7475 alloy were solution heat treated and water quenched prior to hydrostatic extrusion (HE) which resulted in a grain refinement by 3 orders of magnitude, from 70 μm to about 70 nm. The extruded samples were subsequently aged at temperatures resulting in formation of nanoprecipitates.


2014 ◽  
Vol 783-786 ◽  
pp. 842-847 ◽  
Author(s):  
Tibor Kvačkaj ◽  
Jana Bidulská

Nowadays, the strategy for improving of mechanical properties in metals is not oriented to alloying followed by heat treatment. An effective way how to improve the mechanical properties of metals is focused on the research looking for some additional structural abilities of steels. Structural refinement is one of the ways. Refinement of the austenitic grain size (AGS) carried out through plastic deformation in a spontaneous recrystallization region of austenite, formation of AGS by plastic deformations in a non-recrystallized region of austenite will be considered as potential ways for AGS refinement. After classic methods of plastic deformations, next structure refinement can be obtained by an application of severe plastic deformation (SPD) methods.


Materials ◽  
2020 ◽  
Vol 13 (5) ◽  
pp. 1116
Author(s):  
Alena Michalcová ◽  
Dalibor Vojtěch ◽  
Jaroslav Vavřík ◽  
Kristína Bartha ◽  
Přemysl Beran ◽  
...  

Severe plastic deformation represented by three passes in Conform SPD and subsequent rotary swaging was applied on Ti grade 4. This process caused extreme strengthening of material, accompanied by reduction of ductility. Mechanical properties of such material were then tuned by a suitable heat treatment. Measurements of in situ electrical resistance, in situ XRD and hardness indicated the appropriate temperature to be 450 °C for the heat treatment required to obtain desired mechanical properties. The optimal duration of annealing was stated to be 3 h. As was verified by neutron diffraction, SEM and TEM microstructure observation, the material underwent recrystallization during this heat treatment. That was documented by changes of the grain shape and evaluation of crystallite size, as well as of the reduction of internal stresses. In annealed state, the yield stress and ultimate tensile stress decreased form 1205 to 871 MPa and 1224 to 950 MPa, respectively, while the ductility increased from 7.8% to 25.1%. This study also shows that mechanical properties of Ti grade 4 processed by continual industrially applicable process (Conform SPD) are comparable with those obtained by ECAP.


2021 ◽  
Vol 43 (1) ◽  
pp. 1
Author(s):  
Agus Pramono ◽  
Suryana Suryana ◽  
Alfirano Alfirano ◽  
A. Ali Alhamidi ◽  
Adhitya Trenggono ◽  
...  

AbstrakProses produksi dengan menggunakan metode pengerjaan logam konvensional seringkali sulit terutama untuk produk masif, dimana peralatan dan produk seperti gaya dan tekanan tinggi diperlukan. Keterbatasan ini bisa diatasi dengan menggunakan teknologi terbaru yaitu severe plastic deformation (SPD), dengan metode spesifiknya yaitu equal channel angulatr pressing (ECAP). Perkembangan ECAP sudah mencapai tahap aplikasi produk, salah satu pengembangan metodenya yaitu model parallel channel, atau disebut ECAP-PC. Dalam aplikasi pembuatan komponen, diperlukan proses perlakuan panas material, bertujuan untuk mengubah sifat material. Perlakuan panas yang sesuai diantaranya adalah proses pelunakan anealling untuk pengerjaan komponen dan perlakuan panas jenis T6; artificial aging/age-hardening sebagai proses akhir, untuk penerapan aplikasi tertentu. Serbuk aluminium (Al) dengan campuran zirconium (Zr) diaktivasi secara mekanis menggunakan ball milling. Pencampuran menggunakan cairan etanol dan heptane untuk memudahkan pengeringan. Fraksi volume yang digunakan dalam komposit Al sebagai matriks dan Zr yaitu 97:3%. Serbuk komposit dilakukan penggilingan dengan proses ball milling menggunakan putaran 60 rpm selama 24 jam. Hasil perlakuan panas age-hardening menghasilkan sifat mekanik tertinggi sebesar 144-222 HV/1406-2177 MPa dibanding dengan jenis annealing yaitu 31-46 HV/301-449 MPa. Hal ini sesuai dengan tujuan dari perlakuan panas yaitu untuk menurunkan sifat mekanik agar material mudah diproses. AbstractThe production of conventional metalworking methods is often difficult especially for massive products, where equipment and products such as high force and pressure are required. This limitation can be overcome by using the latest technology, namely severe plastic deformation (SPD). By specific method, namely Equal Channel Angular Pressing (ECAP). The development of ECAP has reached the product application stage, one of the methods development is parallel channel model, or called ECAP-PC. Application of component manufacturing requires a material heat treatment process, aims to change the properties of the material. Suitable heat treatments include the annealing softening process for component work and the T6 type heat treatment; artificial aging/age-hardening as a finishing process for the application of certain applications. Aluminum (Al) powder and zirconium (Zr), mixture were activated mechanically by ball milling. Mixing processed using liquid ethanol and heptane for easy drying. The volume fraction used in the Al composite as a matrix and Zr is 97: 3%. The composites powder was milled by ball milling used a 60 rpm rotation for 24 hours. The results of age-hardening heat treatment produced the highest mechanical properties of 144-222 HV / 1406-2177 MPa compared to the type of annealing, namely 31-46 HV / 301-449 MPa. This is in accordance with the purpose of heat treatment, namely to reduce mechanical properties so that the material is easy to process.


2018 ◽  
Vol 1 (1) ◽  
pp. 77-90
Author(s):  
Walaa Abdelaziem ◽  
Atef Hamada ◽  
Mohsen A. Hassan

Severe plastic deformation is an effective method for improving the mechanical properties of metallic alloys through promoting the grain structure. In the present work, simple cyclic extrusion compression technique (SCEC) has been developed for producing a fine structure of cast Al-1 wt. % Cu alloy and consequently enhancing the mechanical properties of the studied alloy. It was found that the grain structure was significantly reduced from 1500 µm to 100 µm after two passes of cyclic extrusion. The ultimate tensile strength and elongation to failure of the as-cast alloy were 110 MPa and 12 %, respectively. However, the corresponding mechanical properties of the two pass CEC deformed alloy are 275 MPa and 35%, respectively. These findings ensure that a significant improvement in the grain structure has been achieved. Also, cyclic extrusion deformation increased the surface hardness of the alloy by 49 % after two passes. FE-simulation model was adopted to simulate the deformation behavior of the material during the cyclic extrusion process using DEFORMTM-3D Ver11.0. The FE-results revealed that SCEC technique was able to impose severe plastic strains with the number of passes. The model was able to predict the damage, punch load, back pressure, and deformation behavior.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3467
Author(s):  
Anna Nocivin ◽  
Doina Raducanu ◽  
Bogdan Vasile ◽  
Corneliu Trisca-Rusu ◽  
Elisabeta Mirela Cojocaru ◽  
...  

The present paper analyzed the microstructural characteristics and the mechanical properties of a Ti–Nb–Zr–Fe–O alloy of β-Ti type obtained by combining severe plastic deformation (SPD), for which the total reduction was of etot = 90%, with two variants of super-transus solution treatment (ST). The objective was to obtain a low Young’s modulus with sufficient high strength in purpose to use the alloy as a biomaterial for orthopedic implants. The microstructure analysis was conducted through X-ray diffraction (XRD), scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM) investigations. The analyzed mechanical properties reveal promising values for yield strength (YS) and ultimate tensile strength (UTS) of about 770 and 1100 MPa, respectively, with a low value of Young’s modulus of about 48–49 GPa. The conclusion is that satisfactory mechanical properties for this type of alloy can be obtained if considering a proper combination of SPD + ST parameters and a suitable content of β-stabilizing alloying elements, especially the Zr/Nb ratio.


2010 ◽  
Vol 667-669 ◽  
pp. 925-930
Author(s):  
S.V. Krymskiy ◽  
Elena Avtokratova ◽  
M.V. Markushev ◽  
Maxim Yu. Murashkin ◽  
O.S. Sitdikov

The effects of severe plastic deformation (SPD) by isothermal rolling at the temperature of liquid nitrogen combined with prior- and post-SPD heat treatment, on microstructure and hardness of Al-4.4%Cu-1.4%Mg-0.7%Mn (D16) alloy were investigated. It was found no nanostructuring even after straining to 75%. Сryodeformation leads to microshear banding and processing the high-density dislocation substructures with a cell size of ~ 100-200 nm. Such a structure remains almost stable under 1 hr annealing up to 200oC and with further temperature increase initially transforms to bimodal with a small fraction of nanograins and then to uniform coarse grained one. It is found the change in the alloy post–SPD aging response leading to more active decomposition of the preliminary supersaturated aluminum solid solution, and to the alloy extra hardening under aging with shorter times and at lower temperatures compared to T6 temper.


2007 ◽  
Vol 550 ◽  
pp. 289-294
Author(s):  
Suk Hoon Kang ◽  
Jae Hyung Cho ◽  
Joon Sub Hwang ◽  
Jong Soo Cho ◽  
Yong Jin Park ◽  
...  

Cold drawn gold wires are widely applied in electronic packaging process to interconnect micro-electronic components. They basically provides a conducting path for electronic signal transfer, and experience thermo-mechanical loads in use. The mechanical stability of drawn gold wires is a matter of practical concern in the reliable functioning of electronic devices. It is known that mechanical properties of materials are deeply related to the microstructure. With appropriate control of deformation and heat processes, the mechanical properties of final products, such as tensile strength and elongation can be improved. Severe plastic deformation by torsion usually contributes to grain refinement and increment of strength. In this study, microstructure variations with torsion strain followed by drawing and heat treatment were investigated. Analyses by focused ion beam (FIB) and electron backscattered diffraction (EBSD) were carried out to characterize the effect of deformation and heat treatment on the drawn gold wires. Pattern quality of EBSD measurements was used as a quantitative measure for plastic deformation.


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