scholarly journals Single-step Synthesis and Characterization of Zr-MOF onto Wool Fabric: Preparation of Antibacterial Wound Dressing with High Absorption Capacity

2021 ◽  
Author(s):  
Reihane Rezaee ◽  
Majid Montazer ◽  
Ali Mianehro ◽  
Mahnaz Mahmoudirad
Keyword(s):  
Wound Dressing ◽  
Absorption Capacity ◽  
Single Step ◽  
Synthesis And Characterization ◽  
Wool Fabric ◽  
High Absorption

scholarly journals Sintesis dan karakterisasi polimer superabsorban dari akrilamida

2018 ◽  
Vol 11 (2) ◽  
pp. 84
Author(s):  
A. Zainal Abidin ◽  
G Susanto ◽  
N.M.T. Sastra ◽  
T Puspasari
Keyword(s):  
Absorption Capacity ◽  
Synthesis And Characterization ◽  
Superabsorbent Polymer ◽  
Ammonium Persulphate ◽  
Surface Contact Area ◽  
Acrylamide Monomer ◽  
Cross Linker ◽  
Short Time ◽  
High Absorption

Synthesis and Characterization of Superabsorbent from Acrylamide Superabsorbent polymer (SAP) is a material that can absorb water in a large amount in a short time. In this research, the polymer has been synthesized from acrylamide monomer (Am) using N,N methylene bisacrylamide (MBA)as a cross-linker and ammonium persulphate (APS) as an initiator. Effects of MBA and APS on the SAP characteristic were studied by varying composition of MBA and APS each of 0.1%-wt, 0.2 %-wt, 0.6 %-wt and 1.0 %-wt. SAP was characterized by measuring its absorption capacity to distilled water. Based on the experiment, the highest absorption capacity for 1 gram SAP is 14.5 gram water. The highest absorption is produced by SAP with APS 0.2 %-wt and MBA 0.6 %-wt. Further studies by using SEM showed that SAP which had high absorption capacity contained a lot of pores with the waving surface. Therefore, the surface contact area between SAP and water is high. Keywords: acrylamide, absorption capacity, superabsorbent polymerAbstrakSuperabsorbent Polymer (SAP) merupakan polimer yang dapat menyerap air dalam jumlah yang sangat banyak. Dalam penelitian ini, polimer tersebut disintesis dari monomer akrilamida menggunakan crosslinker N,N-metilene bisakrilamide (MBA) dan inisiator amonium persulfat (APS). Pengaruh crosslinker dan inisiator terhadap karakteristik SAP dipelajari dengan melakukan variasi komposisi APS dan (MBA) masing-masing sebesar 0,1 %-b, 0,2 %-b, 0,6 %-b, dan 1 %-b. Karakteristik produk SAP dipelajari dengan FTIR untuk menganalisis gugus fungsi yang terbentuk untuk menunjukkan bahwa polimerisasi betul terjadi dan produknya berupa SAP. Pengukuran kemampuan absorpsi SAP terhadap air destilasi menunjukkan bahwa kapasitas absorpsi terbesar yang dihasilkan oleh superabsorbent polymer dari penelitian ini sebesar 14,5 gram air dalam 1 gram produk SAP yang dibuat. Kapasitas terbesar ini dimiliki oleh SAP dengan 0,2 %-b APS dan 0,6 %-b MBA. Studi lebih lanjut dengan SEM menunjukkan bahwa SAP yang memiliki kapasitas absorpsi tertinggi itu mempunyai morfologi permukaan yang berombak dan jumlah pori yang tertinggi sehingga luas permukaan kontak antara SAP dan air juga tertinggi. Kata kunci: akrilamida, kapasitas absorpsi, superabsorbent polymer

Synthesis and characterization of a novel wound dressing by PVP/ PAANa/chitosan with semi-interpenetrating polymer network structure

e-Polymers ◽  
2012 ◽  
Vol 12 (1) ◽  
Author(s):  
Ying Wu ◽  
Qing Yang ◽  
Yali Gi ◽  
Yueting Zhang
Keyword(s):  
Network Structure ◽  
Wound Dressing ◽  
Polymer Network ◽  
Interpenetrating Polymer Network ◽  
Wound Dressings ◽  
Synthesis And Characterization ◽  
Cross Linking ◽  
Mass Ratio ◽  
Scanning Electron

AbstractA novel hydrogel wound dressing with semi-interpenetrating polymer network structure (semi-IPN) was prepared by radical polymerization of acrylic acid with potassium persulfate (K2S2O8) as initiator and N, N'-methylenebisacrylamide (MBA) as cross-linking agent in the presence of chitosan (CTS) and polyvinyl pyrrolidone (PVP). Hydrogels were characterized by scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR). SEM displayed semi- IPN hydrogels' creased surface with some scale-like wrinkles, thus improving the absorptive capability which has been considered as a most important characteristic of wound dressings. It was found that the content of cross-linking agent and the mass ratio of PVP and CTS had much influence on the mechanical properties of the hydrogel, varying from brittle plastics to elastomer due to the different degrees of cross linking. Since tensile strength is partly in inverse ratio to the hydrogel absorbent capability, the article offers an analysis of varying material proportion in order to obtain an optimum properties of the hydrogel wound dressing .

Single step synthesis and characterization of ZnAl2O4 nanoparticles

2018 ◽  
Author(s):  
Megha Jain ◽  
Manju ◽  
Kulwinder Singh ◽  
Akshay Kumar ◽  
Jeewan Sharma ◽  
...  
Keyword(s):  
Single Step ◽  
Synthesis And Characterization

Synthesis and characterization of antimicrobial wound dressing material based on silver nanoparticles loaded gum Arabic nanofibers

2020 ◽  
Vol 155 ◽  
pp. 119-130 ◽  
Author(s):  
Naeimeh Eghbalifam ◽  
Seyed Abbas Shojaosadati ◽  
Sameereh Hashemi-Najafabadi ◽  
Alireza Chackoshian Khorasani
Keyword(s):  
Silver Nanoparticles ◽  
Wound Dressing ◽  
Gum Arabic ◽  
Synthesis And Characterization

Preparation and Characterization of Bacterial Cellulose/TiO2 Hydrogel Nanocomposite

2016 ◽  
Vol 43 ◽  
pp. 73-80 ◽  
Author(s):  
Ricardo Brandes ◽  
Letícia de Souza ◽  
Vanessa Vargas ◽  
Eliana Oliveira ◽  
Alexandre Mikowski ◽  
...  
Keyword(s):  
Bacterial Cellulose ◽  
Water Retention ◽  
Morphological Analysis ◽  
Sol Gel ◽  
Absorption Capacity ◽  
Ex Situ ◽  
High Tensile Strength ◽  
Hydrogel Nanocomposite ◽  
High Absorption

Bacterial cellulose (BC) is a biopolymer with interesting properties, such as biocompatibility, high tensile strength, high absorption capacity, water retention and high crystallinity. Nanoparticles of titanium dioxide (TiO2) are extremely important in electrical applications, photocatalysis, sensors and biomedical areas. Multifunctional materials, based on bacterial cellulose, with differentiated properties can be designed from the BC/TiO2 nanocomposite by ex situ method of sol-gel immersion. It was manufactured as a nanocomposite consisting of BC/TiO2 hydrogel. Characterizations were carried out by scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and fourier transform infrared spectroscopy (FTIR). The morphological analysis of nanocomposite revealed the existence of molecular interaction and adhesion between TiO2 nanoparticles and cellulosic nanofibers matrix, where the presence of Ti peaks in EDS spectra was discovered, proving the successful incorporation of nanoparticles. The FTIR showed modification on the functional groups, suggesting interaction between the components. The manufacturing of a BC/TiO2 nanocomposite by method of sol-gel immersion has a great potential for future applications.

Synthesis and Characterization of Polycaprolactone/Cellulose Acetate by Electrospinning for Wound Dressing Applications

2020 ◽  
Vol 981 ◽  
pp. 291-295
Author(s):  
Nurul Nadirah Suteris ◽  
Izan Izwan Misnon ◽  
Rasidi Roslan ◽  
Farah Hanani Zulkifli ◽  
Jayarama Reddy Venugopal ◽  
...  
Keyword(s):  
Cellulose Acetate ◽  
Wound Dressing ◽  
Functional Materials ◽  
Recent Time ◽  
Synthesis And Characterization ◽  
Environmental Load ◽  
High Quality ◽  
Electrospinning Technique ◽  
Renewable Material

Cellulose as a renewable material has received enormous interest in recent time with an effort to minimize the environmental load from mining earthborn functional materials as well as reducing carbon footprint. This work demonstrates that high quality cellulose could be produced from empty fruit bunch of oil palm plantation and could be developed into nanofibers. A small amount of poly (ε-caprolactone) (PCL) was added to the EFB driven cellulose acetate (CA) to develop them as nanofibers by electrospinning technique; this composition was further enhanced by adding curcumin, which is a natural anti-inflammatory, and compared their morphology, structure, mechanical and surface properties.

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