Cost-effective one-pot surface modified method to engineer a green superhydrophobic sponge for efficient oil/water mixtures as well as emulsions separation

Author(s):  
Li Zhang ◽  
Dongyu Dong ◽  
Leishan Shao ◽  
Yifan Xia ◽  
Teng Zeng ◽  
...  
Materials ◽  
2019 ◽  
Vol 12 (17) ◽  
pp. 2702 ◽  
Author(s):  
Evren Boyraz ◽  
Fatma Yalcinkaya ◽  
Jakub Hruza ◽  
Jiri Maryska

Preparing easily scaled up, cost-effective, and recyclable membranes for separation technology is challenging. In the present study, a unique and new type of modified polyvinylidene fluoride (PVDF) nanofibrous membrane was prepared for the separation of oil–water emulsions. Surface modification was done in two steps. In the first step, dehydrofluorination of PVDF membranes was done using an alkaline solution. After the first step, oil removal and permeability of the membranes were dramatically improved. In the second step, TiO2 nanoparticles were grafted onto the surface of the membranes. After adding TiO2 nanoparticles, membranes exhibited outstanding anti-fouling and self-cleaning performance. The as-prepared membranes can be of great use in new green separation technology and have great potential to deal with the separation of oil–water emulsions in the near future.


RSC Advances ◽  
2015 ◽  
Vol 5 (44) ◽  
pp. 34942-34948 ◽  
Author(s):  
Sayantan Mazumdar ◽  
Aninda J. Bhattacharyya

An unprecedented morphology of a titanium dioxide (TiO2) and cadmium sulfide (CdS) self-assembly obtained using a ‘truly’ one-pot and highly cost effective method with a multi-gram scale yield is reported here.


2018 ◽  
Vol 2018 ◽  
pp. 1-13 ◽  
Author(s):  
Haliza Katas ◽  
Noor Zianah Moden ◽  
Chei Sin Lim ◽  
Terence Celesistinus ◽  
Jie Yee Chan ◽  
...  

Biosynthesized or biogenic metallic nanoparticles, particularly silver and gold nanoparticles (AgNPs and AuNPs, respectively), have been increasingly used because of their advantages, including high stability and loading capacity; moreover, these nanoparticles are synthesized using a green and cost-effective method. Previous studies have investigated reducing and/or stabilizing agents from various biological sources, including plants, microorganisms, and marine-derived products, using either a one-pot or a multistep process at different conditions. In addition, extensive studies have been performed to determine the biological or pharmacological effects of these nanoparticles, such as antimicrobial, antitumor, anti-inflammatory, and antioxidant effects. In the recent years, chitosan, a natural cationic polysaccharide, has been increasingly investigated as a reducing and/or stabilizing agent in the synthesis of biogenic metallic nanoparticles with potential applications in nanomedicine. Here, we have reviewed the mechanism of biosynthesis and potential applications of AgNPs and AuNPs and their chitosan-mediated nanocomposites in nanomedicine.


Author(s):  
Lai Yan Xia ◽  
Hamidah Abu Bakar

Malaria is a life-threatening disease which has claimed many lives. Giemsa's stain is the gold standard method in malaria diagnosis. Generally, Giemsa's stain is diluted with buffered water. However, sometimes, it produces poor staining of the blood smears, in which can create a major challenge in detecting and identifying positive malaria parasites in a peripheral blood smear. This can lead to misdiagnosis and mistreatment to a patient. The present study examined the effect of replacing the buffered water to distilled water during the preparation of 3% Giemsa's solution. Blood specimens were collected from selected positive (n=80) and negative (n=300) malaria cases in EDTA tube. The modified method employed distilled water and different concentrations of buffered water for diluting Giemsa’s solution stock. The microscopy observation was performed on each set of blood film stained by both modified and standard Giemsa staining methods by two WHO’s qualified technicians. All Giemsa solutions with different diluents were comparable in detecting malaria parasites in the blood films. There was no difference between distilled water and different concentrations of buffered water. Furthermore, distilled water produced homogeneous staining and clearer background of the blood films, which enables different species of malaria to be identified. The present study demonstrates that the modified staining using distilled water in malaria parasites identification is comparable to the gold standard method. In addition, the modified method is rapid, easily available, cost-effective, and reliable.


Author(s):  
Ali Ghafarloo ◽  
Reza Sabzi ◽  
Naser Samadi ◽  
Hamed Hamishehkar

Synthesis of carbon dots (CDs) from natural resources not only enables green synthesis and production of environmentally friendly materials, but also provides a cost-effective probe as a fluorescence nanosensor. The proposed sensor introduces a unique one-pot hydrothermal CDs synthesis from alfalfa leaves, which is promising for sensing hydrochlorothiazide (HCTZ) via inner filter effect (IFE) and resonance Rayleigh scattering (RRS). The as-prepared CDs had wide emission spectra, excitation-dependent emission, high solubility, high stability, and visible fluorescence light with a quantum yield of up to 11%. The absorption of HCTZ overlapped with the excitation spectra of CDs. Therefore, CDs represented excellent quenching due to IFE when HCTZ was gradually added. Furthermore, this fluorescent sensor was successfully used to quantify HCTZ in the linear ranges (0.17-2.50 μg mL-1) with the limit of detection of 0.11 μg mL-1. The sensing system was simple as no surface functionalization was required for CDs, leading to less laborious steps and more cost-effective synthesis. The reaction time was short, i.e., less than 2 min, indicating a simple approach for rapid analysis of HCTZ. By optimizing conditions, successful measurements were carried out on pharmaceutical tablets.


2022 ◽  
Vol 233 (1) ◽  
Author(s):  
Arthi Karunanithi ◽  
Jyotiraman De ◽  
Sumit Saxena ◽  
Shobha Shukla

2021 ◽  
Author(s):  
Abdelhak Ladmia ◽  
Dr. Younes bin Darak Al Blooshi ◽  
Abdullah Alobedli ◽  
Dragoljub Zivanov ◽  
Myrat Kuliyev ◽  
...  

Abstract The expected profiles of the water produced from the mature ADNOC fields in the coming years imply an important increase and the OPEX of the produced and injected water will increase considerably. This requires in-situ water separation and reinjection. The objective of in-situ fluid separation is to reduce the cost of handling produced water and to extend the well natural flow performance resulting in increased and accelerated production. The current practice of handling produced water is inexpensive in the short term, but it can affect the operating cost and the recovery in the long term as the expected water cut for the next 10-15 years is forecasted to incease significantly. A new water management tool called downhole separation technology was developed. It separates oil and & gas from associated water inside the wellbore to be reinjected back into the disposal wells. The Downhole Oil Water Separation (DHOWS) Technology is one of the key development strategies that can reduce considerable amounts of produced water, improve hydrocarbon recovery, and minimize field development cost by eliminating surface water treatment and handling costs. The main benefits of DHOWS include acceleration of oil offtake, reduction of production cost, lessening produced water volumes, and improved utilization of surface facilities. In effect, DHOWS technologies require specific design criteria to meet the objectives of the well. Therefore, multi--discipline input data are needed to install an effective DHOWS with a robust design that economically outperforms and boosts oil and/or gas productions. This paper describes the fundamental criteria and workflow for selecting the most suitable DHOWS design for new and sidetracked wells to deliver ADNOC production mandates in a cost-effective manner while meeting completion requirements and adhering to reservoir management guidelines.


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