Influence of the final heat treatment temperature on the magnetic property losses of Sm(Co,Fe,Cu,Zr)z high temperature magnets

2021 ◽  
Vol 528 ◽  
pp. 167763
Author(s):  
Wei Xia ◽  
Tianli Zhang ◽  
Jinghua Liu ◽  
Ying Dong ◽  
Hui Wang ◽  
...  
2015 ◽  
Vol 658 ◽  
pp. 14-18
Author(s):  
Tanaporn Rojhirunsakool ◽  
Duangkwan Thongpian ◽  
Nutthita Chuankrerkkul ◽  
Panyawat Wangyao

Nickel-base superalloys have been used as high temperature materials in land-base gas turbine application. When subjected to long term, high temperature service, large crack propagation was observed. Typical refurbishment method of these turbines is carried out by using TIG welding followed by post-weld standard heat treatment. However, new crack initiation is found in the heat-affected zone after TIG welding. Pre-weld heat treatment has been discovered to improves final γ + γ’ microstructure. This study focuses on the effect of pre-weld heat treatment temperature on final γ + γ’ microstructure. Seven different conditions of pre-weld heat treatment temperature were investigated. Scanning electron microscopy studies were carried out after pre-weld and post-weld heat treatments to compare the γ + γ’ microstructure and capture microcracks. The best pre-weld heat treatment temperature produces uniform distribution of finely dispersed γ’ precipitates in the γ matrix without post-weld crack.


Processes ◽  
2020 ◽  
Vol 8 (8) ◽  
pp. 933 ◽  
Author(s):  
Gerrit Ralf Surup ◽  
Tommy Andre Pedersen ◽  
Annah Chaldien ◽  
Johan Paul Beukes ◽  
Merete Tangstad

This study reports the effect of high-temperature treatment on the electrical properties of charcoal, coal, and coke. The electrical resistivity of industrial charcoal samples used as a reducing agent in electric arc furnaces was investigated as a renewable carbon source. A set-up to measure the electrical resistivity of bulk material at heat treatment temperatures up to 1700 ∘C was developed. Results were also evaluated at room temperature by a four-point probe set-up with adjustable load. It is shown that the electrical resistivity of charcoal decreases with increasing heat treatment temperature and approaches the resistivity of fossil carbon materials at temperatures greater than 1400 ∘C. The heat treatment temperature of carbon material is the main influencing parameter, whereas the measurement temperature and residence time showed only a minor effect on electrical resistivity. Bulk density of the carbon material and load on the burden have a large impact on the electrical resistivity of each material, while the effect of particle size can be neglected at high heat treatment temperature or compacting pressure. The mechanical durability of charcoal slightly increased after heat treatment and decreased for coal and semi-coke samples. The results indicate that charcoal can be used as an efficient carbon source for electric arc furnaces.


2014 ◽  
Vol 809-810 ◽  
pp. 815-821
Author(s):  
Xiao Hu Hua ◽  
Xiao Gang Wang ◽  
Jia Qing Yang ◽  
Shu He Lu ◽  
Li Rong Deng ◽  
...  

Anthracite and bitumite were processed respectively at 1400°C,1700°C, 2000°C, 2200°C, 2400°C and 2600°C,and their chemical composition,resistivity,microstructure, phase composition,and the internal migration of molecular functional group were tested and characterized. The results indicate that moisture, ash and volatile in coal have gradually shifted and lost with the elevation of heat treatment temperature, while the higher temperature, the quicker and completer phase change. Heat treatment can make the coal transform from approximately insulative phase to conductive phase,. Furthermore, as the temperature increases, the conductive phase transformation effect is better. The higher the heat treatment temperature of coal, the more amorphous carbon transforming into crystalline carbon completely, but the less types of phases .


2015 ◽  
Vol 761 ◽  
pp. 412-416 ◽  
Author(s):  
Kok Tee Lau ◽  
Mohd Hafrez Razi Ab Razak ◽  
Swee Leong Kok ◽  
Muhammad Zaimi ◽  
Mohd Warikh Abd Rashid ◽  
...  

Polymeric poly (vinyliden fluoride) (PVDF) is nontoxic. It possesses a better mechanical flexibility and requires a lower synthesis temperature, as compared to the piezoceramic counterparts. In order to achieve a competitive advantage against the current piezoelectric sensor, graphite could replace a more expensive silver-palladium as the electrodes for the piezoelectric PVDF. This paper reports the preliminary results on the synthesis of steel-supported graphite-PVDF/PVDF/graphite-PVDF composite films using the two-step process, consisted of the electrophoretic deposition (EPD) and heat treatment. The composite films were characterized by means of the optical microscopy, scanning electron microscopy, X-ray diffraction and differential scanning calorimetry. The heat treated graphite-PVDF electrode deposited by EPD provides adequate mechanical strength for the subsequent depositions of pure PVDF layer and the second layer of graphite-PVDF composite electrode. However, the final heat treatment stage did not eliminate the fine and large cracks of the composite film, which might be attributed to high residue stresses and weak bonding between graphite and PVDF particles in the post-heat treated composite films. Nevertheless, the increase in final heat treatment temperature of the composite film at Stage 3 improved the graphite and PVDF grain alignment, as well as its crystallinity.


2018 ◽  
Vol 281 ◽  
pp. 959-963
Author(s):  
Feng Zhang ◽  
Chuan Qi Hu ◽  
Shi Chao Zhang ◽  
Hao Ran Sun ◽  
Yuan Tian ◽  
...  

In this paper, the modified phenolic resin-based adhesive was prepared by dissolving different components. After low temperature curing, SiC samples were bonded by the binder. The samples were treated at different temperatures (400°C, 800°C, 1200°C, 1500°C) under an inert atmosphere. The bonding strength of samples was tested after heat treatment at room temperature. The results showed that the bonding strength of the B4C modified phenolic resin (PF) based adhesive is the highest. When the heat treatment temperature was above 1200°C, the bond strength increased with the additive amount of boron carbide at room temperature. The microstructures of the samples were observed by optical microscope and scanning electron microscope. The effects of the modified filler and heat treatment temperature on the bonding strength of the phenolic resin based adhesive were investigated. The bonding strength of boron carbide-modified phenolic resin-based binder was tested under high temperature. It was found that the bond strength at high temperature was lower than that at room temperature, and the bond strength decreased with the increase of temperature.


2021 ◽  
Vol 353 ◽  
pp. 01020
Author(s):  
Yan Xu ◽  
Yinglai Liu ◽  
Xianghui Nie ◽  
Zhenjun Feng ◽  
Liang Li ◽  
...  

During the welding of in-service pipeline, natural gas is continuously transported in the pipeline, which maintains a high gas pressure. Therefore, the welding process is completed under strong cooling conditions, and welding delay crack is easy to occur. Preheating before welding and heat treatment after welding can effectively control the hardened microstructure, reduce the residual stress and ensure the welding quality. In this study, the influence of heating temperature on the bearing capacity of high steel grade pipe during in-service welding repair was studied. The high temperature tensile test was used to simulate the bearing capacity of the pipe under heating and high temperature environment. It is found that when the heating temperature is below 400°C, the pipe strength remains at the original level. With the increase of heating temperature, when the test temperature is higher than 400°C, the yield strength and tensile strength of the pipe decrease significantly. When the test temperature is 450°C, the yield strength and tensile strength of the material decrease by 15.8% and 11.1%, respectively, compared with the normal temperature, which are lower than the pipe standard requirements. Therefore, it is suggested that when the heat treatment temperature is higher than 400°C during in-service welding repair, it is necessary to consider reducing the pipeline pressure. At the same time, the box furnace heat treatment method was adopted to heat treat the pipe, and the tensile properties of the pipe after heat treatment were tested to analyze the bearing capacity of the pipe after heat treatment. It is found that when the heating temperature is higher than 700°C, the tensile properties of high grade pipeline steel pipe decrease sharply. It is suggested that when the heat treatment temperature is higher than 700°C, the risk assessment of the service safety of the heat treated pipeline should be carried out.


Geofluids ◽  
2020 ◽  
Vol 2020 ◽  
pp. 1-17
Author(s):  
Zhengdai Li ◽  
Jianping Zuo ◽  
Yue Shi ◽  
Fei Xu ◽  
Meilu Yu ◽  
...  

Due to the influences of various factors, such as temperature, stress, and composition, the research regarding rock permeability has been complicated. This study examined the variation laws of sandstone specimens under changing rates of confining and pore pressures after high-temperature heat treatments. The results showed that the free water in the rock volatilized during the low-temperature heat treatments in the range of 100°C to 300°C, with the increase of the heat-treatment temperature above 500°C; the crystal water in the rock is gradually separated out; and the particles in the samples had undergone phase transformations resulting in increased permeability. According to ultrasonic wave velocity test results, the internal cracks of the samples expanded with the increases in the heat-treatment temperatures. In addition, the high-temperature heat treatments were found to improve the accuracy of the direction of the Earth’s stress when using circumferential wave velocity anisotropy methods. Under the influence of slippage effects, as the pore pressure increased, the measured permeability of the samples decreased and the slippage effect occurs in the rock samples with the permeability of 10-3 μm2~10-6 μm2. The experimental results showed that the contribution rate of the slippage effect decreases with the increase of the heat-treatment temperature of the specimen, and the contribution rates of the sandstone slippage effect were generally higher than 5%. Therefore, the impact effects on the permeability of sandstone slippage should be considered in practical engineering processes.


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