HREM interface studies in SiC-whisker-reinforced Al2O3 and Si3N4 ceramics

1988 ◽  
Vol 46 ◽  
pp. 734-735
Author(s):  
W. Braue ◽  
R.W. Carpenter ◽  
D.J. Smith
Keyword(s):  
Analytical Data ◽  
Base Material ◽  
High Strength ◽  
Ceramic Composites ◽  
Good Thermal Stability ◽  
All Ceramic ◽  
Sic Whiskers ◽  
Base Composite ◽  
C 30 ◽  
Si3n4 Ceramics

Whisker and fiber reinforcement has been established as an effective toughening concept for monolithic structural ceramics to overcome limited fracture toughness and brittleness. SiC whiskers in particular combine both high strength and elastic moduli with good thermal stability and are compatible with most oxide and nonoxide matrices. As the major toughening mechanisms - crack branching, deflection and bridging - in SiC whiskenreinforced Al2O3 and Si3N41 are critically dependent on interface properties, a detailed TEM investigation was conducted on whisker/matrix interfaces in these all-ceramic- composites.In this study we present HREM images obtained at 400 kV from β-SiC/α-Al2O3 and β-SiC/β-Si3N4 interfaces, as well as preliminary analytical data. The Al2O3- base composite was hotpressed at 1830 °C/60 MPa in vacuum and the Si3N4-base material at 1725 °C/30 MPa in argon atmosphere, respectively, adding a total of 6 vt.% (Y2O3 + Al2O3) to the latter to promote densification.

Biomimetic materials: An introduction

1992 ◽  
Vol 50 (2) ◽  
pp. 1020-1021 ◽  
Author(s):  
M. Sarikaya ◽  
J. T. Staley ◽  
I. A. Aksay
Keyword(s):  
Self Assembly ◽  
Structural Control ◽  
Hierarchical Structures ◽  
Ceramic Composites ◽  
Advanced Materials ◽  
Length Scale ◽  
Spider Webs ◽  
Biomimetic Materials ◽  
Synthetic Materials ◽  
All Ceramic

Biomimetics is an area of research in which the analysis of structures and functions of natural materials provide a source of inspiration for design and processing concepts for novel synthetic materials. Through biomimetics, it may be possible to establish structural control on a continuous length scale, resulting in superior structures able to withstand the requirements placed upon advanced materials. It is well recognized that biological systems efficiently produce complex and hierarchical structures on the molecular, micrometer, and macro scales with unique properties, and with greater structural control than is possible with synthetic materials. The dynamism of these systems allows the collection and transport of constituents; the nucleation, configuration, and growth of new structures by self-assembly; and the repair and replacement of old and damaged components. These materials include all-organic components such as spider webs and insect cuticles (Fig. 1); inorganic-organic composites, such as seashells (Fig. 2) and bones; all-ceramic composites, such as sea urchin teeth, spines, and other skeletal units (Fig. 3); and inorganic ultrafine magnetic and semiconducting particles produced by bacteria and algae, respectively (Fig. 4).

Microstructure of resistance spot welding of maraging steels

1990 ◽  
Vol 48 (4) ◽  
pp. 900-901
Author(s):  
I. Neuman ◽  
S.F. Dirnfeld ◽  
I. Minkoff
Keyword(s):  
Maraging Steel ◽  
Spot Welding ◽  
Lath Martensite ◽  
Base Material ◽  
Aging Treatment ◽  
High Strength ◽  
Maraging Steels ◽  
Heat Treated ◽  
Current Cycle ◽  
Welding Processes

Experimental work on the spot welding of Maraging Steels revealed a surprisingly low level of strength - both in the as welded and in aged conditions. This appeared unusual since in the welding of these materials by other welding processes (TIG,MIG) the strength level is almost that of the base material. The maraging steel C250 investigated had the composition: 18wt%Ni, 8wt%Co, 5wt%Mo and additions of Al and Ti. It has a nominal tensile strength of 250 KSI. The heat treated structure of maraging steel is lath martensite the final high strength is reached by aging treatment at 485°C for 3-4 hours. During the aging process precipitation takes place of Ni3Mo and Ni3Ti and an ordered solid solution containing Co is formed.Three types of spot welding cycles were investigated: multi-pulse current cycle, bi-pulse cycle and single pulsle cycle. TIG welded samples were also tested for comparison.The microstructure investigations were carried out by SEM and EDS as well as by fractography. For multicycle spot welded maraging C250 (without aging), the dendrites start from the fusion line towards the nugget centre with an epitaxial growth region of various widths, as seen in Figure 1.

scholarly journals Development of laser welding of high strength aluminium alloy 2024-T4 with controlled thermal cycle

2020 ◽  
Vol 326 ◽  
pp. 08005
Author(s):  
Mete Demirorer ◽  
Wojciech Suder ◽  
Supriyo Ganguly ◽  
Simon Hogg ◽  
Hassam Naeem
Keyword(s):  
Laser Beam ◽  
Laser Welding ◽  
Heat Input ◽  
Thermal Cycle ◽  
Laser Beam Welding ◽  
Base Material ◽  
High Strength ◽  
Cooling Rates ◽  
Aa 2024 ◽  
Welding Processes

An innovative process design, to avoid thermal degradation during autogenous fusion welding of high strength AA 2024-T4 alloy, based on laser beam welding, is being developed. A series of instrumented laser welds in 2 mm thick AA 2024-T4 alloys were made with different processing conditions resulting in different thermal profiles and cooling rates. The welds were examined under SEM, TEM and LOM, and subjected to micro-hardness examination. This allowed us to understand the influence of cooling rate, peak temperature, and thermal cycle on the growth of precipitates, and related degradation in the weld and heat affected area, evident as softening. Although laser beam welding allows significant reduction of heat input, and higher cooling rates, as compared to other high heat input welding processes, this was found insufficient to completely supress coarsening of precipitate in HAZ. To understand the required range of thermal cycles, additional dilatometry tests were carried out using the same base material to understand the time-temperature relationship of precipitate formation. The results were used to design a novel laser welding process with enhanced cooling, such as with copper backing bar and cryogenic cooling.

Synthesis and Characterization of Porous ZrO2-Y2O3-TiO2 Ceramics Prepared by Coprecipitation

2012 ◽  
Vol 727-728 ◽  
pp. 1387-1392 ◽  
Author(s):  
Luan M. Medeiros ◽  
Fernando S. Silva ◽  
Juliana Marchi ◽  
Walter Kenji Yoshito ◽  
Dolores Ribeiro Ricci Lazar ◽  
...  
Keyword(s):  
Ceramic Composite ◽  
High Strength ◽  
Ceramic Composites ◽  
Rice Starch ◽  
X Ray Diffraction ◽  
Zirconia Ceramics ◽  
Pore Former ◽  
X Ray ◽  
Cold Pressed

Zirconium dioxide (zirconia) ceramics are known by its high strength and toughness and titanium dioxide (titania) ceramics has outstanding surface properties. The ceramic composite formed between the two oxides are expected to have advantages of both ceramics, especially when its surface area is increased by pores. In this work, ceramic composites of ZrO2-Y2O3-TiO2were synthesized by coprecipitation and rice starch was added as pore former in 10, 20 and 30 wt%. Powders were cold pressed as cylindrical pellets and sintered at 1500 °C for 01 hour and ceramics were characterized by techniques as Archimedes method for density measurements, X-ray diffraction and scanning electron microscopy. Results showed that pores are inhomogeneously distributed through ceramic bodies.

scholarly journals High Strength Si3N4 Ceramics

1989 ◽  
Vol 97 (1128) ◽  
pp. 872-874 ◽  
Author(s):  
Yoshio UKYO ◽  
Shigetaka WADA
Keyword(s):  
High Strength ◽  
Si3n4 Ceramics

Mechanical Behaviour of Welded Joints Achieved by Multi-Wire Submerged Arc Welding

2017 ◽  
Vol 1143 ◽  
pp. 52-57
Author(s):  
Elena Scutelnicu ◽  
Carmen Catalina Rusu ◽  
Bogdan Georgescu ◽  
Octavian Mircea ◽  
Melat Bormambet
Keyword(s):  
Mechanical Behaviour ◽  
Welded Joints ◽  
Arc Welding ◽  
Base Material ◽  
High Strength ◽  
Submerged Arc Welding ◽  
Steel Plates ◽  
Wire Saw ◽  
Api 5L X70 Steel ◽  
Submerged Arc

The paper addresses the development of advanced welding technologies with two and three solid wires for joining of HSLA API-5l X70 (High-strength low-alloy) steel plates with thickness of 19.1 mm. The experiments were performed using a multi-wire Submerged Arc Welding (SAW) system that was developed for welding of steels with solid, tubular and cold wires, in different combinations. The main goal of the research was to assess the mechanical performances of the welded joints achieved by multi-wire SAW technology and then to compare them with the single wire variant, as reference system. The welded samples were firstly subjected to NDT control by examinations with liquid penetrant, magnetic particle, ultrasonic and gamma radiation, with the aim of detecting the specimens with flaws and afterwards to reconsider and redesign the corresponding Welding Procedure Specifications (WPS). The defect-free welded samples were subjected to tensile, Charpy V-notch impact and bending testing in order to analyse and report the mechanical behaviour of API-5l X70 steel during multi-wire SAW process. The experimental results were processed and comparatively discussed. The challenge of the investigation was to find the appropriate welding technology which responds simultaneously to the criteria of quality and productivity. Further research on metallurgical behaviour of the base material will be developed, in order to conclude the complete image of the SAW process effects and to understand how the multi-wire technologies affect the mechanical and metallurgical characteristics of the API-5L X70 steel used in pipelines fabrication.

Strengthening Effect of In-Situ Dispersed Hexagonal Boron Nitride in Ceramic Composites

2006 ◽  
Vol 317-318 ◽  
pp. 163-166
Author(s):  
Guo Jun Zhang ◽  
Hideki Kita ◽  
Naoki Kondo ◽  
Tatsuki Ohji
Keyword(s):  
Grain Size ◽  
Boron Nitride ◽  
Hexagonal Boron Nitride ◽  
High Strength ◽  
Ceramic Composites ◽  
Strengthening Effect ◽  
Mechanical Shock ◽  
Metallic Particles ◽  
Reactive Hot Pressing

High strength particulate ceramic composites are in general reinforced by strong dispersoids, such as strong ceramic particles (SiC, TiB2, ZrO2, et al) and strong metallic particles (Mo, W, et al). In this work high strength ceramic composites with in-situ synthesized hexagonal boron nitride (h-BN) have been prepared and characterized. As an example, we manufactured mullite-BN composites by reactive hot pressing (RHP) using aluminum borates (9Al2O3·2B2O3 and 2Al2O3·B2O3) and silicon nitride as starting materials. The obtained material RHPed at 1800°C showed a strength of 540 MPa, which was 1.64 times higher than that of the monolithic mullite ceramics. TEM observation revealed that the composite had an isotropic microstructure with a fine mullite matrix grain size of less than 1 μm and a nano-sized h-BN platelets of about 200 nm in length and 60∼80 nm in thickness. The high strength was suggested to be from the reduced matrix grain size and the small toughening effect by the h-BN platelets. In addition, this kind of ceramic composite demonstrates low Young’s modulus that is beneficial to the thermal/mechanical shock resistance, and excellent machinability.

Influence of the base material on the mechanical behaviors of polycrystal-like meta-crystals

2021 ◽  
pp. 2150004
Author(s):  
J. Lertthanasarn ◽  
C. Liu ◽  
M.-S. Pham
Keyword(s):  
Synergistic Effects ◽  
High Surface ◽  
Base Material ◽  
High Strength ◽  
Yield Stability ◽  
Yield Behavior ◽  
Specific Strength ◽  
Base Materials ◽  
Lattice Materials ◽  
Strength And Stiffness

Architected lattice metamaterials offer extraordinary specific strength and stiffness that can be tailored through the architecture. Meta-crystals mimic crystalline strengthening features in crystalline alloys to obtain high strength and improved post-yield stability of lattice materials. This study investigates synergistic effects of the base material’s intrinsic crystalline microstructure and architected polycrystal-like architecture on the mechanical behavior of architected metamaterials. Four different polygrain-like meta-crystals were fabricated from 316L, Inconel 718 (IN718) and Ti6Al4V via laser powder bed fusion (L-PBF). While the elastic modulus of the meta-crystals did not vary significantly with the base material or the number of meta-grains, the strength of the meta-crystals showed strong increasing correlation with reducing the size of meta-grains. The differences between meta-crystals made by the three alloys were the most substantial in the post-yield behavior, where the 316L meta-crystals were the most stable while Ti6Al4V meta-crystals were the most erratic. The differences in the post-yield behavior were attributed to the base material’s ductility and intrinsic work-hardening. For all base materials, increasing the number of meta-grains improved the post-yield stability of meta-crystals. The tolerance to the processing defects also differed with the base material. Detrimental defects such as the high surface roughness on the downskin of the struts or the large, irregularly shaped pores near the surface of the struts led to early strut fracture in Ti6Al4V meta-crystals. In contrast, ductile IN718 was able to tolerate such defects, enabling the most significant synergistic strengthening across lengthscales to achieve architected materials of low relative density, but with a very high strength and an excellent energy absorption.

Nanomaterials and Nanocomposites Thermal and Mechanical Properties Modelling

2019 ◽  
pp. 234-256 ◽  
Author(s):  
Siddhartha Kosti
Keyword(s):  
Thermal Properties ◽  
Structural Properties ◽  
Base Material ◽  
High Strength ◽  
Mechanical And Thermal Properties ◽  
Thermal And Mechanical Properties ◽  
Weight Percentage ◽  
Structural Applications ◽  
Glass Frp ◽  
Selection Of

This chapter deals with the modelling of nanomaterial and nanocomposite mechanical and thermal properties. Enrichment in the technology requires materials having higher thermal properties or higher structural properties. Nanomaterials and nanocomposites can serve this purpose accurately for aerospace or thermal applications and structural applications respectively. The thermal system requires materials having high thermal conductivity while structural system requires materials having high strength. Selection of the material for particular application is very critical and requires knowledge and experience. Al, Cu, TiO2, Al2O3, etc. are considered for thermal applications while epoxy-glass, FRP, etc. are considered for structural applications. Modelling of these nanomaterials and nanocomposites is done with the help of different mathematical models available in the literature. Results show that addition of the nanoparticle/composite in the base material can enhance the thermal and structural properties. Results also show that amount of weight percentage added also affects the properties.

Nanomaterials and Nanocomposites Thermal and Mechanical Properties Modelling

2021 ◽  
pp. 180-199
Author(s):  
Siddhartha Kosti
Keyword(s):  
Thermal Properties ◽  
Structural Properties ◽  
Base Material ◽  
High Strength ◽  
Mechanical And Thermal Properties ◽  
Thermal And Mechanical Properties ◽  
Weight Percentage ◽  
Structural Applications ◽  
Glass Frp ◽  
Selection Of

This chapter deals with the modelling of nanomaterial and nanocomposite mechanical and thermal properties. Enrichment in the technology requires materials having higher thermal properties or higher structural properties. Nanomaterials and nanocomposites can serve this purpose accurately for aerospace or thermal applications and structural applications respectively. The thermal system requires materials having high thermal conductivity while structural system requires materials having high strength. Selection of the material for particular application is very critical and requires knowledge and experience. Al, Cu, TiO2, Al2O3, etc. are considered for thermal applications while epoxy-glass, FRP, etc. are considered for structural applications. Modelling of these nanomaterials and nanocomposites is done with the help of different mathematical models available in the literature. Results show that addition of the nanoparticle/composite in the base material can enhance the thermal and structural properties. Results also show that amount of weight percentage added also affects the properties.

Sign in / Sign up

Export Citation Format

Share Document