Latent Curing, Chemorheological, Kinetic, and Thermal Behaviors of Epoxy Resin Matrix for Prepregs

Author(s):  
Yeong Jae Kim ◽  
Sung Ho Choi ◽  
Seong Jae Lee ◽  
Keon-Soo Jang
Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2127
Author(s):  
Richard Fürst ◽  
Eliška Fürst ◽  
Tomáš Vlach ◽  
Jakub Řepka ◽  
Marek Pokorný ◽  
...  

Textile-reinforced concrete (TRC) is a material consisting of high-performance concrete (HPC) and tensile reinforcement comprised of carbon roving with epoxy resin matrix. However, the problem of low epoxy resin resistance at higher temperatures persists. In this work, an alternative to the epoxy resin matrix, a non-combustible cement suspension (cement milk) which has proven stability at elevated temperatures, was evaluated. In the first part of the work, microscopic research was carried out to determine the distribution of particle sizes in the cement suspension. Subsequently, five series of plate samples differing in the type of cement and the method of textile reinforcement saturation were designed and prepared. Mechanical experiments (four-point bending tests) were carried out to verify the properties of each sample type. It was found that the highest efficiency of carbon roving saturation was achieved by using finer ground cement (CEM 52.5) and the pressure saturation method. Moreover, this solution also exhibited the best results in the four-point bending test. Finally, the use of CEM 52.5 in the cement matrix appears to be a feasible variant for TRC constructions that could overcome problems with its low temperature resistance.


2020 ◽  
Vol 10 (3) ◽  
pp. 1159 ◽  
Author(s):  
Yingmei Xie ◽  
Hiroki Kurita ◽  
Ryugo Ishigami ◽  
Fumio Narita

Epoxy resins are a widely used common polymer due to their excellent mechanical properties. On the other hand, cellulose nanofiber (CNF) is one of the new generation of fibers, and recent test results show that CNF reinforced polymers have high mechanical properties. It has also been reported that an extremely low CNF addition increases the mechanical properties of the matrix resin. In this study, we prepared extremely-low CNF (~1 wt.%) reinforced epoxy resin matrix (epoxy-CNF) composites, and tried to understand the strengthening mechanism of the epoxy-CNF composite through the three-point flexural test, finite element analysis (FEA), and discussion based on organic chemistry. The flexural modulus and strength were significantly increased by the extremely low CNF addition (less than 0.2 wt.%), although the theories for short-fiber-reinforced composites cannot explain the strengthening mechanism of the epoxy-CNF composite. Hence, we propose the possibility that CNF behaves as an auxiliary agent to enhance the structure of the epoxy molecule, and not as a reinforcing fiber in the epoxy resin matrix.


2012 ◽  
Vol 510-511 ◽  
pp. 577-584 ◽  
Author(s):  
A. Quddos ◽  
Mohammad Bilal Khan ◽  
R.N. Khan ◽  
M.K.K. Ghauri

The impregnation of the fiber with a resin system, the polymeric matrix with the interface needs to be properly cured so that the dimensional stability of the matrix and the composite is ensured. A modified epoxy resin matrix was obtained with a reactive toughening agent and anhydride as a curing agent. The mechanical properties of the modified epoxy matrix and its fiber reinforced composites were investigated systematically. The polymeric matrix possessed many good properties, including high strength, high elongation at break, low viscosity, long pot life at room temperature, and good water resistance. The special attentions are given to the matrix due to its low out gassing, low water absorption and radiation resistance. In addition, the fiber-reinforced composites showed a high strength conversion ratio of the fiber and good fatigue resistance. The dynamic and static of the composite material were studied by thermo gravimetric analysis (TGA), Differential Scanning Calorimetry (DSC) and Scanning Electron Microscopy (SEM) with EDX. The influences of processing technique such as curing and proper mixing on the mechanical and interfacial properties were determined. The results demonstrated that the modified epoxy resin matrix is very suitable for applications in products fabricated with fiber-reinforced composites.


2015 ◽  
Vol 466 ◽  
pp. 100-107 ◽  
Author(s):  
Ran Li ◽  
Yizhuo Gu ◽  
Zhongjia Yang ◽  
Min Li ◽  
Shaokai Wang ◽  
...  

2005 ◽  
Vol 13 (5) ◽  
pp. 525-527
Author(s):  
Cheng Yiyun ◽  
Cui Ronghui ◽  
He Pingsheng

This study presents a new method of preparing Mg(OH)2/epoxy resin nanocomposites. An epoxy resin micro-emulsion is taken as a micro-reactor for the formation of Mg(OH)2 nano-crystals. After the reaction, the collected epoxy proved to be a composite with embedded nano-Mg(OH)2. Transmission electron microscopy (TEM) indicated that the Mg(OH)2 nano-crystals were dispersed uniformly in cured epoxy resin matrix.


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