scholarly journals Efficient Continuous Hydrothermal Flow Synthesis of Carbon Quantum Dots from a Targeted Biomass Precursor for On–Off Metal Ions Nanosensing

2021 ◽  
Vol 9 (6) ◽  
pp. 2559-2569 ◽  
Author(s):  
Ioan-Alexandru Baragau ◽  
Nicholas P. Power ◽  
David J. Morgan ◽  
Richard A. Lobo ◽  
Christopher S. Roberts ◽  
...  
2020 ◽  
Vol 8 (6) ◽  
pp. 3270-3279 ◽  
Author(s):  
Ioan-Alexandru Baragau ◽  
Nicholas P. Power ◽  
David J. Morgan ◽  
Tobias Heil ◽  
Richard Alvarez Lobo ◽  
...  

We present the first report of continuous hydrothermal flow synthesis of N-doped carbon quantum dots, with excitation-independent optical properties. They display high selectivity and sensitivity for Cr(vi), and are thus suitable for environmental applications and beyond.


2021 ◽  
Vol 405 ◽  
pp. 126631 ◽  
Author(s):  
Ioan-Alexandru Baragau ◽  
Zhen Lu ◽  
Nicholas P. Power ◽  
David J. Morgan ◽  
James Bowen ◽  
...  

RSC Advances ◽  
2017 ◽  
Vol 7 (24) ◽  
pp. 14716-14720 ◽  
Author(s):  
Suela Kellici ◽  
John Acord ◽  
Nicholas P. Power ◽  
David J. Morgan ◽  
Paolo Coppo ◽  
...  

A rapid and environmentally benign synthesis of green fluorescent graphene quantum dots (GQD) with low cytotoxicity via Continuous Hydrothermal Flow Synthesis (CHFS) aided by calix[4]arene tetrasulfonic acid (SCX4) as a particle size limiting agent.


A green and simple synthesis of carbon quantum dots (CQDs) was derived from dried mint leaves by hydrothermal method. Crystalline structure of the synthesized CQDs was characterized with X-ray diffraction (XRD) method. The morphological properties of the CQDs were investigated with transmission electron microscopy (TEM). The optical behaviors of the CQDs were examined with fourier transfom infrared spectrophotometer (FT-IR), ultraviolet visible (UV-Vis) and photoluminescence spectrophotometer techniques. Crystalline structure of the CQDs was found as amorphous in nature and the average diameter of the CDs was calculated as 8.13 nm from TEM study. According to the fluorescence emission spectra of the samples, synthesized CQDs was sensitive to mainly Ag(I), Cr(III) and Fe(III) ions. Especially, Ag(I) was the most sensible compared to other metal ions. Quenching effect of the CQDs was also evaluated by using ascorbic acid to metal ions added CQDs samples. Ascorbic acid showed the quenching effect for all the metal ion added samples except Sn(II) ion.


2019 ◽  
Vol 962 ◽  
pp. 36-40
Author(s):  
Lan Ching Sim ◽  
Jia Min Khor ◽  
Kah Hon Leong ◽  
Pichiah Saravanan

In this work, carbon quantum dots (C-dots) was successfully synthesized by hydrothermal treatment using dried leaves as green precursor for metal sensing. The performance of C-dots when detecting metal ions in water will be evaluated by testing with different types of metal stock solutions. Quenching effect of fluorescence C-dots solution was observed in the presence of different metal ions. C-dots is more selective towards Fe3+ compared to other metal ions.


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