The influence of hold time on the onset of plastic deformation in silicon

There are two types of edge defects common to glass knives as typically prepared for microtomy purposes: 1) striations and 2) edge chipping. The former is a function of the free breaking process while edge chipping results from usage or bumping of the edge. Because glass has no well defined planes in its structure, it should be highly resistant to plastic deformation of any sort, including tensile loading. In practice, prevention of microscopic surface flaws is impossible. The surface flaws produce stress concentrations so that tensile strengths in glass are typically 10-20 kpsi and vary only slightly with composition. If glass can be kept in compression, wherein failure is literally unknown (1), it will remain intact for long periods of time. Forces acting on the tool in microtomy produce a resultant force that acts to keep the edge in compression.

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Stereo Electron Microscopy Applied to High Resolution Freeze-Etch Replicas

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100068527 ◽

1970 ◽

Vol 28 ◽

pp. 306-307

Author(s):

L. Andrew Staehelin

Keyword(s):

Electron Microscopy ◽

Plastic Deformation ◽

High Resolution ◽

Smooth Surfaces ◽

Small Particles ◽

Membrane Surfaces ◽

Wide Acceptance ◽

New Information ◽

Number Of Particles ◽

Small Holes

Freeze-etched membranes usually appear as relatively smooth surfaces covered with numerous small particles and a few small holes (Fig. 1). In 1966 Branton (1“) suggested that these surfaces represent split inner mem¬brane faces and not true external membrane surfaces. His theory has now gained wide acceptance partly due to new information obtained from double replicas of freeze-cleaved specimens (2,3) and from freeze-etch experi¬ments with surface labeled membranes (4). While theses studies have fur¬ther substantiated the basic idea of membrane splitting and have shown clearly which membrane faces are complementary to each other, they have left the question open, why the replicated membrane faces usually exhibit con¬siderably fewer holes than particles. According to Branton's theory the number of holes should on the average equal the number of particles. The absence of these holes can be explained in either of two ways: a) it is possible that no holes are formed during the cleaving process e.g. due to plastic deformation (5); b) holes may arise during the cleaving process but remain undetected because of inadequate replication and microscope techniques.

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Plastic Deformation in Microtomed Sections

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100066346 ◽

1971 ◽

Vol 29 ◽

pp. 458-459

Author(s):

J. Temple Black

Keyword(s):

Plastic Deformation ◽

Plastic Strain ◽

Applied Stress ◽

Elastic Strain ◽

High Strain ◽

Tool Material ◽

Cutting Edge ◽

Material Structure ◽

Geometrical Constraints

The output of the ultramicrotomy process with its high strain levels is dependent upon the input, ie., the nature of the material being machined. Apart from the geometrical constraints offered by the rake and clearance faces of the tool, each material is free to deform in whatever manner necessary to satisfy its material structure and interatomic constraints. Noncrystalline materials appear to survive the process undamaged when observed in the TEM. As has been demonstrated however microtomed plastics do in fact suffer damage to the top and bottom surfaces of the section regardless of the sharpness of the cutting edge or the tool material. The energy required to seperate the section from the block is not easily propogated through the section because the material is amorphous in nature and has no preferred crystalline planes upon which defects can move large distances to relieve the applied stress. Thus, the cutting stresses are supported elastically in the internal or bulk and plastically in the surfaces. The elastic strain can be recovered while the plastic strain is not reversible and will remain in the section after cutting is complete.

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Surface Structure in Microtomed Sections Caused by Glass and Diamond Knives

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100066334 ◽

1971 ◽

Vol 29 ◽

pp. 456-457

Author(s):

J. Temple Black ◽

William G. Boldosser

Keyword(s):

Plastic Deformation ◽

Epoxy Resin ◽

Carbon Coating ◽

Surface Damage ◽

Body Angle ◽

Normal Manner ◽

Bottom Side ◽

Cutting Direction ◽

Made In ◽

Diamond Knife

Ultramicrotomy produces plastic deformation in the surfaces of microtomed TEM specimens which can not generally be observed unless special preparations are made. In this study, a typical biological composite of tissue (infundibular thoracic attachment) infiltrated in the normal manner with an embedding epoxy resin (Epon 812 in a 60/40 mixture) was microtomed with glass and diamond knives, both with 45 degree body angle. Sectioning was done in Portor Blum Mt-2 and Mt-1 microtomes. Sections were collected on formvar coated grids so that both the top side and the bottom side of the sections could be examined. Sections were then placed in a vacuum evaporator and self-shadowed with carbon. Some were chromium shadowed at a 30 degree angle. The sections were then examined in a Phillips 300 TEM at 60kv.Carbon coating (C) or carbon coating with chrom shadowing (C-Ch) makes in effect, single stage replicas of the surfaces of the sections and thus allows the damage in the surfaces to be observable in the TEM. Figure 1 (see key to figures) shows the bottom side of a diamond knife section, carbon self-shadowed and chrom shadowed perpendicular to the cutting direction. Very fine knife marks and surface damage can be observed.

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Investigation of shock-wave deformation history from recovered structure

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100143754 ◽

1986 ◽

Vol 44 ◽

pp. 434-435

Author(s):

M.A. Mogilevsky ◽

L.S. Bushnev

Keyword(s):

Shock Wave ◽

Plastic Deformation ◽

Dislocation Density ◽

Shock Waves ◽

Shock Front ◽

Single Crystals ◽

Residual Deformation ◽

Deformation Structure ◽

Deformation History ◽

Deformation Velocity

Single crystals of Al were loaded by 15 to 40 GPa shock waves at 77 K with a pulse duration of 1.0 to 0.5 μs and a residual deformation of ∼1%. The analysis of deformation structure peculiarities allows the deformation history to be re-established.After a 20 to 40 GPa loading the dislocation density in the recovered samples was about 1010 cm-2. By measuring the thickness of the 40 GPa shock front in Al, a plastic deformation velocity of 1.07 x 108 s-1 is obtained, from where the moving dislocation density at the front is 7 x 1010 cm-2. A very small part of dislocations moves during the whole time of compression, i.e. a total dislocation density at the front must be in excess of this value by one or two orders. Consequently, due to extremely high stresses, at the front there exists a very unstable structure which is rearranged later with a noticeable decrease in dislocation density.

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Construction of plastic contact deformation maps on ceramics: a case study on aluminum nitride

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100165641 ◽

1996 ◽

Vol 54 ◽

pp. 636-637

Author(s):

D. L. Callahan

Keyword(s):

Plastic Deformation ◽

Aluminum Nitride ◽

Mechanical Response ◽

Three Dimensional ◽

Bright Field Image ◽

Perfectly Plastic ◽

Contrast Analysis ◽

Deformation Patterns

Modern polishing, precision machining and microindentation techniques allow the processing and mechanical characterization of ceramics at nanometric scales and within entirely plastic deformation regimes. The mechanical response of most ceramics to such highly constrained contact is not predictable from macroscopic properties and the microstructural deformation patterns have proven difficult to characterize by the application of any individual technique. In this study, TEM techniques of contrast analysis and CBED are combined with stereographic analysis to construct a three-dimensional microstructure deformation map of the surface of a perfectly plastic microindentation on macroscopically brittle aluminum nitride.The bright field image in Figure 1 shows a lg Vickers microindentation contained within a single AlN grain far from any boundaries. High densities of dislocations are evident, particularly near facet edges but are not individually resolvable. The prominent bend contours also indicate the severity of plastic deformation. Figure 2 is a selected area diffraction pattern covering the entire indentation area.

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Electron microscopy study of shock synthesis of silicides

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100151647 ◽

1993 ◽

Vol 51 ◽

pp. 1162-1163

Author(s):

Kenneth S. Vecchio

Keyword(s):

Shock Wave ◽

Plastic Deformation ◽

Close Contact ◽

Microscopy Study ◽

High Energy ◽

Electron Microscopy Study ◽

Powder Materials ◽

Porous Powder ◽

Wave Effects ◽

Wave Passage

Shock-induced reactions (or shock synthesis) have been studied since the 1960’s but are still poorly understood, partly due to the fact that the reaction kinetics are very fast making experimental analysis of the reaction difficult. Shock synthesis is closely related to combustion synthesis, and occurs in the same systems that undergo exothermic gasless combustion reactions. The thermite reaction (Fe2O3 + 2Al -> 2Fe + Al2O3) is prototypical of this class of reactions. The effects of shock-wave passage through porous (powder) materials are complex, because intense and non-uniform plastic deformation is coupled with the shock-wave effects. Thus, the particle interiors experience primarily the effects of shock waves, while the surfaces undergo intense plastic deformation which can often result in interfacial melting. Shock synthesis of compounds from powders is triggered by the extraordinarily high energy deposition rate at the surfaces of the powders, forcing them in close contact, activating them by introducing defects, and heating them close to or even above their melting temperatures.

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Electron microscope studies of the plastic deformation of ternary alloys based on GaAs

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100178732 ◽

1990 ◽

Vol 48 (4) ◽

pp. 1120-1120

Author(s):

R. Haswell ◽

U. Bangert ◽

P. Charsley

Keyword(s):

Plastic Deformation ◽

Electron Microscope ◽

Room Temperature ◽

Stacking Faults ◽

The Other ◽

Ternary Alloys ◽

Dislocation Mobility ◽

Semiconducting Materials ◽

Micro Indentation

A knowledge of the behaviour of dislocations in semiconducting materials is essential to the understanding of devices which use them . This work is concerned with dislocations in alloys related to the semiconductor GaAs . Previous work on GaAs has shown that microtwinning occurs on one of the <110> rosette arms after indentation in preference to the other . We have shown that the effect of replacing some of the Ga atoms by Al results in microtwinning in both of the rosette arms.In the work to be reported dislocations in specimens of different compositions of Gax Al(1-x) As and Gax In(1-x) As have been studied by using micro indentation on a (001) face at room temperature . A range of electron microscope techniques have been used to investigate the type of dislocations and stacking faults/microtwins in the rosette arms , which are parallel to the [110] and [10] , as a function of composition for both alloys . Under certain conditions microtwinning occurs in both directions . This will be discussed in terms of the dislocation mobility.

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