scholarly journals High-Energy X-Rays: A tool for Advanced Bulk Investigations in Materials Science and Physics

2003 ◽  
Vol 35 (3-4) ◽  
pp. 219-252 ◽  
Author(s):  
Klaus-Dieter Liss ◽  
Arno Bartels ◽  
Andreas Schreyer ◽  
Helmut Clemens
Keyword(s):  
Materials Science ◽  
High Energy ◽  
X Rays

The combination of these techniques is a strong issue for the construction and development of future instruments.

Detector commissioning and development for PETRA-III

2010 ◽  
Vol 1 (SRMS-7) ◽  
Author(s):  
David Pennicard ◽  
Heinz Graafsma ◽  
Michael Lohmann
Keyword(s):  
High Speed ◽  
Materials Science ◽  
Dynamic Range ◽  
Photon Counting ◽  
High Energy ◽  
X Rays ◽  
Silicon Detectors ◽  
Time Resolved ◽  
Wide Range ◽  
Synchrotron Light

The new synchrotron light source PETRA-III produced its first beam last year. The extremely high brilliance of PETRA-III and the large energy range of many of its beamlines make it useful for a wide range of experiments, particularly in materials science. The detectors at PETRA-III will need to meet several requirements, such as operation across a wide dynamic range, high-speed readout and good quantum efficiency even at high photon energies. PETRA-III beamlines with lower photon energies will typically be equipped with photon-counting silicon detectors for two-dimensional detection and silicon drift detectors for spectroscopy and higher-energy beamlines will use scintillators coupled to cameras or photomultiplier tubes. Longer-term developments include ‘high-Z’ semiconductors for detecting high-energy X-rays, photon-counting readout chips with smaller pixels and higher frame rates and pixellated avalanche photodiodes for time-resolved experiments.

scholarly journals Depth-Resolved Residual Stress Analysis with High-Energy Synchrotron X-Rays Using a Conical Slit Cell

2013 ◽  
Vol 768-769 ◽  
pp. 72-75 ◽  
Author(s):  
Peter Staron ◽  
Torben Fischer ◽  
Jozef Keckes ◽  
Sonja Schratter ◽  
Thomas Hatzenbichler ◽  
...  
Keyword(s):  
Residual Stress ◽  
Stress Analysis ◽  
Cross Sections ◽  
Materials Science ◽  
Steel Wire ◽  
High Energy ◽  
X Rays ◽  
Energy Materials ◽  
Residual Stress Analysis ◽  
Good Agreement

A conical slit cell for depth-resolved diffraction of high-energy X-rays was used for residual stress analysis at the high-energy materials science synchrotron beamline HEMS at PETRA III. With a conical slit width of 20 µm and beam cross-sections of 50 µm, a spatial resolution in beam direction of 0.8 mm was achieved. The setup was used for residual stress analysis in a drawn steel wire with 8.3 mm diameter. The residual stress results were in very good agreement with results of a FE simulation.

Three-Dimensional X-Ray Diffraction Microscopy Using High-Energy X-Rays

MRS Bulletin ◽  
2004 ◽  
Vol 29 (3) ◽  
pp. 166-169 ◽  
Author(s):  
Henning F. Poulsen ◽  
Dorte Juul Jensen ◽  
Gavin B.M. Vaughan
Keyword(s):  
Materials Science ◽  
Three Dimensional ◽  
High Energy ◽  
Polycrystalline Materials ◽  
X Rays ◽  
X Ray Diffraction ◽  
X Ray ◽  
Reconstruction Methods ◽  
The Individual ◽  
Individual Grains

AbstractThree-dimensional x-ray diffraction (3DXRD) microscopy is a tool for fast and nondestructive characterization of the individual grains, subgrains, and domains inside bulk materials. The method is based on diffraction with very penetrating hard x-rays (E ≥ 50 keV), enabling 3D studies of millimeter-to-centimeter-thick specimens.The position, volume, orientation, and elastic and plastic strain can be derived for hundreds of grains simultaneously. Furthermore, by applying novel reconstruction methods, 3D maps of the grain boundaries can be generated. The 3DXRD microscope in use at the European Synchrotron Radiation Facility in Grenoble, France, has a spatial resolution of ∼5 μm and can detect grains as small as 150 nm. The technique enables, for the first time, dynamic studies of the individual grains within polycrystalline materials. In this article, some fundamental materials science applications of 3DXRD are reviewed: studies of nucleation and growth kinetics during recrystallization, recovery, and phase transformations, as well as studies of polycrystal deformation.

scholarly journals Depth-Resolved Residual Stress Analysis with Conical Slits for High-Energy X-Rays

2013 ◽  
Vol 772 ◽  
pp. 3-7 ◽  
Author(s):  
Peter Staron ◽  
Torben Fischer ◽  
Eike Henning Eims ◽  
Sebastian Frömbgen ◽  
Norbert Schell ◽  
...  
Keyword(s):  
Residual Stress ◽  
Cross Sections ◽  
Materials Science ◽  
High Energy ◽  
X Rays ◽  
Stress Distributions ◽  
Energy Materials ◽  
Welded Steel ◽  
Overlap Joint ◽  
Good Agreement

A conical slit cell for depth-resolved diffraction of high-energy X-rays was tested at the high-energy materials science beamline HEMS at PETRA III and used for the analysis of residual stresses in a laser beam welded steel overlap joint. With a conical slit width of 20 µm and beam cross-sections below 100 µm, depth resolutions well below 1 mm were achieved. The residual stress distributions obtained from the steel joint were in very good agreement with previous results from neutron diffraction measurements, although they were still noisier because of inferior grain statistics.

The Basic Physical Principles of Ion, Electron, and X-Ray Detectors and Their Application to Microanalysis

1985 ◽  
Vol 43 ◽  
pp. 154-157
Author(s):  
A.J. Tousimis
Keyword(s):  
Ion Beam ◽  
Depth Resolution ◽  
Sample Surface ◽  
High Energy ◽  
X Rays ◽  
X Ray ◽  
Electrons And Ions ◽  
Spatial Depth ◽  
Minimum Surface Area ◽  
Physical Principles

An integral and of prime importance of any microtopography and microanalysis instrument system is its electron, x-ray and ion detector(s). The resolution and sensitivity of the electron microscope (TEM, SEM, STEM) and microanalyzers (SIMS and electron probe x-ray microanalyzers) are closely related to those of the sensing and recording devices incorporated with them.Table I lists characteristic sensitivities, minimum surface area and depth analyzed by various methods. Smaller ion, electron and x-ray beam diameters than those listed, are possible with currently available electromagnetic or electrostatic columns. Therefore, improvements in sensitivity and spatial/depth resolution of microanalysis will follow that of the detectors. In most of these methods, the sample surface is subjected to a stationary, line or raster scanning photon, electron or ion beam. The resultant radiation: photons (low energy) or high energy (x-rays), electrons and ions are detected and analyzed.

“Cartography” in 7-Dimensions at CHESS: Mapping of Structure in Real Space, Reciprocal Space, and Time Using High-Energy X-rays

2020 ◽  
Vol 33 (6) ◽  
pp. 11-16
Author(s):  
K. E. Nygren, ◽  
D. C. Pagan, ◽  
J. P. C. Ruff ◽  
E. Arenholz ◽  
J. D. Brock
Keyword(s):  
High Energy ◽  
Real Space ◽  
Reciprocal Space ◽  
X Rays ◽  
Space And Time

scholarly journals The interstellar medium in young supernova remnants: key to the production of cosmic X-rays and $\gamma $-rays

2021 ◽  
Vol 366 (6) ◽  
Author(s):  
Hidetoshi Sano ◽  
Yasuo Fukui
Keyword(s):  
Interstellar Medium ◽  
Supernova Remnants ◽  
Cosmic Ray ◽  
High Energy ◽  
X Rays ◽  
Interstellar Gas ◽  
High Energy Radiation ◽  
Dense Cores ◽  
The Relationship ◽  
Turbulent Velocity Field

AbstractWe review recent progress in elucidating the relationship between high-energy radiation and the interstellar medium (ISM) in young supernova remnants (SNRs) with ages of ∼2000 yr, focusing in particular on RX J1713.7−3946 and RCW 86. Both SNRs emit strong nonthermal X-rays and TeV $\gamma $ γ -rays, and they contain clumpy distributions of interstellar gas that includes both atomic and molecular hydrogen. We find that shock–cloud interactions provide a viable explanation for the spatial correlation between the X-rays and ISM. In these interactions, the supernova shocks hit the typically pc-scale dense cores, generating a highly turbulent velocity field that amplifies the magnetic field up to 0.1–1 mG. This amplification leads to enhanced nonthermal synchrotron emission around the clumps, whereas the cosmic-ray electrons do not penetrate the clumps. Accordingly, the nonthermal X-rays exhibit a spatial distribution similar to that of the ISM on the pc scale, while they are anticorrelated at sub-pc scales. These results predict that hadronic $\gamma $ γ -rays can be emitted from the dense cores, resulting in a spatial correspondence between the $\gamma $ γ -rays and the ISM. The current pc-scale resolution of $\gamma $ γ -ray observations is too low to resolve this correspondence. Future $\gamma $ γ -ray observations with the Cherenkov Telescope Array will be able to resolve the sub-pc-scale $\gamma $ γ -ray distribution and provide clues to the origin of these cosmic $\gamma $ γ -rays.

scholarly journals Introducing the HD+B model for pulsar wind nebulae: a hybrid hydrodynamics/radiative approach

2020 ◽  
Vol 494 (3) ◽  
pp. 4357-4370
Author(s):  
B Olmi ◽  
D F Torres
Keyword(s):  
Gamma Ray ◽  
High Energy ◽  
Theoretical Modelling ◽  
X Rays ◽  
Pulsar Wind Nebulae ◽  
New Approach ◽  
Energy Gamma ◽  
Radiative Model ◽  
Pulsar Wind

ABSTRACT Identification and characterization of a rapidly increasing number of pulsar wind nebulae is, and will continue to be, a challenge of high-energy gamma-ray astrophysics. Given that such systems constitute -by far- the most numerous expected population in the TeV regime, such characterization is important not only to learn about the sources per se from an individual and population perspective, but also to be able to connect them with observations at other frequencies, especially in radio and X-rays. Also, we need to remove the emission from nebulae in highly confused regions of the sky for revealing other underlying emitters. In this paper, we present a new approach for theoretical modelling of pulsar wind nebulae: a hybrid hydrodynamic-radiative model able to reproduce morphological features and spectra of the sources, with relatively limited numerical cost.

Recent Developments In Monochromatic Microprobe X-Ray Fluorescence (MMXRF)

1998 ◽  
Vol 4 (S2) ◽  
pp. 378-379
Author(s):  
Z. W. Chen ◽  
D. B. Wittry
Keyword(s):  
Materials Science ◽  
High Vacuum ◽  
Three Dimensional ◽  
High Sensitivity ◽  
X Rays ◽  
Fluorescence Excitation ◽  
X Ray ◽  
Quantitative Microanalysis ◽  
Recent Developments ◽  
Fifth Order

A monochromatic x-ray microprobe based on a laboratory source has recently been developed in our laboratory and used for fluorescence excitation. This technique provides high sensitivity (ppm to ppb), nondestructive, quantitative microanalysis with minimum sample preparation and does not require a high vacuum specimen chamber. It is expected that this technique (MMXRF) will have important applications in materials science, geological sciences and biological science.Three-dimensional focusing of x-rays can be obtained by using diffraction from doubly curved crystals. In our MMXRF setup, a small x-ray source was produced by the bombardment of a selected target with a focused electron beam and a toroidal mica diffractor with Johann pointfocusing geometry was used to focus characteristic x-rays from the source. In the previous work ∼ 108 photons/s were obtained in a Cu Kα probe of 75 μm × 43 μm in the specimen plane using the fifth order reflection of the (002) planes of mica.

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