Effects of elastic indenter deformation on spherical instrumented indentation tests: the reduced elastic modulus

Author(s):  
Sara Aida Rodríguez ◽  
Jorge Alcalá ◽  
Roberto Martins Souza
Holzforschung ◽  
2009 ◽  
Vol 63 (4) ◽  
Author(s):  
Stefanie Stanzl-Tschegg ◽  
Wilfried Beikircher ◽  
Dieter Loidl

Abstract Thermal modification is a well established method to improve the dimensional stability and the durability for outdoor use of wood. Unfortunately, these improvements are usually accompanied with a deterioration of mechanical performance (e.g., reduced strength or higher brittleness). In contrast, our investigations of the hardness properties in the longitudinal direction of beech wood revealed a significant improvement with thermal modification. Furthermore, we applied instrumented indentation tests on different hierarchical levels of wood structure (growth ring and cell wall level) to gain closer insights on the mechanisms of thermal treatment of wood on mechanical properties. This approach provides a variety of mechanical data (e.g., elastic parameters, hardness parameters, and viscoelastic properties) from one single experiment. Investigations on the influence of thermal treatment on the mechanical properties of beech revealed similar trends on the growth ring as well as the on the cell wall level of the wood structure.


2001 ◽  
Vol 16 (6) ◽  
pp. 1660-1667 ◽  
Author(s):  
L. Riester ◽  
T. J. Bell ◽  
A. C. Fischer-Cripps

The present work shows how data obtained in a depth-sensing indentation test using a Knoop indenter may be analyzed to provide elastic modulus and hardness of the specimen material. The method takes into account the elastic recovery along the direction of the short axis of the residual impression as the indenter is removed. If elastic recovery is not accounted for, the elastic modulus and hardness are overestimated by an amount that depends on the ratio of E/H of the specimen material. The new method of analysis expresses the elastic recovery of the short diagonal of the residual impression into an equivalent face angle for one side of the Knoop indenter. Conventional methods of analysis using this corrected angle provide results for modulus and hardness that are consistent with those obtained with other types of indenters.


2013 ◽  
Vol 668 ◽  
pp. 616-620
Author(s):  
Shuai Huang ◽  
Huang Yuan

Computational simulations of indentations in elastic-plastic materials showed overestimate in determining elastic modulus using the Oliver & Pharr’s method. Deviations significantly increase with decreasing material hardening. Based on extensive finite element computations the correlation between elastic-plastic material property and indentation has been carried out. A modified method was introduced for estimating elastic modulus from dimensional analysis associated with indentation data. Experimental verifications confirm that the new method produces more accurate prediction of elastic modulus than the Oliver & Pharr’s method.


2020 ◽  
Vol 6 (2) ◽  
pp. 65-70
Author(s):  
Mark V. Weintraub ◽  
Nina S. Kozlova ◽  
Evgeniya V. Zabelina ◽  
Mikhail I. Petrzhik

The effect of growth conditions, anisotropy and polarity of specimens on the mechanical properties of lanthanum-gallium tantalate La3Ta0.5Ga5.5O14 single crystals grown in different atmospheres (argon (Ar), argon with oxygen addition (Ar+(<2%)O2 and Ar+(2%)O2) and air) was studied. The test specimens for the measurements were cut perpendicularly to a 3rd order axis (Z cuts) and in polar directions perpendicular to a 2nd order axis (Y cuts). The polarity of the Y cut specimens was tested by piezoelectric response. The brittleness was evaluated by microindentation at 3, 5, 10 and 25 g loads. The brittleness proved to show itself at a 5 g and the higher loads regardless of growth atmosphere. Therefore microhardness tests were done at loads of within 3 g. The microhardness HV of the specimens was measured with an DM 8B Affri microhardness tester by Vickers methods. The hardness H, elastic modulus E and elastic recovery coefficient R were measured with a Berkovich pyramid on a CSM Nano-Hardness Tester using the instrumented indentation (nanoindentation) method. Growth atmosphere was shown to affect the mechanical properties of lanthanum-gallium tantalate crystals: crystals grown in an oxygen-free argon atmosphere had the lowest microhardness, hardness, elastic modulus and elastic recovery coefficient. The lowest microhardness was detected in Z cut specimens regardless of growth atmosphere. The mechanical properties of polar Y cuts proved to be anisotropic: the microhardness, hardness, elastic modulus and elastic recovery coefficient of these cuts were lower for positive cuts than for negative ones regardless of growth atmosphere. Y and Z cut langatate specimens grown in argon with less than two percent oxygen exhibited strong elastic modulus and elastic recovery coefficient anisotropy.


2012 ◽  
Vol 198-199 ◽  
pp. 193-196
Author(s):  
De Jun Ma ◽  
Jun Hong Guo ◽  
Wei Chen ◽  
Zhong Kang Song

Based on dimensional analysis, finite element numerical calculation is undertaken on elastic–plastic solids to investigate the relationship between instrumented indentation nominal hardness Hn and reduced elastic modulus Er for three different apex angle indenters. The half-included angles of axisymetric conical indenter models are 62.9°, 70.3°and 85.566° which are corresponding to the real indenters of cube corner indenter with 60° face angle, Berkovich indenter with 65.27° face angle and cube corner indenter with 85° face angle, respectively. The relationship between a nominal hardness/reduced elastic modulus (Hn/Er) and elastic work/total indentation work (We/Wt) is established with a sixth-order polynomial form for each apex angle indenter. For rigid indenter of instrumented indentation model, reduced elastic modulus Er=1/[(1+v2)/E], where E and v are elastic modulus and Poisson’s ratio of the indented material. Therefore, Hn/Er–We/Wt relationship can be used to give estimates of E. Accuracy estimation for the each relationship of each half-included angle indenter shows that the large half-included angle of 85.566° gives better Er measurement error of +11.56% for a low yield strength material(e.g., materials for which σy=100MPa, n=0 and E=200GPa), while for the smaller half-included angle of 62.9° or 70.3° indenter, the measurement error is > ±12.74%. The research in this paper confirms that Hn/Er–We/Wt relationship of large apex angle indenter such as 85.566° half-included angle is recommended to be used for estimating the elastic modulus E of indented material.


2016 ◽  
Vol 94 ◽  
pp. 170-179 ◽  
Author(s):  
M. Yetna N'Jock ◽  
F. Roudet ◽  
M. Idriss ◽  
O. Bartier ◽  
D. Chicot

2009 ◽  
Vol 24 (6) ◽  
pp. 1950-1959 ◽  
Author(s):  
N. Hakiri ◽  
A. Matsuda ◽  
M. Sakai

In instrumented indentation tests for a thin film coating on a substrate (film/substrate composite), it is well known that the substrate-affected contact area estimated through conventional approximations includes significant uncertainties, leading to a crucial difficulty in determining the elastic modulus and the contact hardness. To overcome this difficulty, an instrumented indentation microscope that enables researchers to make an in situ determination of the contact area is applied to an elastoplastic film on substrates having various values of their elastic moduli. Using the indentation microscope, the substrate-affected indentation contact parameters including contact hardness of the film/substrate composites are determined directly as well as quantitatively without any undesirable assumptions and approximations associated with the contact area estimate. The effect of a stiffer substrate on the contact profile of impression is significant, switching the profile from sinking in to piling up during penetration, and resulting in the substrate-affected contact hardness being highly enhanced at deeper penetrations. Through the present experimental study, it is demonstrated how efficient that instrumented indentation microscopy is in determining the substrate-affected elastoplastic contact parameters of film/substrate composite systems.


2001 ◽  
Vol 16 (7) ◽  
pp. 2149-2157 ◽  
Author(s):  
A. C. Fischer-Cripps

The present work is concerned with the methods of simulation of data obtained from depth-sensing submicron indentation testing. Details of analysis methods for both spherical and Berkovich indenters using multiple or single unload points are presented followed by a detailed treatment of a method for simulating an experimental load–displacement response where the material properties such as elastic modulus and hardness are given as inputs. A comparison between simulated and experimental data is given.


2006 ◽  
Vol 21 (7) ◽  
pp. 1680-1686
Author(s):  
L.Z. Liu ◽  
Y.W. Bao ◽  
Y.C. Zhou

Finite element analyses were carried out to simulate the loading, unloading, and reloading processes of indentation tests. It was found that the validity of applying the elastic contact theory to the indentation unloading process is strongly related to the strain hardening and residual stress in impression. It is the combination of strain hardening and residual stress that causes the unloading or reloading curves to show elastic loading in the range from zero to the maximum load whereas the reloading curve on the impression without strain hardening and residual stress shows elastic–plastic loading in the same range. These computations indicate that applying the elastic contact theory to the unloading or reloading processes, the fundamental prerequisite of the instrumented indentation technique, is valid because of the existence of strain hardening and residual stress. The mechanism of this hardening effect is discussed through energy analysis.


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