Superconducting state above the boiling point of liquid nitrogen in the GaH3compound

2013 ◽  
Vol 27 (1) ◽  
pp. 015003 ◽  
Author(s):  
R Szczȩśniak ◽  
A P Durajski
2014 ◽  
Vol 31 (3) ◽  
pp. 647-655 ◽  
Author(s):  
Scott N. Paine ◽  
David D. Turner ◽  
Nils Küchler

Abstract An absorbing load in a liquid nitrogen bath is commonly used as a radiance standard for calibrating radiometers operating at microwave to infrared wavelengths. It is generally assumed that the physical temperature of the load is stable and equal to the boiling point temperature of pure N2 at the ambient atmospheric pressure. However, this assumption will fail to hold when air movement, as encountered in outdoor environments, allows O2 gas to condense into the bath. Under typical conditions, initial boiling point drift rates of order 25 mK min−1 can occur, and the boiling point of a bath maintained by repeated refilling with pure N2 can eventually shift by approximately 2 K. Laboratory bench tests of a liquid nitrogen bath under simulated wind conditions are presented together with an example of an outdoor radiometer calibration that demonstrates the effect, and the physical processes involved are explained in detail. A key finding is that in windy conditions, changes in O2 volume fraction are related accurately to fractional changes in bath volume due to boiloff, independent of wind speed. This relation can be exploited to ensure that calibration errors due to O2 contamination remain within predictable bounds.


1989 ◽  
Vol 4 (5) ◽  
pp. 1111-1115 ◽  
Author(s):  
M. H. Ghandehari ◽  
S. G. Brass

Combinations of inert atmosphere sintering and oxygen atmosphere sintering have previously been reported as necessary for the synthesis of LaBa2Cu3Oy superconductors which achieve zero resistance at temperatures above 90 K. Sintering under oxygen atmosphere only is known to produce La(1+x)Ba(2−x)Cu3Oy, in which La is substituted for Ba in the crystal lattice. The latter substituted compounds achieve zero resistance at temperatures well below the boiling point of liquid nitrogen. In this work, we show that during the initial inert atmosphere sintering step, LaBa2Cu3Oy powder decomposes, in part, into several intermediate compounds. These compounds are then recombined in the subsequent oxygen atmosphere sintering step to form LaBa2Cu3Oy, which achieves zero resistance at temperatures above 90 K. We propose that the net effect of these two processing steps is to inhibit the substitution of La for Ba in the lattice of the fully processed material.


2020 ◽  
Vol 227 ◽  
pp. 115903
Author(s):  
P.A. Gushchin ◽  
V.A. Lubimenko ◽  
D.A. Petrova ◽  
E.V. Ivanov ◽  
I.M. Kolesnikov ◽  
...  

Author(s):  
Claude Lechene

Electron probe microanalysis of frozen hydrated kidneysThe goal of the method is to measure on the same preparation the chemical elemental content of the renal luminal tubular fluid and of the surrounding renal tubular cells. The following method has been developed. Rat kidneys are quenched in solid nitrogen. They are trimmed under liquid nitrogen and mounted in a copper holder using a conductive medium. Under liquid nitrogen, a flat surface is exposed by sawing with a diamond saw blade at constant speed and constant pressure using a custom-built cryosaw. Transfer into the electron probe column (Cameca, MBX) is made using a simple transfer device maintaining the sample under liquid nitrogen in an interlock chamber mounted on the electron probe column. After the liquid nitrogen is evaporated by creating a vacuum, the sample is pushed into the special stage of the instrument. The sample is maintained at close to liquid nitrogen temperature by circulation of liquid nitrogen in the special stage.


Author(s):  
Louis T. Germinario

A liquid nitrogen stage has been developed for the JEOL JEM-100B electron microscope equipped with a scanning attachment. The design is a modification of the standard JEM-100B SEM specimen holder with specimen cooling to any temperatures In the range ~ 55°K to room temperature. Since the specimen plane is maintained at the ‘high resolution’ focal position of the objective lens and ‘bumping’ and thermal drift la minimized by supercooling the liquid nitrogen, the high resolution capability of the microscope is maintained (Fig.4).


Author(s):  
O. T. Inal ◽  
L. E. Murr

When sharp metal filaments of W, Fe, Nb or Ta are observed in the field-ion microscope (FIM), their appearance is differentiated primarily by variations in regional brightness. This regional brightness, particularly prominent at liquid nitrogen temperature has been attributed in the main to chemical specificity which manifests itself in a paricular array of surface-atom electron-orbital configurations.Recently, anomalous image brightness and streaks in both fcc and bee materials observed in the FIM have been shown to be the result of surface asperities and related topographic features which arise by the unsystematic etching of the emission-tip end forms.


Author(s):  
T. G. Naymik

Three techniques were incorporated for drying clay-rich specimens: air-drying, freeze-drying and critical point drying. In air-drying, the specimens were set out for several days to dry or were placed in an oven (80°F) for several hours. The freeze-dried specimens were frozen by immersion in liquid nitrogen or in isopentane at near liquid nitrogen temperature and then were immediately placed in the freeze-dry vacuum chamber. The critical point specimens were molded in agar immediately after sampling. When the agar had set up the dehydration series, water-alcohol-amyl acetate-CO2 was carried out. The objectives were to compare the fabric plasmas (clays and precipitates), fabricskeletons (quartz grains) and the relationship between them for each drying technique. The three drying methods are not only applicable to the study of treated soils, but can be incorporated into all SEM clay soil studies.


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