The optimization of spray-drying process for the development of apricot powder using response surface methodology

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Omar Bashir ◽  
Syed Zameer Hussain ◽  
Tawheed Amin ◽  
Nusrat Jan ◽  
Gousia Gani ◽  
...  

PurposeApricots are not only nutritionally-rich but also possess pharmacological significance owing to their high antioxidant activity, and they are rich in vitamins, fibers, bioactive phytochemicals and minerals. Because of its immense organoleptic characteristics, apricot juice (AJ) is well accepted; however, it has a limited shelf-life, thereby demanding it to be converted into other shelf-stable form. One of the approaches is converting this juice into dehydrated powder. Amongst the various dehydration techniques available, spray drying is usually preferred; however, it involves the use of several independent variables, which need to be optimized, thus prompting to optimize the process to obtain spray dried apricot powder (SDAP) with improved quality.Design/methodology/approachThe spray-drying process of apricot juice was done using the response surface approach. The process variables included the inlet air temperature of 135–220°C, gum arabic concentration of 4–25%, feed flow rate of 124–730 mL/h, feed total soluble solids (TSS) of 10-30°Brix and atomization speed of 11,400–28,000 rpm. The dependent responses were powder yield, hygroscopicity, solubility, moisture content, carotenoids (CT), ascorbic acid (AA), radical scavenging activity (RSA), lightness, wettability, bulk density, particle density and porosity.FindingsAmongst all independent variables, inlet air temperature had most predominant impact on all the investigated responses. The optimum processing conditions for development of apricot powder with optimum quality were 190°C inlet air temperature, 18.99% gum arabic, 300.05 mL/h feed flow rate, 24°Brix feed TSS and 17433.41 rpm atomization speed. The experimental values were found to be in agreement with the predicted values, indicating the suitability of models in predicting optimizing responses of apricot powder. Flowability as Carr's index (CI) (22.36 ± 1.01%) suggests fair flow of powder. Glass transition temperature of powder was 57.85 ± 2.03°C, which is much higher than that of ambient, suggesting its better shelf stability.Originality/valueTo the best of author's knowledge, very limited or very few studies have been carried out on the spray-drying process for the manufacture of SDAP. The results of this investigation will open up new horizons in the field of food industry in the Union Territory of Jammu and Kashmir, India or elsewhere in the apricot-growing areas of India.

2011 ◽  
pp. 15-29
Author(s):  
Mohd Azizi Che Yunus ◽  
Ching Yaw Lee ◽  
Zuhaili Idham

Teknik reka bentuk komposit pusat dalam kaedah gerak balas permukaan (RSM), telah dipilih untuk memeriksa pengaruh parameter-parameter pengeringan sembur terhadap kandungan lembapan dan ketumpatan pukal serbuk buah naga. Pemboleh ubah-pemboleh ubah tak bersandar dengan julat seperti yang disebutkan telah diuji kaji: suhu masukan (156-224°C), kadar aliran suapan (16.6-33.4 ml/min) dan kepekatan maltodextrin (31.6-48.4%). Keputusan menunjukkan bahawa data eksperimen dapat diwakili oleh bentuk polinomial tertib kedua. Bagaimanapun, hanya istilah linear mempunyai pengaruh mutlak terhadap keadaan serbuk. Parameter-parameter terbaik untuk mencapai nilai kandungan lembapan terendah adalah suhu masukan 224°C, kadar aliran suapan 22.9 ml/min dan kepekatan maltodextrin 40%, dengan jangkaan 3.88% kandungan lembapan. Nilai ketumpatan pukal yang maksimum iaitu 0.45 g/ml dicapai pada suhu masukan 156°C, kadar aliran suapan 16.6 ml/min dan kepekatan maltodextrin 48.4%. Kata kunci: Kaedah gerak balas permukaan; sembur kering; buah naga Central Composite Design technique from Response Surface Methodology (RSM) was used to investigate the effects of spray drying conditions on red-fleshed pitaya powder moisture content and bulk density. The spray drying independent variables and ranges are inlet air temperature (156-224°C), feed flow rate (16.6-33.4 ml/min) and maltodextrin concentration (31.6-48.4 %). Results showed that the data were adequately fitted to second order polynomial model. However, only linear terms proved to be significant for powder attributes. The best spray drying conditions within the experimental ranges for minimum powder moisture content of 3.88% would be inlet air temperature, feed flow rate and maltodextrin concentration of 224°C, 22.9 ml/min and 40% respectively. The maximum powder bulk density of 0.45 g/ml was obtained at inlet air temperature of 156°C, 16.6 ml/min feed flow rate and 48.4% maltodextrin concentration. Key words: Response surface methodology; spray-drying; red-fleshed pitaya


Author(s):  
Juan Rodríguez-Ramírez ◽  
Irene Chaparro-Hernández ◽  
Lilia L. Méndez-Lagunas ◽  
Luis Gerardo Barriada-Bernal

In this work the spray drying of the fresh stevia leaves aqueous extract without encapsulating agents was carried out. The effect of the inlet air temperature (160-200 ºC) and the feed flow rate (2-3 kg/h) on the total phenolic content, the total flavonoid content and the antioxidant capacity were evaluated using Folin-Ciocalteau, aluminum chloride and DPPH methods respectively. The inlet air temperature had a significant effect on all parameters evaluated that showed a decrease when increasing the inlet air temperature, the feed flow rate had a significant effect on total flavonoids content and the antioxidant capacity, by increasing the feed flow rate the inhibition of the DPPH radical decreased and the total flavonoid content increased. The treatment at 160 ºC and 3 kg/h retained highest total flavonoid content and the antioxidant capacity. Keywords: Phenolic compounds, stevia, spray drying, antioxidant capacity


2020 ◽  
Vol 87 (3) ◽  
pp. 375-378
Author(s):  
Ahsen Burcin Himmetagaoglu ◽  
Serap Berktas ◽  
Mustafa Cam ◽  
Zafer Erbay

AbstractIn this Research Communication we describe the optimisation of spray drying conditions in the production of microencapsulated cream powder. Oil-in-water emulsions were prepared using maltodextrin (18 DE) and sodium caseinate as wall materials (with the total wall material per total solid content ratio of 30%) and then converted into powder by spray drying. Response surface methodology was used to optimise the factors of spray drying system i.e. inlet drying temperature, feed flow rate, and aspiration rate, where the levels were in the range of 150–190°C, 9–30 ml/min, and 50–100%, respectively. Our objective was to perform spray drying with the highest drying yield and to obtain a microencapsulated cream powder with the highest bulk density, the shortest wetting time, and the lowest surface fat content. The calculated and validated optimum conditions for the spray drying process were found to be 162.8°C for inlet drying temperature, 11.51 ml/min for feed flow rate, and 72.8% for aspiration rate. At these optimum conditions, drying yield, bulk density, wettability, and surface fat content values were 36.37%, 269.9 kg/m3, 115.2 s and 26.2%, respectively.


Author(s):  
Luis F. Cuevas-Glory ◽  
Jorge A. Pino ◽  
Odri Sosa-Moguel ◽  
Enrique Sauri-Duch ◽  
Madai Bringas-Lantigua

Abstract Response surface methodology was used to optimize the spray-drying process for the development of stingless bee honey powder. The independent variables were: inlet air temperature (110–150 oC) and maltodextrin 10DE content (50–70 % wb). The responses were powder yield, moisture, volatiles retention, solubility time, hygroscopicity, bulk loose, and hydroxymethylfurfural content. Powder moisture content, solubility time, hygroscopicity and loose bulk density were negatively affected by inlet air temperature, while powder yield, volatiles retention and hydroxymethylfurfural content were directly related. Powder yield, volatiles retention and solubility time increased with the rise in maltodextrin content, while moisture content, hygroscopicity, loose bulk density and hydroxymethylfurfural content were negatively affected by maltodextrin content. Multiple response optimization indicated that an inlet air temperature of 150 oC and maltodextrin content of 61 % wb were predicted to provide 40 % powder yield, 4.9 % wb moisture content, 71 % volatiles retention, 242 s solubility time and 232 mg/kg hydroxymethylfurfural content.


2014 ◽  
Vol 1033-1034 ◽  
pp. 709-712
Author(s):  
Xian Jun Meng ◽  
Jia Chen Zhang ◽  
Bin Li

The effects of maltodextrin concentration,inlet air temperature and outlet air temperature on the anthocyanins extraction from blueberry pomace by spray-drying technology were studied by response surface methodology. Based on single factor experiment, the quadratic regression model of the powder yield and loss rate of anthocyanins were deduced, then variables were analyzed with response surface methodology (RSM) by Box - Benhnken experiment. Results showed that the optimal technological conditions for spray drying the anthocyanins extraction from blueberry pomace were obtained as follows: maltodextrin concentration was 25.15% , inlet air temperature was 183.03°Cand outlet air temperature was 60.00°C.


2018 ◽  
Vol 69 (5) ◽  
pp. 1149-1151
Author(s):  
Laura Ruxandra Zicman ◽  
Elena Neacsu ◽  
Felicia Nicoleta Dragolici ◽  
Catalin Ciobanu ◽  
Gheorghe Dogaru ◽  
...  

Ultrafiltration of untreated and pretreated aqueous radioactive wastes was conducted using a spiral-wound polysulphonamide membrane. The influence of process factors on its performances was experimental studied and predicted. Permeate volumetric flux and permeate total suspended solids (TSS) were measured at different values of feed flow rate (7 and 10 m3/h), operating pressure (0.1-0.4 MPa), and feed TSS (15 and 60 mg/L). Permeate flux (42-200 L/(m2�h)) increased with feed flow rate and operating pressure as well as it decreased with an increase in feed TSS, whereas permeate TSS (0.1-33.2 mg/L) exhibited an opposite trend. A 23 factorial plan was used to establish correlations between dependent and independent variables of ultrafiltration process.


2020 ◽  
Vol 6 (1) ◽  
Author(s):  
Wasim Akram ◽  
Navneet Garud

Abstract Background Chicory is one of the major source of inulin. In our study, Box–Behnken model/response surface analysis (RSM) was used for the optimization of spray drying process variables to get the maximum inulin yield from chicory (Cichorium intybus L.). For this investigation, the investigational plan utilized three process variables drying temperature (115–125 °C), creep speed (20–24 rpm), and pressure (0.02–0.04 MPa). Result The optimal variables established by applying the Box–Behnken model were as follows: drying temperature 119.20 °C, creep speed 21.64 rpm, and pressure 0.03 MPa. The obtained powdered inulin by spray drying was investigated for the yield value, identification, size, and surface morphology of the particle. The inulin obtained from the spray drying process consists of a fine molecule-sized white powder. Instead, the drying methods shows a significant effect on the morphology and internal configuration of the powdered inulin, as the inulin obtained from spray drying was of a widespread and uniform size and shape, with a rough surface on increase in temperature and smoother surface while increasing the creep speed. The findings indicate that the spray drying with optimum parameters resulted in maximum product yield. Conclusion The outcomes of the study concluded that the product yield through spray drying technique under optimized condition is optimal as compared to other drying technique. Hence, this technique may be applied at commercial scale for the production of inulin.


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Younes Bahammou ◽  
Mounir Kouhila ◽  
Haytem Moussaoui ◽  
Hamza Lamsyehe ◽  
Zakaria Tagnamas ◽  
...  

PurposeThis work aims to study the hydrothermal behavior of mortar cement toward certain environmental factors (ambient air temperature and air velocity) based on its drying kinetics data. The objective is to provide a better understanding and controlling the stability of mortar structures, which integrate the sorption phenomenon, drying process, air pressure and intrinsic characteristics. This leads to predict the comportment of mortar structures in relation with main environmental factors and minimize the risk of cracking mortar structures at an early age.Design/methodology/approachThermokinetic study was carried out in natural and forced convection solar drying at three temperatures 20, 30 and 40°C and three air velocities (1, 3 and 5 m.s-1). The empirical and semiempirical models tested successfully describe the drying kinetics of mortar. These models simulate the drying process of water absorbed by capillarity, which is the most common humidity transfer mechanism in building materials and contain parameters with physical significance, which integrate the effect of several environmental factors and intrinsic characteristics of mortar structures.FindingsThe models simulate the drying process of water absorbed by capillarity, which is the most common humidity transfer mechanism in building materials and contain parameters with physical significance, which integrate the effect of several environmental factors and intrinsic characteristics of mortar structures. The average activation energy obtained expressed the temperature effect on the mortar diffusivity. The drying constant and the diffusion coefficient can be used to predict the influence of these environmental factors on the drying behavior of various building materials and therefore on their durability.Originality/valueEvaluation of the effect of several environmental factors and intrinsic characteristics of mortar structures on their durability.


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