Thermal treatment process of PET bottles filaments using industrial design of experiments

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Syntia Lemos Cotrim ◽  
Ageu Araújo Machado ◽  
Gislaine Camila Lapasini Leal ◽  
Mauro Antonio da Silva Sá Ravagnani ◽  
Edwin Vladimir Cardoza Galdamez
Keyword(s):  
Heat Treatment ◽  
Design Of Experiments ◽  
Treatment Process ◽  
Transformation Process ◽  
Specific Response ◽  
Quality Performance ◽  
Content Type ◽  
Pet Bottles ◽  
Control Factors ◽  
Response Parameter

PurposeThe purpose of this paper is to present the application of Design of Experiments techniques for the analysis of operating parameters of an industrial oven for the heat treatment process of polyethylene terephthalate (PET) bottle filaments.Design/methodology/approachThe focus is on evaluating new ways of operating the transformation process. The main issue is to raise what are the variables interfering with the performance of the oven. The complete 2k factorial for three factors of control was used to analyze the behavior of these variables and their relationships in the specific response parameter for the process.FindingsThe results presented in this work allow the company to have greater knowledge about the operation of the equipment. The study showed possibilities of 14.8% energy reduction.Research limitations/implicationsThe heat treatment activity was characterized as a critical point in the production process, and techniques with empirical approaches, based on statistical techniques, was an opportunity that the company has to improve the execution of activities without major investments for the quality of the final product. The application of statistical quality techniques showed to be very promising.Originality/valueThe fact that the study was conducted using subjective quality performance makes this work different from others presented in the literature, showing the possibility to apply Design of Experiments using main control factors based on the opinion of experienced personnel involved in the process analyzed.

Microstructural, surface and fatigue analysis of stress peened leaf springs

2015 ◽  
Vol 6 (5) ◽  
pp. 589-604 ◽  
Author(s):  
Georgios Savaidis ◽  
Stylianos Karditsas ◽  
Alexander Savaidis ◽  
Roselita Fragoudakis
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Fatigue Life ◽  
Manufacturing Process ◽  
Treatment Process ◽  
High Strength ◽  
Content Type ◽  
Leaf Springs ◽  
Life Analysis ◽  
Fatigue Life Analysis

Purpose – The purpose of this paper is to investigate the fatigue and failure of commercial vehicle serial stress-peened leaf springs, emphasizing the technological impact of the material, the thermal treatment and the stress-peening process on the microstructure, the mechanical properties and the fatigue life. Theoretical fatigue analysis determines the influence of each individual technological parameter. Design engineers can assess the effectiveness of each manufacturing process step qualitatively and quantitatively, and derive conclusions regarding its improvement in terms of mechanical properties and fatigue life. Design/methodology/approach – Two different batches of 51CrV4 were examined to account for potential batch influences. Both specimen batches were subjected to the same heat treatment and stress-peening process. Investigations of their microstructure, hardness and residual stress state on the surface’ areas show the effect of the manufacturing process on the mechanical properties. Wöhler curves have been experimentally determined for the design of high-performance leaf springs. Theoretical fatigue analyses reveal the influence of every above mentioned technological factor on the fatigue life of the specimens. Therewith, the effectiveness and potential for further improvement of the manufacturing process steps are assessed. Findings – Microstructural analysis and hardness measurements quantify the decarburization and the degradation of the specimens’ surface properties. The stress-peening process causes significant compressive residual stresses which improve the fatigue life. On the other hand, it also leads to pronounced surface roughness, which reduces the fatigue life. The theoretical fatigue life analysis assesses the mutual effect of these two parameters. Both parameters cancel each other out in regards to the final effect on fatigue life. The sensitivity of the material and the potential for further improvement of both heat treatment and stress peening is appointed. Research limitations/implications – All quantitative values given here are strictly valid for the present leaf spring batches and should not be widely applied. The results of the present study indicate the sensitivity of high-strength spring steel used here to the various technological factors resulting from the heat treatment and the stress-peening process. In addition, it can be concluded that further research is necessary to improve the two processes (heat treatment process and the stress peening) under serial production conditions. Practical implications – The microstructure investigations in conjunction with the hardness measurements reveal the significant decrease of the mechanical properties of the highly stressed (failure-critical) tensile surface. Therewith, the potential for improvement of the heat treatment process, e.g. in more neutral and controlled atmosphere, can be derived. In addition, significant potential for improvement of the serially applied stress-peening process is revealed. Originality/value – The paper shows a systematic procedure to assess every individual manufacturing factor affecting the microstructure, the surface properties and finally, the fatigue life of leaf springs. An essential result is the quantification of the surface decarburization and its influence on the mechanical properties. The methodology proposed and applied within the theoretical fatigue life analysis to quantify the effect of technological factors on the fatigue life of leaf springs can be extended to any engineering component made of high-strength steel.

Control Factors on the Heat Treatment Process Applied to A537 Steel for Increasing Hardness Using Hardening and Tempering

2020 ◽  
Vol 43 (3) ◽  
pp. 37-42
Author(s):  
Nelu CAZACU ◽  
◽  
◽  
Keyword(s):  
Heat Treatment ◽  
Laboratory Experiments ◽  
Treatment Process ◽  
Heating Temperature ◽  
Taguchi Methods ◽  
Maximum Hardness ◽  
Tempering Temperature ◽  
Control Factors ◽  
Structures And Properties ◽  
Heat Treatment Regime

The paper is based on laboratory experiments of heat treatments applied to samples of A537/A537M steel. The work continues other previous works aimed at modifying structures and properties of this steel, including through surface treatments. The experiments were performed using Taguchi methods from Quality Engineering. A number of four factors were selected as influencing the structure after heat treatment: heating temperature for hardening, cooling rate on hardening, time and tempering temperature. A number of nine experiments were performed using an L9 orthogonal matrix. Objective function was changed to maximum hardness after the heat treatment regime. The results show that the tempering temperature has the greatest influence on the final hardness of the A537 steel samples.

Heat treatment of electron beam melted (EBM) Ti-6Al-4V: microstructure to mechanical property correlations

2018 ◽  
Vol 24 (4) ◽  
pp. 774-783 ◽  
Author(s):  
Srinivasan Raghavan ◽  
Mui Ling Sharon Nai ◽  
Pan Wang ◽  
Wai Jack Sin ◽  
Tao Li ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Mechanical Property ◽  
Electron Beam ◽  
Treatment Process ◽  
Heat Treatment Process ◽  
Post Processing ◽  
Content Type ◽  
Optimal Heat ◽  
Optimal Heat Treatment ◽  
Lath Width

Purpose The paper presents a wide range of post processing heat treatment cycles performed to Electron Beam Melted (EBM) Ti6Al4V alloy and establishes correlations of heat treat process to microstructure and mechanical property (microhardness). The research also identifies the optimal heat treatment to obtain the best microstructure and mechanical properties (hardness and tensile). Design/methodology/approach Rectangular bars fabricated using EBM was used to study the different heat treatment cycles. A variety of heat treatments from sub ß-transus, super ß-transus, near ß-transus and solution aircool plus ageing were designed. After the heat treatment process, the samples were analysed for, α lath width, prior ß grain size, microhardness and nanohardness. Tensile tests were done for the heat treated samples showing most refined α lath structure with uniform globular grains. Findings A clear correlation was observed between α lath width and the microhardness values. The solution aircooled plus aged samples exhibited the best refinement in α-ß morphology with uniform equiaxed grains. The tensile properties of the solution aircooled plus aged samples were comparable to that of the EBM printed samples and better than ASTMF1472 specifications. Originality/value There is hardly any prior work related to post processing heat treatment of EBM built Ti6Al4V other than HIP treatments. The variety of heat treatment cycles and its influence in microstructure and properties, studied in this research, gives a clear understanding on how to tailor final microstructures and select the optimal heat treatment process.

Optimization of Heat Treatment Process of ZE41A Magnesium Alloy Using Grey- Based Taguchi Method

2008 ◽  
Vol 3 (2) ◽  
pp. 63-69
Author(s):  
M. Sivapragash ◽  
◽  
V. Sateeshkumar ◽  
P.R. Lakshminarayanan ◽  
R. Karthikeyan ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Magnesium Alloy ◽  
Taguchi Method ◽  
Treatment Process ◽  
Heat Treatment Process

Teknologi Inokulasi Besi Cor Kelabu FC-250 Untuk Mencegah Pengerasan Pada Dove Tale Produk Ragum Tipe 125

2019 ◽  
Vol 16 (2) ◽  
Author(s):  
Amin Suhadi ◽  
Seodihono
Keyword(s):  
Mechanical Properties ◽  
Cast Iron ◽  
Treatment Process ◽  
Gray Cast Iron ◽  
Spare Parts ◽  
Gray Cast ◽  
Micro Structure ◽  
Control Factors ◽  
Seed Inoculation ◽  
Casting Industry

Production technology of metal casting industry in Indonesia needs to be improved, especially in the manufacturing of spare parts and box engine made of gray cast iron which has various wall thick such as dove tale construction. Microstructure of gray cast iron is influenced by cooling rate during casting, chemical composition and melting treatment process (inoculation). The part which has the thinnest thickness has the fastest cooling therefore, the grain boundary is smaller compared to other section. As a result this part has highest hardness and difficult to be machined. This research is conducted to solve this problem by modifying melting and solidification treatment process. The research starting from micro structure analysis, composition and mechanical properties tests on the product, and then conducting modification treatment through Taguchi method approach. Experimental results obtained show that the best level settings to control factors which affect to the uniformity of the microstructure and mechanical properties in gray cast iron is the addition of seed inoculation super ® 75, as much as 0.25% with the method of inoculation material entering into the Transfer Ladle.Teknologi produksi pada industri pengecoran di Indonesia masih membutuhkan perbaikan terutama dalam pembuatan komponen mesin perkakas dan peralatan pabrik yang terbuat dari besi tuang kelabu yang mempunyai variasi ketebalan yang besar seperti konstruksi ekor burung (dove tale). Pada pengecoran, struktur mikro dari besi tuang kelabu sangat dipengaruhi oleh kecepatan pendinginan, komposisi kimia dan proses perlakuan pada logam cair (inokulasi). Bagian yang mempunyai ukuran paling tipis mempunyai kecepatan pendinigan paling tinggi karena itu ukuran butirnya jauh lebih kecil dari bagian lain, akibatnya bagian ini mempunyai kekerasan lebih tinggi dan sulit dilakukan pengerjaan mesin. Penelitian ini bertujuan untuk memperbaiki hal ini yang terjadi pada dove taledengan cara memodifikasi proses perlakuan pada cairan besi dan proses pendinginan. Penelitian dimulai dari analisa struktur mikro, pengujian komposisi kimia, pengujian sifat mekanis pada produk kemudian dilakukan modifikasi menggunakan pendekatan metode statistik Taguchi. Hasil penelitian menunjukkan bahwa pengaturan terbaik yang dapat diperoleh untuk mendapatkan keseragaman struktur mikro dan sifat mekanis pada pengecoran besi tuang kelabu adalah penambahan seed inoculation super ® 75, sebesar 0.25% dengan metode pemasukan inokulasi kedalam Ladle pengangkut logam cair.Keywords: carbon, micro structure, hardness, inoculation

EFFECT ON HARDNESS and MICRO STRUCTURAL BEHAVIOUR OF TOOL STEEL AFTER HEAT TREATMENT PROCESS

2017 ◽  
Vol 4 (24) ◽  
Author(s):  
Karanbir Singh ◽  
Aditya Chhabra ◽  
Vaibhav Kapoor ◽  
Vaibhav Kapoor
Keyword(s):  
Heat Treatment ◽  
Empirical Study ◽  
Tool Steel ◽  
Treatment Process ◽  
Heat Treatment Process ◽  
Structural Behaviour ◽  
Treatment Processes ◽  
En 31

This study is conducted to analyze the effect on the Hardness and Micro Structural Behaviour of three Sample Grades of Tool Steel i.e. EN-31, EN-8, and D3 after Heat Treatment Processes Such As Annealing, Normalizing, and Hardening and Tempering. The purpose of Selecting Tool Steel is Because Tool Steel is Mostly Used in the Manufacturing Industry.This study is based upon the empirical study which means it is derived from experiment and observation rather than theory.

scholarly journals The effect of heat treatment and impact angle on the erosion behavior of nickel-tungsten carbide cold spray coating using response surface methodology

2021 ◽  
Author(s):  
Marios Kazasidis ◽  
Elisa Verna ◽  
Shuo Yin ◽  
Rocco Lupoi
Keyword(s):  
Heat Treatment ◽  
Response Surface Methodology ◽  
Mass Loss ◽  
Tungsten Carbide ◽  
Response Surface ◽  
Spray Coating ◽  
Impact Angle ◽  
Control Factors ◽  
Heat Treated ◽  
The Impact

AbstractThis study elucidates the performance of cold-sprayed tungsten carbide-nickel coating against solid particle impingement erosion using alumina (corundum) particles. After the coating fabrication, part of the specimens followed two different annealing heat treatment cycles with peak temperatures of 600 °C and 800 °C. The coatings were examined in terms of microstructure in the as-sprayed (AS) and the two heat-treated conditions (HT1, HT2). Subsequently, the erosion tests were carried out using design of experiments with two control factors and two replicate measurements in each case. The effect of the heat treatment on the mass loss of the coatings was investigated at the three levels (AS, HT1, HT2), as well as the impact angle of the erodents (30°, 60°, 90°). Finally, the response surface methodology (RSM) was applied to analyze and optimize the results, building the mathematical models that relate the significant variables and their interactions to the output response (mass loss) for each coating condition. The obtained results demonstrated that erosion minimization was achieved when the coating was heat treated at 600 °C and the angle was 90°.

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